Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets

In the present work, we report the results on exfoliation and coating formation of inorganic–organic hybrids based on the layered perovskite-like bismuth titanate H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<·H<...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Iana A. Minich [verfasserIn] Oleg I. Silyukov [verfasserIn] Sergei A. Kurnosenko [verfasserIn] Veronika V. Gak [verfasserIn] Vladimir D. Kalganov [verfasserIn] Petr D. Kolonitskiy [verfasserIn] Irina A. Zvereva [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2021

Schlagwörter:	layered oxides perovskites bismuth titanates exfoliation nanosheets coating

Übergeordnetes Werk:	In: Nanomaterials - MDPI AG, 2012, 11(2021), 10, p 2708
Übergeordnetes Werk:	volume:11 ; year:2021 ; number:10, p 2708

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/nano11102708

Katalog-ID:	DOAJ005834597

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allfieldsGer	10.3390/nano11102708 doi (DE-627)DOAJ005834597 (DE-599)DOAJf200f11c81394129a6185a2ff10a98d2 DE-627 ger DE-627 rakwb eng QD1-999 Iana A. Minich verfasserin aut Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the present work, we report the results on exfoliation and coating formation of inorganic–organic hybrids based on the layered perovskite-like bismuth titanate H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<·H<sub<2</sub<O that could be prepared by a simple ion exchange reaction from a Ruddlesden–Popper phase K<sub<2.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<. The inorganic–organic hybrids were synthesized by intercalation reactions. Exfoliation into nanosheets was performed for the starting hydrated protonated titanate and for the derivatives intercalated by <i<n-</i<alkylamines to study the influence of preliminary intercalation on exfoliation efficiency. The selected precursors were exfoliated in aqueous solutions of tetrabutylammonium hydroxide using facile stirring and ultrasonication. The suspensions of nanosheets obtained were characterized using UV–vis spectrophotometry, dynamic light scattering, inductively coupled plasma spectroscopy, and gravimetry. Nanosheets were coated on preliminarily polyethyleneimine-covered Si substrates using a self-assembly procedure and studied using atomic force and scanning electron microscopy. layered oxides perovskites bismuth titanates exfoliation nanosheets coating Chemistry Oleg I. Silyukov verfasserin aut Sergei A. Kurnosenko verfasserin aut Veronika V. Gak verfasserin aut Vladimir D. Kalganov verfasserin aut Petr D. Kolonitskiy verfasserin aut Irina A. Zvereva verfasserin aut In Nanomaterials MDPI AG, 2012 11(2021), 10, p 2708 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:11 year:2021 number:10, p 2708 https://doi.org/10.3390/nano11102708 kostenfrei https://doaj.org/article/f200f11c81394129a6185a2ff10a98d2 kostenfrei https://www.mdpi.com/2079-4991/11/10/2708 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 11 2021 10, p 2708
allfieldsSound	10.3390/nano11102708 doi (DE-627)DOAJ005834597 (DE-599)DOAJf200f11c81394129a6185a2ff10a98d2 DE-627 ger DE-627 rakwb eng QD1-999 Iana A. Minich verfasserin aut Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the present work, we report the results on exfoliation and coating formation of inorganic–organic hybrids based on the layered perovskite-like bismuth titanate H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<·H<sub<2</sub<O that could be prepared by a simple ion exchange reaction from a Ruddlesden–Popper phase K<sub<2.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<. The inorganic–organic hybrids were synthesized by intercalation reactions. Exfoliation into nanosheets was performed for the starting hydrated protonated titanate and for the derivatives intercalated by <i<n-</i<alkylamines to study the influence of preliminary intercalation on exfoliation efficiency. The selected precursors were exfoliated in aqueous solutions of tetrabutylammonium hydroxide using facile stirring and ultrasonication. The suspensions of nanosheets obtained were characterized using UV–vis spectrophotometry, dynamic light scattering, inductively coupled plasma spectroscopy, and gravimetry. Nanosheets were coated on preliminarily polyethyleneimine-covered Si substrates using a self-assembly procedure and studied using atomic force and scanning electron microscopy. layered oxides perovskites bismuth titanates exfoliation nanosheets coating Chemistry Oleg I. Silyukov verfasserin aut Sergei A. Kurnosenko verfasserin aut Veronika V. Gak verfasserin aut Vladimir D. Kalganov verfasserin aut Petr D. Kolonitskiy verfasserin aut Irina A. Zvereva verfasserin aut In Nanomaterials MDPI AG, 2012 11(2021), 10, p 2708 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:11 year:2021 number:10, p 2708 https://doi.org/10.3390/nano11102708 kostenfrei https://doaj.org/article/f200f11c81394129a6185a2ff10a98d2 kostenfrei https://www.mdpi.com/2079-4991/11/10/2708 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 11 2021 10, p 2708
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authorswithroles_txt_mv	Iana A. Minich @@aut@@ Oleg I. Silyukov @@aut@@ Sergei A. Kurnosenko @@aut@@ Veronika V. Gak @@aut@@ Vladimir D. Kalganov @@aut@@ Petr D. Kolonitskiy @@aut@@ Irina A. Zvereva @@aut@@
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callnumber-first	Q - Science
author	Iana A. Minich
spellingShingle	Iana A. Minich misc QD1-999 misc layered oxides misc perovskites misc bismuth titanates misc exfoliation misc nanosheets misc coating misc Chemistry Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets
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topic_title	QD1-999 Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets layered oxides perovskites bismuth titanates exfoliation nanosheets coating
topic	misc QD1-999 misc layered oxides misc perovskites misc bismuth titanates misc exfoliation misc nanosheets misc coating misc Chemistry
topic_unstemmed	misc QD1-999 misc layered oxides misc perovskites misc bismuth titanates misc exfoliation misc nanosheets misc coating misc Chemistry
topic_browse	misc QD1-999 misc layered oxides misc perovskites misc bismuth titanates misc exfoliation misc nanosheets misc coating misc Chemistry
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title	Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets
