Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production
The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900°C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phas...
Ausführliche Beschreibung
Autor*in: |
Leandro Marques Correia [verfasserIn] Juan Antonio Cecilia [verfasserIn] Enrique Rodríguez-Castellón [verfasserIn] Célio Loureiro Cavalcante [verfasserIn] Rodrigo Silveira Vieira [verfasserIn] |
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Format: |
E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2017 |
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Übergeordnetes Werk: |
In: Journal of Chemistry - Hindawi Limited, 2012, (2017) |
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Übergeordnetes Werk: |
year:2017 |
Links: |
Link aufrufen |
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DOI / URN: |
10.1155/2017/5679512 |
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Katalog-ID: |
DOAJ007300727 |
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10.1155/2017/5679512 doi (DE-627)DOAJ007300727 (DE-599)DOAJc60c92e3b1a74425aeac04e3fa85558d DE-627 ger DE-627 rakwb eng QD1-999 Leandro Marques Correia verfasserin aut Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900°C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phase of the catalyst. Both precursor and catalyst were characterized using Hammett indicators method, X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TG/DTG), CO2 temperature-programmed desorption (CO2-TPD), X-ray photoelectronic spectroscopy (XPS), Fourier infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N2 adsorption-desorption at −196°C, and distribution particle size. The maximum biodiesel production was of 99.00 ± 0.02 wt.% obtained in the following transesterification reaction conditions: XMR (sunflower oil/methanol molar ratio of 1 : 10.5 mol : mol), XCAT (catalyst loading of 2 wt.%), XTIME (reaction time of 2 h), stirring rate of 1000 rpm, and temperature of 60°C. Chemistry Juan Antonio Cecilia verfasserin aut Enrique Rodríguez-Castellón verfasserin aut Célio Loureiro Cavalcante verfasserin aut Rodrigo Silveira Vieira verfasserin aut In Journal of Chemistry Hindawi Limited, 2012 (2017) (DE-627)736081518 (DE-600)2703077-5 20909071 nnns year:2017 https://doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/article/c60c92e3b1a74425aeac04e3fa85558d kostenfrei http://dx.doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/toc/2090-9063 Journal toc kostenfrei https://doaj.org/toc/2090-9071 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_171 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 2017 |
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10.1155/2017/5679512 doi (DE-627)DOAJ007300727 (DE-599)DOAJc60c92e3b1a74425aeac04e3fa85558d DE-627 ger DE-627 rakwb eng QD1-999 Leandro Marques Correia verfasserin aut Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900°C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phase of the catalyst. Both precursor and catalyst were characterized using Hammett indicators method, X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TG/DTG), CO2 temperature-programmed desorption (CO2-TPD), X-ray photoelectronic spectroscopy (XPS), Fourier infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N2 adsorption-desorption at −196°C, and distribution particle size. The maximum biodiesel production was of 99.00 ± 0.02 wt.% obtained in the following transesterification reaction conditions: XMR (sunflower oil/methanol molar ratio of 1 : 10.5 mol : mol), XCAT (catalyst loading of 2 wt.%), XTIME (reaction time of 2 h), stirring rate of 1000 rpm, and temperature of 60°C. Chemistry Juan Antonio Cecilia verfasserin aut Enrique Rodríguez-Castellón verfasserin aut Célio Loureiro Cavalcante verfasserin aut Rodrigo Silveira Vieira verfasserin aut In Journal of Chemistry Hindawi Limited, 2012 (2017) (DE-627)736081518 (DE-600)2703077-5 20909071 nnns year:2017 https://doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/article/c60c92e3b1a74425aeac04e3fa85558d kostenfrei http://dx.doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/toc/2090-9063 Journal toc kostenfrei https://doaj.org/toc/2090-9071 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_171 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 2017 |
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10.1155/2017/5679512 doi (DE-627)DOAJ007300727 (DE-599)DOAJc60c92e3b1a74425aeac04e3fa85558d DE-627 ger DE-627 rakwb eng QD1-999 Leandro Marques Correia verfasserin aut Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900°C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phase of the catalyst. Both precursor and catalyst were characterized using Hammett indicators method, X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TG/DTG), CO2 temperature-programmed desorption (CO2-TPD), X-ray photoelectronic spectroscopy (XPS), Fourier infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N2 adsorption-desorption at −196°C, and distribution particle size. The maximum biodiesel production was of 99.00 ± 0.02 wt.% obtained in the following transesterification reaction conditions: XMR (sunflower oil/methanol molar ratio of 1 : 10.5 mol : mol), XCAT (catalyst loading of 2 wt.%), XTIME (reaction time of 2 h), stirring rate of 1000 rpm, and temperature of 60°C. Chemistry Juan Antonio Cecilia verfasserin aut Enrique Rodríguez-Castellón verfasserin aut Célio Loureiro Cavalcante verfasserin aut Rodrigo Silveira Vieira verfasserin aut In Journal of Chemistry Hindawi Limited, 2012 (2017) (DE-627)736081518 (DE-600)2703077-5 20909071 nnns year:2017 https://doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/article/c60c92e3b1a74425aeac04e3fa85558d kostenfrei http://dx.doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/toc/2090-9063 Journal toc kostenfrei https://doaj.org/toc/2090-9071 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_171 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 2017 |
