2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate

In the title compound, C24H17N2O4+·NO3−·0.25H2O, the central pyridine ring of the 2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium cation is almost coplanar with one benzene ring [dihedral angle = 1.03 (5)°], while it makes dihedral angles of 9.59 (5)° with the other benzene ring and 13.66 (6)° with...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Yaping Li [verfasserIn] Hu Zang [verfasserIn] Guanfang Su [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2012

Übergeordnetes Werk:	In: Acta Crystallographica Section E - International Union of Crystallography, 2005, 68(2012), 1, Seite o43-o43
Übergeordnetes Werk:	volume:68 ; year:2012 ; number:1 ; pages:o43-o43

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1107/S1600536811051506

Katalog-ID:	DOAJ014320029

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allfields	10.1107/S1600536811051506 doi (DE-627)DOAJ014320029 (DE-599)DOAJ61789776d7dd4c62998e07d6fb6f67a0 DE-627 ger DE-627 rakwb eng QD901-999 Yaping Li verfasserin aut 2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the title compound, C24H17N2O4+·NO3−·0.25H2O, the central pyridine ring of the 2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium cation is almost coplanar with one benzene ring [dihedral angle = 1.03 (5)°], while it makes dihedral angles of 9.59 (5)° with the other benzene ring and 13.66 (6)° with the pyridinium ring. In the crystal, N—H...O and O—H...O hydrogen bonds link the cations and nitrate anions into a sheet in the (302) plane. The crystal structure also exhibits π–π interactions between the central pyridine ring and the benzene rings of neighboring molecules [centroid–centroid distance = 3.6756 (13) Å]. Crystallography Hu Zang verfasserin aut Guanfang Su verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 68(2012), 1, Seite o43-o43 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:68 year:2012 number:1 pages:o43-o43 https://doi.org/10.1107/S1600536811051506 kostenfrei https://doaj.org/article/61789776d7dd4c62998e07d6fb6f67a0 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811051506 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 68 2012 1 o43-o43
spelling	10.1107/S1600536811051506 doi (DE-627)DOAJ014320029 (DE-599)DOAJ61789776d7dd4c62998e07d6fb6f67a0 DE-627 ger DE-627 rakwb eng QD901-999 Yaping Li verfasserin aut 2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the title compound, C24H17N2O4+·NO3−·0.25H2O, the central pyridine ring of the 2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium cation is almost coplanar with one benzene ring [dihedral angle = 1.03 (5)°], while it makes dihedral angles of 9.59 (5)° with the other benzene ring and 13.66 (6)° with the pyridinium ring. In the crystal, N—H...O and O—H...O hydrogen bonds link the cations and nitrate anions into a sheet in the (302) plane. The crystal structure also exhibits π–π interactions between the central pyridine ring and the benzene rings of neighboring molecules [centroid–centroid distance = 3.6756 (13) Å]. Crystallography Hu Zang verfasserin aut Guanfang Su verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 68(2012), 1, Seite o43-o43 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:68 year:2012 number:1 pages:o43-o43 https://doi.org/10.1107/S1600536811051506 kostenfrei https://doaj.org/article/61789776d7dd4c62998e07d6fb6f67a0 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811051506 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 68 2012 1 o43-o43
allfields_unstemmed	10.1107/S1600536811051506 doi (DE-627)DOAJ014320029 (DE-599)DOAJ61789776d7dd4c62998e07d6fb6f67a0 DE-627 ger DE-627 rakwb eng QD901-999 Yaping Li verfasserin aut 2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the title compound, C24H17N2O4+·NO3−·0.25H2O, the central pyridine ring of the 2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium cation is almost coplanar with one benzene ring [dihedral angle = 1.03 (5)°], while it makes dihedral angles of 9.59 (5)° with the other benzene ring and 13.66 (6)° with the pyridinium ring. In the crystal, N—H...O and O—H...O hydrogen bonds link the cations and nitrate anions into a sheet in the (302) plane. The crystal structure also exhibits π–π interactions between the central pyridine ring and the benzene rings of neighboring molecules [centroid–centroid distance = 3.6756 (13) Å]. Crystallography Hu Zang verfasserin aut Guanfang Su verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 68(2012), 1, Seite o43-o43 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:68 year:2012 number:1 pages:o43-o43 https://doi.org/10.1107/S1600536811051506 kostenfrei https://doaj.org/article/61789776d7dd4c62998e07d6fb6f67a0 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811051506 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 68 2012 1 o43-o43
allfieldsGer	10.1107/S1600536811051506 doi (DE-627)DOAJ014320029 (DE-599)DOAJ61789776d7dd4c62998e07d6fb6f67a0 DE-627 ger DE-627 rakwb eng QD901-999 Yaping Li verfasserin aut 2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the title compound, C24H17N2O4+·NO3−·0.25H2O, the central pyridine ring of the 2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium cation is almost coplanar with one benzene ring [dihedral angle = 1.03 (5)°], while it makes dihedral angles of 9.59 (5)° with the other benzene ring and 13.66 (6)° with the pyridinium ring. In the crystal, N—H...O and O—H...O hydrogen bonds link the cations and nitrate anions into a sheet in the (302) plane. The crystal structure also exhibits π–π interactions between the central pyridine ring and the benzene rings of neighboring molecules [centroid–centroid distance = 3.6756 (13) Å]. Crystallography Hu Zang verfasserin aut Guanfang Su verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 68(2012), 1, Seite o43-o43 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:68 year:2012 number:1 pages:o43-o43 https://doi.org/10.1107/S1600536811051506 kostenfrei https://doaj.org/article/61789776d7dd4c62998e07d6fb6f67a0 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811051506 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 68 2012 1 o43-o43
