INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs)

The effects of sintering temperature on the microstructural and physical properties of NiO-SDCC anode pellets are evaluated in this study. Composite powders of NiO-SDCC (nickel oxide, samarium-doped ceria, Sm0.2Ce0.8O1.9) mixed with binary carbonates (67 mol% Li₂CO₃ and 33 mol% Na₂CO₃) was prepared,...
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Gespeichert in:

Autor*in:	Lily Siong Mahmud [verfasserIn] Somalu Mahendra Rao [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2016

Schlagwörter:	SOFCs Composite NiO-SDCC anode Microstructures Sintering

Übergeordnetes Werk:	In: Ceramics-Silikáty - University of Chemistry and Technology, Prague, 2005, 60(2016), 4, Seite 317-323
Übergeordnetes Werk:	volume:60 ; year:2016 ; number:4 ; pages:317-323

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc Journal toc

DOI / URN:	10.13168/cs.2016.0047

Katalog-ID:	DOAJ009305130

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spelling	10.13168/cs.2016.0047 doi (DE-627)DOAJ009305130 (DE-599)DOAJb0b5c900250c455d84af8ef43756914c DE-627 ger DE-627 rakwb eng TP785-869 Lily Siong Mahmud verfasserin aut INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs) 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The effects of sintering temperature on the microstructural and physical properties of NiO-SDCC anode pellets are evaluated in this study. Composite powders of NiO-SDCC (nickel oxide, samarium-doped ceria, Sm0.2Ce0.8O1.9) mixed with binary carbonates (67 mol% Li₂CO₃ and 33 mol% Na₂CO₃) was prepared, ball-milled, and oven-dried. Carbon black and polyethylene glycol were added to the NiO-SDCC powders as pore former and binder, respectively, to fabricate NiO-SDCC pellets. This mixture was then pressed onto a cylindrical mold under a pressure of 32 MPa. The pellets were subsequently sintered at 600, 700, 800, 900 and 1000 °C for 2 h. Phase transformation, particle size, morphology, and specific surface area (SBET) of the NiO-SDCC composite powder were investigated. Porosity and microstructure of the NiO-SDCC anode pellets were then evaluated after sintering. Results showed that the porosities of the NiO-SDCC pellets decreased as the sintering temperature increased. The increments of sintering temperature reduced the porosity of the pellets, but NiO-SDCC pellets sintered at 800 °C exhibited an acceptable porosity of 32.60%. Furthermore, surface images showed that the microstructures of sintered pellets at 800 °C were well-bonded and kept a uniform particle size distribution. SOFCs Composite NiO-SDCC anode Microstructures Sintering Clay industries. Ceramics. Glass Somalu Mahendra Rao verfasserin aut In Ceramics-Silikáty University of Chemistry and Technology, Prague, 2005 60(2016), 4, Seite 317-323 (DE-627)336453655 (DE-600)2061184-5 18045847 nnns volume:60 year:2016 number:4 pages:317-323 https://doi.org/10.13168/cs.2016.0047 kostenfrei https://doaj.org/article/b0b5c900250c455d84af8ef43756914c kostenfrei http://www.ceramics-silikaty.cz/index.php?page=cs_detail_doi&id=591 kostenfrei https://doaj.org/toc/0862-5468 Journal toc kostenfrei https://doaj.org/toc/1804-5847 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 60 2016 4 317-323
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allfieldsGer	10.13168/cs.2016.0047 doi (DE-627)DOAJ009305130 (DE-599)DOAJb0b5c900250c455d84af8ef43756914c DE-627 ger DE-627 rakwb eng TP785-869 Lily Siong Mahmud verfasserin aut INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs) 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The effects of sintering temperature on the microstructural and physical properties of NiO-SDCC anode pellets are evaluated in this study. Composite powders of NiO-SDCC (nickel oxide, samarium-doped ceria, Sm0.2Ce0.8O1.9) mixed with binary carbonates (67 mol% Li₂CO₃ and 33 mol% Na₂CO₃) was prepared, ball-milled, and oven-dried. Carbon black and polyethylene glycol were added to the NiO-SDCC powders as pore former and binder, respectively, to fabricate NiO-SDCC pellets. This mixture was then pressed onto a cylindrical mold under a pressure of 32 MPa. The pellets were subsequently sintered at 600, 700, 800, 900 and 1000 °C for 2 h. Phase transformation, particle size, morphology, and specific surface area (SBET) of the NiO-SDCC composite powder were investigated. Porosity and microstructure of the NiO-SDCC anode pellets were then evaluated after sintering. Results showed that the porosities of the NiO-SDCC pellets decreased as the sintering temperature increased. The increments of sintering temperature reduced the porosity of the pellets, but NiO-SDCC pellets sintered at 800 °C