Preparation of electrochromic film by combination of electrostatic spray method/in-situ washing method
Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with t...
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| Autor*in: |
ZHU Chenjie [verfasserIn] CHEN Haiquan [verfasserIn] YU Youhai [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Chinesisch |
| Erschienen: |
2022 |
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In: Cailiao gongcheng ; 50(2022), 1, Seite 109-116 volume:50 ; year:2022 ; number:1 ; pages:109-116 |
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| DOI / URN: |
10.11868/j.issn.1001-4381.2020.001087 |
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| 520 | |a Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with the in-situ elution method. According to the color adaptability and solubility of the electrolyte salt, tetrabutylammonium perchlorate (TBAP) was selected as the template, and different proportions of electrolyte salt were added to the easy-to-process TPA-OMe-PA solution, then film was deposited on the surface of the ITO glass by electrostatic spray technology. After that, the electrolyte salt was precipitated by in-situ washing method. The morphology of the film was analyzed using scanning electron microscope, and the electrochromic properties of the film were studied using the electrochemical workstation combined with ultraviolet/visible/infrared spectrometer. The research results show that the polymer film prepared by electrostatic spray technology and in-situ elution method have multi-level pore structure and excellent electrochromic properties. Especially when the electrolyte content is 33.3%(mass fraction), the multi-layer porosity is the highest, and the electrochromic performance is the best. The bleaching time/coloration time is reduced to 0.6 s/1 s, and the coloration efficiency reaches 608.2 cm2·C-1, which is the best record for the polyamide based electrochromic film. | ||
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10.11868/j.issn.1001-4381.2020.001087 doi (DE-627)DOAJ000560006 (DE-599)DOAJ95f0905a1a4f4c7a88a5978de40683a1 DE-627 ger DE-627 rakwb chi TA401-492 ZHU Chenjie verfasserin aut Preparation of electrochromic film by combination of electrostatic spray method/in-situ washing method 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with the in-situ elution method. According to the color adaptability and solubility of the electrolyte salt, tetrabutylammonium perchlorate (TBAP) was selected as the template, and different proportions of electrolyte salt were added to the easy-to-process TPA-OMe-PA solution, then film was deposited on the surface of the ITO glass by electrostatic spray technology. After that, the electrolyte salt was precipitated by in-situ washing method. The morphology of the film was analyzed using scanning electron microscope, and the electrochromic properties of the film were studied using the electrochemical workstation combined with ultraviolet/visible/infrared spectrometer. The research results show that the polymer film prepared by electrostatic spray technology and in-situ elution method have multi-level pore structure and excellent electrochromic properties. Especially when the electrolyte content is 33.3%(mass fraction), the multi-layer porosity is the highest, and the electrochromic performance is the best. The bleaching time/coloration time is reduced to 0.6 s/1 s, and the coloration efficiency reaches 608.2 cm2·C-1, which is the best record for the polyamide based electrochromic film. electrochromic film electrostatic spray deposition in-situ washing method multi-level pore structure electrochemical performance Materials of engineering and construction. Mechanics of materials CHEN Haiquan verfasserin aut YU Youhai verfasserin aut In Cailiao gongcheng 50(2022), 1, Seite 109-116 volume:50 year:2022 number:1 pages:109-116 https://doi.org/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/article/95f0905a1a4f4c7a88a5978de40683a1 kostenfrei http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/toc/1001-4381 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ AR 50 2022 1 109-116 |
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10.11868/j.issn.1001-4381.2020.001087 doi (DE-627)DOAJ000560006 (DE-599)DOAJ95f0905a1a4f4c7a88a5978de40683a1 DE-627 ger DE-627 rakwb chi TA401-492 ZHU Chenjie verfasserin aut Preparation of electrochromic film by combination of electrostatic spray method/in-situ washing method 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with the in-situ elution method. According to the color adaptability and solubility of the electrolyte salt, tetrabutylammonium perchlorate (TBAP) was selected as the template, and different proportions of electrolyte salt were added to the easy-to-process TPA-OMe-PA solution, then film was deposited on the surface of the ITO glass by electrostatic spray technology. After that, the electrolyte salt was precipitated by in-situ washing method. The morphology of the film was analyzed using scanning electron microscope, and the electrochromic properties of the film were studied using the electrochemical workstation combined with ultraviolet/visible/infrared spectrometer. The research results show that the polymer film prepared by electrostatic spray technology and in-situ elution method have multi-level pore structure and excellent electrochromic properties. Especially when the electrolyte content is 33.3%(mass fraction), the multi-layer porosity is the highest, and the electrochromic performance is the best. The bleaching time/coloration time is reduced to 0.6 s/1 s, and the coloration efficiency reaches 608.2 cm2·C-1, which is the best record for the polyamide based electrochromic film. electrochromic film electrostatic spray deposition in-situ washing method multi-level pore structure electrochemical performance Materials of engineering and construction. Mechanics of materials CHEN Haiquan verfasserin aut YU Youhai verfasserin aut In Cailiao gongcheng 50(2022), 1, Seite 109-116 volume:50 year:2022 number:1 pages:109-116 https://doi.org/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/article/95f0905a1a4f4c7a88a5978de40683a1 kostenfrei http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/toc/1001-4381 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ AR 50 2022 1 109-116 |
