Metathesis reactions with a low-cost spinning disk system

Experimental procedures have been developed to provide at the laboratory scale an efficient and relatively inexpensive continuous flow processing system to undertake metathesis chemistry. Glass discs, coated with porous silica particles impregnated with Grubbs (I) generation or Hoveyda–Grubbs (II) g...
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Autor*in:	Shahid A. Kazi [verfasserIn] Peter Clark [verfasserIn] Eva. M. Campi [verfasserIn] W. Roy Jackson [verfasserIn] Milton T. W. Hearn [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2019

Schlagwörter:	metathesis reactions spinning disc reactors catalyst-coated silica in situ product separation

Übergeordnetes Werk:	In: Green Chemistry Letters and Reviews - Taylor & Francis Group, 2015, 12(2019), 4, Seite 407-419
Übergeordnetes Werk:	volume:12 ; year:2019 ; number:4 ; pages:407-419

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc Journal toc

DOI / URN:	10.1080/17518253.2019.1679264

Katalog-ID:	DOAJ006484409

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language	English
source	In Green Chemistry Letters and Reviews 12(2019), 4, Seite 407-419 volume:12 year:2019 number:4 pages:407-419
sourceStr	In Green Chemistry Letters and Reviews 12(2019), 4, Seite 407-419 volume:12 year:2019 number:4 pages:407-419
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	metathesis reactions spinning disc reactors catalyst-coated silica in situ product separation Science Q Chemistry
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container_title	Green Chemistry Letters and Reviews
authorswithroles_txt_mv	Shahid A. Kazi @@aut@@ Peter Clark @@aut@@ Eva. M. Campi @@aut@@ W. Roy Jackson @@aut@@ Milton T. W. Hearn @@aut@@
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callnumber-first	Q - Science
author	Shahid A. Kazi
spellingShingle	Shahid A. Kazi misc QD1-999 misc metathesis reactions misc spinning disc reactors misc catalyst-coated silica misc in situ product separation misc Science misc Q misc Chemistry Metathesis reactions with a low-cost spinning disk system
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topic	misc QD1-999 misc metathesis reactions misc spinning disc reactors misc catalyst-coated silica misc in situ product separation misc Science misc Q misc Chemistry
topic_unstemmed	misc QD1-999 misc metathesis reactions misc spinning disc reactors misc catalyst-coated silica misc in situ product separation misc Science misc Q misc Chemistry
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abstract	Experimental procedures have been developed to provide at the laboratory scale an efficient and relatively inexpensive continuous flow processing system to undertake metathesis chemistry. Glass discs, coated with porous silica particles impregnated with Grubbs (I) generation or Hoveyda–Grubbs (II) generation catalysts through non-covalent interactions, have been successfully used as annular zones for in situ metathesis reactions. The supported catalysts were active for ring closing metathesis and self-metathesis reactions with a variety of substrates with nearly quantitative conversion depending on the substrate structure. Advantages of these procedures include the ability to conduct reactions efficiently at small (low mmole) scale under ambient laboratory conditions, thereby avoiding the need for high energy/thermal procedures. Multiple experiments can be undertaken during the same day if catalyst screening is required. Moreover, separation of starting materials from products can be achieved using the same unit operations, avoiding the need for additional purification steps, thereby reducing the total solvent consumption.
abstractGer	Experimental procedures have been developed to provide at the laboratory scale an efficient and relatively inexpensive continuous flow processing system to undertake metathesis chemistry. Glass discs, coated with porous silica particles impregnated with Grubbs (I) generation or Hoveyda–Grubbs (II) generation catalysts through non-covalent interactions, have been successfully used as annular zones for in situ metathesis reactions. The supported catalysts were active for ring closing metathesis and self-metathesis reactions with a variety of substrates with nearly quantitative conversion depending on the substrate structure. Advantages of these procedures include the ability to conduct reactions efficiently at small (low mmole) scale under ambient laboratory conditions, thereby avoiding the need for high energy/thermal procedures. Multiple experiments can be undertaken during the same day if catalyst screening is required. Moreover, separation of starting materials from products can be achieved using the same unit operations, avoiding the need for additional purification steps, thereby reducing the total solvent consumption.
abstract_unstemmed	Experimental procedures have been developed to provide at the laboratory scale an efficient and relatively inexpensive continuous flow processing system to undertake metathesis chemistry. Glass discs, coated with porous silica particles impregnated with Grubbs (I) generation or Hoveyda–Grubbs (II) generation catalysts through non-covalent interactions, have been successfully used as annular zones for in situ metathesis reactions. The supported catalysts were active for ring closing metathesis and self-metathesis reactions with a variety of substrates with nearly quantitative conversion depending on the substrate structure. Advantages of these procedures include the ability to conduct reactions efficiently at small (low mmole) scale under ambient laboratory conditions, thereby avoiding the need for high energy/thermal procedures. Multiple experiments can be undertaken during the same day if catalyst screening is required. Moreover, separation of starting materials from products can be achieved using the same unit operations, avoiding the need for additional purification steps, thereby reducing the total solvent consumption.
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title_short	Metathesis reactions with a low-cost spinning disk system
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Metathesis reactions with a low-cost spinning disk system

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