exhibited an acceptable porosity of 32.60%. Furthermore, surface images showed that the microstructures of sintered pellets at 800 °C were well-bonded and kept a uniform particle size distribution. SOFCs Composite NiO-SDCC anode Microstructures Sintering Clay industries. Ceramics. Glass Somalu Mahendra Rao verfasserin aut In Ceramics-Silikáty University of Chemistry and Technology, Prague, 2005 60(2016), 4, Seite 317-323 (DE-627)336453655 (DE-600)2061184-5 18045847 nnns volume:60 year:2016 number:4 pages:317-323 https://doi.org/10.13168/cs.2016.0047 kostenfrei https://doaj.org/article/b0b5c900250c455d84af8ef43756914c kostenfrei http://www.ceramics-silikaty.cz/index.php?page=cs_detail_doi&id=591 kostenfrei https://doaj.org/toc/0862-5468 Journal toc kostenfrei https://doaj.org/toc/1804-5847 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 60 2016 4 317-323
allfieldsSound	10.13168/cs.2016.0047 doi (DE-627)DOAJ009305130 (DE-599)DOAJb0b5c900250c455d84af8ef43756914c DE-627 ger DE-627 rakwb eng TP785-869 Lily Siong Mahmud verfasserin aut INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs) 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The effects of sintering temperature on the microstructural and physical properties of NiO-SDCC anode pellets are evaluated in this study. Composite powders of NiO-SDCC (nickel oxide, samarium-doped ceria, Sm0.2Ce0.8O1.9) mixed with binary carbonates (67 mol% Li₂CO₃ and 33 mol% Na₂CO₃) was prepared, ball-milled, and oven-dried. Carbon black and polyethylene glycol were added to the NiO-SDCC powders as pore former and binder, respectively, to fabricate NiO-SDCC pellets. This mixture was then pressed onto a cylindrical mold under a pressure of 32 MPa. The pellets were subsequently sintered at 600, 700, 800, 900 and 1000 °C for 2 h. Phase transformation, particle size, morphology, and specific surface area (SBET) of the NiO-SDCC composite powder were investigated. Porosity and microstructure of the NiO-SDCC anode pellets were then evaluated after sintering. Results showed that the porosities of the NiO-SDCC pellets decreased as the sintering temperature increased. The increments of sintering temperature reduced the porosity of the pellets, but NiO-SDCC pellets sintered at 800 °C exhibited an acceptable porosity of 32.60%. Furthermore, surface images showed that the microstructures of sintered pellets at 800 °C were well-bonded and kept a uniform particle size distribution. SOFCs Composite NiO-SDCC anode Microstructures Sintering Clay industries. Ceramics. Glass Somalu Mahendra Rao verfasserin aut In Ceramics-Silikáty University of Chemistry and Technology, Prague, 2005 60(2016), 4, Seite 317-323 (DE-627)336453655 (DE-600)2061184-5 18045847 nnns volume:60 year:2016 number:4 pages:317-323 https://doi.org/10.13168/cs.2016.0047 kostenfrei https://doaj.org/article/b0b5c900250c455d84af8ef43756914c kostenfrei http://www.ceramics-silikaty.cz/index.php?page=cs_detail_doi&id=591 kostenfrei https://doaj.org/toc/0862-5468 Journal toc kostenfrei https://doaj.org/toc/1804-5847 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 60 2016 4 317-323
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source	In Ceramics-Silikáty 60(2016), 4, Seite 317-323 volume:60 year:2016 number:4 pages:317-323
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callnumber-first	T - Technology
author	Lily Siong Mahmud
spellingShingle	Lily Siong Mahmud misc TP785-869 misc SOFCs misc Composite misc NiO-SDCC anode misc Microstructures misc Sintering misc Clay industries. Ceramics. Glass INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs)
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topic_title	TP785-869 INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs) SOFCs Composite NiO-SDCC anode Microstructures Sintering
topic	misc TP785-869 misc SOFCs misc Composite misc NiO-SDCC anode misc Microstructures misc Sintering misc Clay industries. Ceramics. Glass
topic_unstemmed	misc TP785-869 misc SOFCs misc Composite misc NiO-SDCC anode misc Microstructures misc Sintering misc Clay industries. Ceramics. Glass
topic_browse	misc TP785-869 misc SOFCs misc Composite misc NiO-SDCC anode misc Microstructures misc Sintering misc Clay industries. Ceramics. Glass
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title	INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs)
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title_full	INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs)
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author-letter	Lily Siong Mahmud
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title_sort	influence of sintering temperature on nio-sdcc anode for low-temperature solid oxide fuel cells (lt-sofcs)