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10.11868/j.issn.1001-4381.2020.001087 doi (DE-627)DOAJ000560006 (DE-599)DOAJ95f0905a1a4f4c7a88a5978de40683a1 DE-627 ger DE-627 rakwb chi TA401-492 ZHU Chenjie verfasserin aut Preparation of electrochromic film by combination of electrostatic spray method/in-situ washing method 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with the in-situ elution method. According to the color adaptability and solubility of the electrolyte salt, tetrabutylammonium perchlorate (TBAP) was selected as the template, and different proportions of electrolyte salt were added to the easy-to-process TPA-OMe-PA solution, then film was deposited on the surface of the ITO glass by electrostatic spray technology. After that, the electrolyte salt was precipitated by in-situ washing method. The morphology of the film was analyzed using scanning electron microscope, and the electrochromic properties of the film were studied using the electrochemical workstation combined with ultraviolet/visible/infrared spectrometer. The research results show that the polymer film prepared by electrostatic spray technology and in-situ elution method have multi-level pore structure and excellent electrochromic properties. Especially when the electrolyte content is 33.3%(mass fraction), the multi-layer porosity is the highest, and the electrochromic performance is the best. The bleaching time/coloration time is reduced to 0.6 s/1 s, and the coloration efficiency reaches 608.2 cm2·C-1, which is the best record for the polyamide based electrochromic film. electrochromic film electrostatic spray deposition in-situ washing method multi-level pore structure electrochemical performance Materials of engineering and construction. Mechanics of materials CHEN Haiquan verfasserin aut YU Youhai verfasserin aut In Cailiao gongcheng 50(2022), 1, Seite 109-116 volume:50 year:2022 number:1 pages:109-116 https://doi.org/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/article/95f0905a1a4f4c7a88a5978de40683a1 kostenfrei http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/toc/1001-4381 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ AR 50 2022 1 109-116 |
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10.11868/j.issn.1001-4381.2020.001087 doi (DE-627)DOAJ000560006 (DE-599)DOAJ95f0905a1a4f4c7a88a5978de40683a1 DE-627 ger DE-627 rakwb chi TA401-492 ZHU Chenjie verfasserin aut Preparation of electrochromic film by combination of electrostatic spray method/in-situ washing method 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with the in-situ elution method. According to the color adaptability and solubility of the electrolyte salt, tetrabutylammonium perchlorate (TBAP) was selected as the template, and different proportions of electrolyte salt were added to the easy-to-process TPA-OMe-PA solution, then film was deposited on the surface of the ITO glass by electrostatic spray technology. After that, the electrolyte salt was precipitated by in-situ washing method. The morphology of the film was analyzed using scanning electron microscope, and the electrochromic properties of the film were studied using the electrochemical workstation combined with ultraviolet/visible/infrared spectrometer. The research results show that the polymer film prepared by electrostatic spray technology and in-situ elution method have multi-level pore structure and excellent electrochromic properties. Especially when the electrolyte content is 33.3%(mass fraction), the multi-layer porosity is the highest, and the electrochromic performance is the best. The bleaching time/coloration time is reduced to 0.6 s/1 s, and the coloration efficiency reaches 608.2 cm2·C-1, which is the best record for the polyamide based electrochromic film. electrochromic film electrostatic spray deposition in-situ washing method multi-level pore structure electrochemical performance Materials of engineering and construction. Mechanics of materials CHEN Haiquan verfasserin aut YU Youhai verfasserin aut In Cailiao gongcheng 50(2022), 1, Seite 109-116 volume:50 year:2022 number:1 pages:109-116 https://doi.org/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/article/95f0905a1a4f4c7a88a5978de40683a1 kostenfrei http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/toc/1001-4381 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ AR 50 2022 1 109-116 |
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10.11868/j.issn.1001-4381.2020.001087 doi (DE-627)DOAJ000560006 (DE-599)DOAJ95f0905a1a4f4c7a88a5978de40683a1 DE-627 ger DE-627 rakwb chi TA401-492 ZHU Chenjie verfasserin aut Preparation of electrochromic film by combination of electrostatic spray method/in-situ washing method 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with the in-situ elution method. According to the color adaptability and solubility of the electrolyte salt, tetrabutylammonium perchlorate (TBAP) was selected as the template, and different proportions of electrolyte salt were added to the easy-to-process TPA-OMe-PA solution, then film was deposited on the surface of the ITO glass by electrostatic spray technology. After that, the electrolyte salt was precipitated by in-situ washing method. The morphology of the film was analyzed using scanning electron microscope, and the electrochromic properties of the film were studied using the electrochemical workstation combined with ultraviolet/visible/infrared spectrometer. The research results show that the polymer film prepared by electrostatic spray technology and in-situ elution method have multi-level pore structure and excellent electrochromic properties. Especially when the electrolyte content is 33.3%(mass fraction), the multi-layer porosity is the highest, and the electrochromic performance is the best. The bleaching time/coloration time is reduced to 0.6 s/1 s, and the coloration efficiency reaches 608.2 cm2·C-1, which is the best record for the polyamide based electrochromic film. electrochromic film electrostatic spray deposition in-situ washing method multi-level pore structure electrochemical performance Materials of engineering and construction. Mechanics of materials CHEN Haiquan verfasserin aut YU Youhai verfasserin aut In Cailiao gongcheng 50(2022), 1, Seite 109-116 volume:50 year:2022 number:1 pages:109-116 https://doi.org/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/article/95f0905a1a4f4c7a88a5978de40683a1 kostenfrei http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2020.001087 kostenfrei https://doaj.org/toc/1001-4381 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ AR 50 2022 1 109-116 |