allfieldsSound	10.1107/S1600536811051506 doi (DE-627)DOAJ014320029 (DE-599)DOAJ61789776d7dd4c62998e07d6fb6f67a0 DE-627 ger DE-627 rakwb eng QD901-999 Yaping Li verfasserin aut 2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the title compound, C24H17N2O4+·NO3−·0.25H2O, the central pyridine ring of the 2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium cation is almost coplanar with one benzene ring [dihedral angle = 1.03 (5)°], while it makes dihedral angles of 9.59 (5)° with the other benzene ring and 13.66 (6)° with the pyridinium ring. In the crystal, N—H...O and O—H...O hydrogen bonds link the cations and nitrate anions into a sheet in the (302) plane. The crystal structure also exhibits π–π interactions between the central pyridine ring and the benzene rings of neighboring molecules [centroid–centroid distance = 3.6756 (13) Å]. Crystallography Hu Zang verfasserin aut Guanfang Su verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 68(2012), 1, Seite o43-o43 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:68 year:2012 number:1 pages:o43-o43 https://doi.org/10.1107/S1600536811051506 kostenfrei https://doaj.org/article/61789776d7dd4c62998e07d6fb6f67a0 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811051506 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 68 2012 1 o43-o43
language	English
source	In Acta Crystallographica Section E 68(2012), 1, Seite o43-o43 volume:68 year:2012 number:1 pages:o43-o43
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format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Crystallography
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container_title	Acta Crystallographica Section E
authorswithroles_txt_mv	Yaping Li @@aut@@ Hu Zang @@aut@@ Guanfang Su @@aut@@
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callnumber-first	Q - Science
author	Yaping Li
spellingShingle	Yaping Li misc QD901-999 misc Crystallography 2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate
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topic_title	QD901-999 2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate
topic	misc QD901-999 misc Crystallography
topic_unstemmed	misc QD901-999 misc Crystallography
topic_browse	misc QD901-999 misc Crystallography
format_facet	Elektronische Aufsätze Aufsätze Elektronische Ressource
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title	2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate
ctrlnum	(DE-627)DOAJ014320029 (DE-599)DOAJ61789776d7dd4c62998e07d6fb6f67a0
title_full	2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate
author_sort	Yaping Li
journal	Acta Crystallographica Section E
journalStr	Acta Crystallographica Section E
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author_browse	Yaping Li Hu Zang Guanfang Su
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format_se	Elektronische Aufsätze
author-letter	Yaping Li
doi_str_mv	10.1107/S1600536811051506
author2-role	verfasserin
title_sort	2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate
callnumber	QD901-999
title_auth	2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate
abstract	In the title compound, C24H17N2O4+·NO3−·0.25H2O, the central pyridine ring of the 2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium cation is almost coplanar with one benzene ring [dihedral angle = 1.03 (5)°], while it makes dihedral angles of 9.59 (5)° with the other benzene ring and 13.66 (6)° with the pyridinium ring. In the crystal, N—H...O and O—H...O hydrogen bonds link the cations and nitrate anions into a sheet in the (302) plane. The crystal structure also exhibits π–π interactions between the central pyridine ring and the benzene rings of neighboring molecules [centroid–centroid distance = 3.6756 (13) Å].
abstractGer	In the title compound, C24H17N2O4+·NO3−·0.25H2O, the central pyridine ring of the 2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium cation is almost coplanar with one benzene ring [dihedral angle = 1.03 (5)°], while it makes dihedral angles of 9.59 (5)° with the other benzene ring and 13.66 (6)° with the pyridinium ring. In the crystal, N—H...O and O—H...O hydrogen bonds link the cations and nitrate anions into a sheet in the (302) plane. The crystal structure also exhibits π–π interactions between the central pyridine ring and the benzene rings of neighboring molecules [centroid–centroid distance = 3.6756 (13) Å].
abstract_unstemmed	In the title compound, C24H17N2O4+·NO3−·0.25H2O, the central pyridine ring of the 2′,6′-bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium cation is almost coplanar with one benzene ring [dihedral angle = 1.03 (5)°], while it makes dihedral angles of 9.59 (5)° with the other benzene ring and 13.66 (6)° with the pyridinium ring. In the crystal, N—H...O and O—H...O hydrogen bonds link the cations and nitrate anions into a sheet in the (302) plane. The crystal structure also exhibits π–π interactions between the central pyridine ring and the benzene rings of neighboring molecules [centroid–centroid distance = 3.6756 (13) Å].
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container_issue	1
title_short	2′,6′-Bis(4-carboxyphenyl)-4,4′-bipyridin-1-ium nitrate 0.25-hydrate
url	https://doi.org/10.1107/S1600536811051506 https://doaj.org/article/61789776d7dd4c62998e07d6fb6f67a0 http://scripts.iucr.org/cgi-bin/paper?S1600536811051506 https://doaj.org/toc/1600-5368
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doi_str	10.1107/S1600536811051506
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up_date	2024-07-03T22:25:48.855Z
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