callnumber	TP785-869
title_auth	INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs)
abstract	The effects of sintering temperature on the microstructural and physical properties of NiO-SDCC anode pellets are evaluated in this study. Composite powders of NiO-SDCC (nickel oxide, samarium-doped ceria, Sm0.2Ce0.8O1.9) mixed with binary carbonates (67 mol% Li₂CO₃ and 33 mol% Na₂CO₃) was prepared, ball-milled, and oven-dried. Carbon black and polyethylene glycol were added to the NiO-SDCC powders as pore former and binder, respectively, to fabricate NiO-SDCC pellets. This mixture was then pressed onto a cylindrical mold under a pressure of 32 MPa. The pellets were subsequently sintered at 600, 700, 800, 900 and 1000 °C for 2 h. Phase transformation, particle size, morphology, and specific surface area (SBET) of the NiO-SDCC composite powder were investigated. Porosity and microstructure of the NiO-SDCC anode pellets were then evaluated after sintering. Results showed that the porosities of the NiO-SDCC pellets decreased as the sintering temperature increased. The increments of sintering temperature reduced the porosity of the pellets, but NiO-SDCC pellets sintered at 800 °C exhibited an acceptable porosity of 32.60%. Furthermore, surface images showed that the microstructures of sintered pellets at 800 °C were well-bonded and kept a uniform particle size distribution.
abstractGer	The effects of sintering temperature on the microstructural and physical properties of NiO-SDCC anode pellets are evaluated in this study. Composite powders of NiO-SDCC (nickel oxide, samarium-doped ceria, Sm0.2Ce0.8O1.9) mixed with binary carbonates (67 mol% Li₂CO₃ and 33 mol% Na₂CO₃) was prepared, ball-milled, and oven-dried. Carbon black and polyethylene glycol were added to the NiO-SDCC powders as pore former and binder, respectively, to fabricate NiO-SDCC pellets. This mixture was then pressed onto a cylindrical mold under a pressure of 32 MPa. The pellets were subsequently sintered at 600, 700, 800, 900 and 1000 °C for 2 h. Phase transformation, particle size, morphology, and specific surface area (SBET) of the NiO-SDCC composite powder were investigated. Porosity and microstructure of the NiO-SDCC anode pellets were then evaluated after sintering. Results showed that the porosities of the NiO-SDCC pellets decreased as the sintering temperature increased. The increments of sintering temperature reduced the porosity of the pellets, but NiO-SDCC pellets sintered at 800 °C exhibited an acceptable porosity of 32.60%. Furthermore, surface images showed that the microstructures of sintered pellets at 800 °C were well-bonded and kept a uniform particle size distribution.
abstract_unstemmed	The effects of sintering temperature on the microstructural and physical properties of NiO-SDCC anode pellets are evaluated in this study. Composite powders of NiO-SDCC (nickel oxide, samarium-doped ceria, Sm0.2Ce0.8O1.9) mixed with binary carbonates (67 mol% Li₂CO₃ and 33 mol% Na₂CO₃) was prepared, ball-milled, and oven-dried. Carbon black and polyethylene glycol were added to the NiO-SDCC powders as pore former and binder, respectively, to fabricate NiO-SDCC pellets. This mixture was then pressed onto a cylindrical mold under a pressure of 32 MPa. The pellets were subsequently sintered at 600, 700, 800, 900 and 1000 °C for 2 h. Phase transformation, particle size, morphology, and specific surface area (SBET) of the NiO-SDCC composite powder were investigated. Porosity and microstructure of the NiO-SDCC anode pellets were then evaluated after sintering. Results showed that the porosities of the NiO-SDCC pellets decreased as the sintering temperature increased. The increments of sintering temperature reduced the porosity of the pellets, but NiO-SDCC pellets sintered at 800 °C exhibited an acceptable porosity of 32.60%. Furthermore, surface images showed that the microstructures of sintered pellets at 800 °C were well-bonded and kept a uniform particle size distribution.
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title_short	INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs)
url	https://doi.org/10.13168/cs.2016.0047 https://doaj.org/article/b0b5c900250c455d84af8ef43756914c http://www.ceramics-silikaty.cz/index.php?page=cs_detail_doi&id=591 https://doaj.org/toc/0862-5468 https://doaj.org/toc/1804-5847
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up_date	2024-07-03T23:01:53.975Z
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INFLUENCE OF SINTERING TEMPERATURE ON NiO-SDCC ANODE FOR LOW-TEMPERATURE SOLID OXIDE FUEL CELLS (LT-SOFCs)

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