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preparation of electrochromic film by combination of electrostatic spray method/in-situ washing method |
| callnumber |
TA401-492 |
| title_auth |
Preparation of electrochromic film by combination of electrostatic spray method/in-situ washing method |
| abstract |
Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with the in-situ elution method. According to the color adaptability and solubility of the electrolyte salt, tetrabutylammonium perchlorate (TBAP) was selected as the template, and different proportions of electrolyte salt were added to the easy-to-process TPA-OMe-PA solution, then film was deposited on the surface of the ITO glass by electrostatic spray technology. After that, the electrolyte salt was precipitated by in-situ washing method. The morphology of the film was analyzed using scanning electron microscope, and the electrochromic properties of the film were studied using the electrochemical workstation combined with ultraviolet/visible/infrared spectrometer. The research results show that the polymer film prepared by electrostatic spray technology and in-situ elution method have multi-level pore structure and excellent electrochromic properties. Especially when the electrolyte content is 33.3%(mass fraction), the multi-layer porosity is the highest, and the electrochromic performance is the best. The bleaching time/coloration time is reduced to 0.6 s/1 s, and the coloration efficiency reaches 608.2 cm2·C-1, which is the best record for the polyamide based electrochromic film. |
| abstractGer |
Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with the in-situ elution method. According to the color adaptability and solubility of the electrolyte salt, tetrabutylammonium perchlorate (TBAP) was selected as the template, and different proportions of electrolyte salt were added to the easy-to-process TPA-OMe-PA solution, then film was deposited on the surface of the ITO glass by electrostatic spray technology. After that, the electrolyte salt was precipitated by in-situ washing method. The morphology of the film was analyzed using scanning electron microscope, and the electrochromic properties of the film were studied using the electrochemical workstation combined with ultraviolet/visible/infrared spectrometer. The research results show that the polymer film prepared by electrostatic spray technology and in-situ elution method have multi-level pore structure and excellent electrochromic properties. Especially when the electrolyte content is 33.3%(mass fraction), the multi-layer porosity is the highest, and the electrochromic performance is the best. The bleaching time/coloration time is reduced to 0.6 s/1 s, and the coloration efficiency reaches 608.2 cm2·C-1, which is the best record for the polyamide based electrochromic film. |
| abstract_unstemmed |
Electrochromic materials have good development prospect under the development concept of promoting low carbon and energy saving. In order to explore the efficient, simple and excellent preparation process, the polymer electrochromic film was prepared by the electrostatic spray method combined with the in-situ elution method. According to the color adaptability and solubility of the electrolyte salt, tetrabutylammonium perchlorate (TBAP) was selected as the template, and different proportions of electrolyte salt were added to the easy-to-process TPA-OMe-PA solution, then film was deposited on the surface of the ITO glass by electrostatic spray technology. After that, the electrolyte salt was precipitated by in-situ washing method. The morphology of the film was analyzed using scanning electron microscope, and the electrochromic properties of the film were studied using the electrochemical workstation combined with ultraviolet/visible/infrared spectrometer. The research results show that the polymer film prepared by electrostatic spray technology and in-situ elution method have multi-level pore structure and excellent electrochromic properties. Especially when the electrolyte content is 33.3%(mass fraction), the multi-layer porosity is the highest, and the electrochromic performance is the best. The bleaching time/coloration time is reduced to 0.6 s/1 s, and the coloration efficiency reaches 608.2 cm2·C-1, which is the best record for the polyamide based electrochromic film. |
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Preparation of electrochromic film by combination of electrostatic spray method/in-situ washing method |
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https://doi.org/10.11868/j.issn.1001-4381.2020.001087 https://doaj.org/article/95f0905a1a4f4c7a88a5978de40683a1 http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2020.001087 https://doaj.org/toc/1001-4381 |
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CHEN Haiquan YU Youhai |
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CHEN Haiquan YU Youhai |
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TA - General and Civil Engineering |
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10.11868/j.issn.1001-4381.2020.001087 |
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TA401-492 |
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2024-07-03T15:20:19.126Z |
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