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title_full	Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets
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author_browse	Iana A. Minich Oleg I. Silyukov Sergei A. Kurnosenko Veronika V. Gak Vladimir D. Kalganov Petr D. Kolonitskiy Irina A. Zvereva
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author-letter	Iana A. Minich
doi_str_mv	10.3390/nano11102708
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title_sort	physical–chemical exfoliation of <i<n-</i<alkylamine derivatives of layered perovskite-like oxide h<sub<2</sub<k<sub<0.5</sub<bi<sub<2.5</sub<ti<sub<4</sub<o<sub<13</sub< into nanosheets
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title_auth	Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets
abstract	In the present work, we report the results on exfoliation and coating formation of inorganic–organic hybrids based on the layered perovskite-like bismuth titanate H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<·H<sub<2</sub<O that could be prepared by a simple ion exchange reaction from a Ruddlesden–Popper phase K<sub<2.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<. The inorganic–organic hybrids were synthesized by intercalation reactions. Exfoliation into nanosheets was performed for the starting hydrated protonated titanate and for the derivatives intercalated by <i<n-</i<alkylamines to study the influence of preliminary intercalation on exfoliation efficiency. The selected precursors were exfoliated in aqueous solutions of tetrabutylammonium hydroxide using facile stirring and ultrasonication. The suspensions of nanosheets obtained were characterized using UV–vis spectrophotometry, dynamic light scattering, inductively coupled plasma spectroscopy, and gravimetry. Nanosheets were coated on preliminarily polyethyleneimine-covered Si substrates using a self-assembly procedure and studied using atomic force and scanning electron microscopy.
abstractGer	In the present work, we report the results on exfoliation and coating formation of inorganic–organic hybrids based on the layered perovskite-like bismuth titanate H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<·H<sub<2</sub<O that could be prepared by a simple ion exchange reaction from a Ruddlesden–Popper phase K<sub<2.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<. The inorganic–organic hybrids were synthesized by intercalation reactions. Exfoliation into nanosheets was performed for the starting hydrated protonated titanate and for the derivatives intercalated by <i<n-</i<alkylamines to study the influence of preliminary intercalation on exfoliation efficiency. The selected precursors were exfoliated in aqueous solutions of tetrabutylammonium hydroxide using facile stirring and ultrasonication. The suspensions of nanosheets obtained were characterized using UV–vis spectrophotometry, dynamic light scattering, inductively coupled plasma spectroscopy, and gravimetry. Nanosheets were coated on preliminarily polyethyleneimine-covered Si substrates using a self-assembly procedure and studied using atomic force and scanning electron microscopy.
abstract_unstemmed	In the present work, we report the results on exfoliation and coating formation of inorganic–organic hybrids based on the layered perovskite-like bismuth titanate H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<·H<sub<2</sub<O that could be prepared by a simple ion exchange reaction from a Ruddlesden–Popper phase K<sub<2.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<. The inorganic–organic hybrids were synthesized by intercalation reactions. Exfoliation into nanosheets was performed for the starting hydrated protonated titanate and for the derivatives intercalated by <i<n-</i<alkylamines to study the influence of preliminary intercalation on exfoliation efficiency. The selected precursors were exfoliated in aqueous solutions of tetrabutylammonium hydroxide using facile stirring and ultrasonication. The suspensions of nanosheets obtained were characterized using UV–vis spectrophotometry, dynamic light scattering, inductively coupled plasma spectroscopy, and gravimetry. Nanosheets were coated on preliminarily polyethyleneimine-covered Si substrates using a self-assembly procedure and studied using atomic force and scanning electron microscopy.
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title_short	Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets
url	https://doi.org/10.3390/nano11102708 https://doaj.org/article/f200f11c81394129a6185a2ff10a98d2 https://www.mdpi.com/2079-4991/11/10/2708 https://doaj.org/toc/2079-4991
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author2	Oleg I. Silyukov Sergei A. Kurnosenko Veronika V. Gak Vladimir D. Kalganov Petr D. Kolonitskiy Irina A. Zvereva
author2Str	Oleg I. Silyukov Sergei A. Kurnosenko Veronika V. Gak Vladimir D. Kalganov Petr D. Kolonitskiy Irina A. Zvereva
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Minich</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2021</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">In the present work, we report the results on exfoliation and coating formation of inorganic–organic hybrids based on the layered perovskite-like bismuth titanate H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<·H<sub<2</sub<O that could be prepared by a simple ion exchange reaction from a Ruddlesden–Popper phase K<sub<2.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub<. The inorganic–organic hybrids were synthesized by intercalation reactions. Exfoliation into nanosheets was performed for the starting hydrated protonated titanate and for the derivatives intercalated by <i<n-</i<alkylamines to study the influence of preliminary intercalation on exfoliation efficiency. The selected precursors were exfoliated in aqueous solutions of tetrabutylammonium hydroxide using facile stirring and ultrasonication. The suspensions of nanosheets obtained were characterized using UV–vis spectrophotometry, dynamic light scattering, inductively coupled plasma spectroscopy, and gravimetry. 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Physical–Chemical Exfoliation of <i<n-</i<Alkylamine Derivatives of Layered Perovskite-like Oxide H<sub<2</sub<K<sub<0.5</sub<Bi<sub<2.5</sub<Ti<sub<4</sub<O<sub<13</sub< into Nanosheets

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