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10.1155/2017/5679512 doi (DE-627)DOAJ007300727 (DE-599)DOAJc60c92e3b1a74425aeac04e3fa85558d DE-627 ger DE-627 rakwb eng QD1-999 Leandro Marques Correia verfasserin aut Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900°C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phase of the catalyst. Both precursor and catalyst were characterized using Hammett indicators method, X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TG/DTG), CO2 temperature-programmed desorption (CO2-TPD), X-ray photoelectronic spectroscopy (XPS), Fourier infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N2 adsorption-desorption at −196°C, and distribution particle size. The maximum biodiesel production was of 99.00 ± 0.02 wt.% obtained in the following transesterification reaction conditions: XMR (sunflower oil/methanol molar ratio of 1 : 10.5 mol : mol), XCAT (catalyst loading of 2 wt.%), XTIME (reaction time of 2 h), stirring rate of 1000 rpm, and temperature of 60°C. Chemistry Juan Antonio Cecilia verfasserin aut Enrique Rodríguez-Castellón verfasserin aut Célio Loureiro Cavalcante verfasserin aut Rodrigo Silveira Vieira verfasserin aut In Journal of Chemistry Hindawi Limited, 2012 (2017) (DE-627)736081518 (DE-600)2703077-5 20909071 nnns year:2017 https://doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/article/c60c92e3b1a74425aeac04e3fa85558d kostenfrei http://dx.doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/toc/2090-9063 Journal toc kostenfrei https://doaj.org/toc/2090-9071 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_171 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 2017 |
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10.1155/2017/5679512 doi (DE-627)DOAJ007300727 (DE-599)DOAJc60c92e3b1a74425aeac04e3fa85558d DE-627 ger DE-627 rakwb eng QD1-999 Leandro Marques Correia verfasserin aut Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900°C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phase of the catalyst. Both precursor and catalyst were characterized using Hammett indicators method, X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TG/DTG), CO2 temperature-programmed desorption (CO2-TPD), X-ray photoelectronic spectroscopy (XPS), Fourier infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N2 adsorption-desorption at −196°C, and distribution particle size. The maximum biodiesel production was of 99.00 ± 0.02 wt.% obtained in the following transesterification reaction conditions: XMR (sunflower oil/methanol molar ratio of 1 : 10.5 mol : mol), XCAT (catalyst loading of 2 wt.%), XTIME (reaction time of 2 h), stirring rate of 1000 rpm, and temperature of 60°C. Chemistry Juan Antonio Cecilia verfasserin aut Enrique Rodríguez-Castellón verfasserin aut Célio Loureiro Cavalcante verfasserin aut Rodrigo Silveira Vieira verfasserin aut In Journal of Chemistry Hindawi Limited, 2012 (2017) (DE-627)736081518 (DE-600)2703077-5 20909071 nnns year:2017 https://doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/article/c60c92e3b1a74425aeac04e3fa85558d kostenfrei http://dx.doi.org/10.1155/2017/5679512 kostenfrei https://doaj.org/toc/2090-9063 Journal toc kostenfrei https://doaj.org/toc/2090-9071 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_171 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 2017 |
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Leandro Marques Correia @@aut@@ Juan Antonio Cecilia @@aut@@ Enrique Rodríguez-Castellón @@aut@@ Célio Loureiro Cavalcante @@aut@@ Rodrigo Silveira Vieira @@aut@@ |
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QD1-999 Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production |
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Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production |
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The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900°C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phase of the catalyst. Both precursor and catalyst were characterized using Hammett indicators method, X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TG/DTG), CO2 temperature-programmed desorption (CO2-TPD), X-ray photoelectronic spectroscopy (XPS), Fourier infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N2 adsorption-desorption at −196°C, and distribution particle size. The maximum biodiesel production was of 99.00 ± 0.02 wt.% obtained in the following transesterification reaction conditions: XMR (sunflower oil/methanol molar ratio of 1 : 10.5 mol : mol), XCAT (catalyst loading of 2 wt.%), XTIME (reaction time of 2 h), stirring rate of 1000 rpm, and temperature of 60°C. |
abstractGer |
The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900°C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phase of the catalyst. Both precursor and catalyst were characterized using Hammett indicators method, X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TG/DTG), CO2 temperature-programmed desorption (CO2-TPD), X-ray photoelectronic spectroscopy (XPS), Fourier infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N2 adsorption-desorption at −196°C, and distribution particle size. The maximum biodiesel production was of 99.00 ± 0.02 wt.% obtained in the following transesterification reaction conditions: XMR (sunflower oil/methanol molar ratio of 1 : 10.5 mol : mol), XCAT (catalyst loading of 2 wt.%), XTIME (reaction time of 2 h), stirring rate of 1000 rpm, and temperature of 60°C. |
abstract_unstemmed |
The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900°C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phase of the catalyst. Both precursor and catalyst were characterized using Hammett indicators method, X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TG/DTG), CO2 temperature-programmed desorption (CO2-TPD), X-ray photoelectronic spectroscopy (XPS), Fourier infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N2 adsorption-desorption at −196°C, and distribution particle size. The maximum biodiesel production was of 99.00 ± 0.02 wt.% obtained in the following transesterification reaction conditions: XMR (sunflower oil/methanol molar ratio of 1 : 10.5 mol : mol), XCAT (catalyst loading of 2 wt.%), XTIME (reaction time of 2 h), stirring rate of 1000 rpm, and temperature of 60°C. |
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Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production |
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