Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures

Chemically modified graphene–based materials (CMG) are currently attracting a vast interest in their application in different fields. In particular, heteroatom-doped graphenes have revealed great potentialities in the field of electrocatalysis as substitutes of fuel cell noble metal&nd...
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Autor*in:	Francesco Carraro [verfasserIn] Mattia Cattelan [verfasserIn] Marco Favaro [verfasserIn] Laura Calvillo [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2018

Schlagwörter:	graphene chemically modified graphene crumpled graphene nitrogen doping sulfur doping dual doping aerosol synthesis

Übergeordnetes Werk:	In: Nanomaterials - MDPI AG, 2012, 8(2018), 6, p 406
Übergeordnetes Werk:	volume:8 ; year:2018 ; number:6, p 406

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/nano8060406

Katalog-ID:	DOAJ01458588X

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allfields	10.3390/nano8060406 doi (DE-627)DOAJ01458588X (DE-599)DOAJba5fb46b40cf483f9a24680dded63a1e DE-627 ger DE-627 rakwb eng QD1-999 Francesco Carraro verfasserin aut Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Chemically modified graphene–based materials (CMG) are currently attracting a vast interest in their application in different fields. In particular, heteroatom-doped graphenes have revealed great potentialities in the field of electrocatalysis as substitutes of fuel cell noble metal–based catalysts. In this work, we investigate an innovative process for doping graphene nanostructures. We optimize a novel synthetic route based on aerosol preparation, which allows the simultaneous doping, crumpling, and reduction of graphene oxide (GO). Starting from aqueous solutions containing GO and the dopant precursors, we synthesize N- and N,S-dual-doped 3D graphene nanostructures (N-cGO and N,S-cGO). In the aerosol process, every aerosol droplet can be considered as a microreactor where dopant precursors undergo thermal decomposition and react with the GO flakes. Simultaneously, thanks to the relatively high temperature, GO undergoes crumpling and partial reduction. Using a combination of spectroscopic and microscopic characterization techniques, we investigate the morphology of the obtained materials and the chemical nature of the dopants within the crumpled graphene sheets. This study highlights the versatility of the aerosol process for the design of new CMG materials with tailored electrocatalytic properties. graphene chemically modified graphene crumpled graphene nitrogen doping sulfur doping dual doping aerosol synthesis Chemistry Mattia Cattelan verfasserin aut Marco Favaro verfasserin aut Laura Calvillo verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 6, p 406 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:6, p 406 https://doi.org/10.3390/nano8060406 kostenfrei https://doaj.org/article/ba5fb46b40cf483f9a24680dded63a1e kostenfrei http://www.mdpi.com/2079-4991/8/6/406 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 6, p 406
spelling	10.3390/nano8060406 doi (DE-627)DOAJ01458588X (DE-599)DOAJba5fb46b40cf483f9a24680dded63a1e DE-627 ger DE-627 rakwb eng QD1-999 Francesco Carraro verfasserin aut Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Chemically modified graphene–based materials (CMG) are currently attracting a vast interest in their application in different fields. In particular, heteroatom-doped graphenes have revealed great potentialities in the field of electrocatalysis as substitutes of fuel cell noble metal–based catalysts. In this work, we investigate an innovative process for doping graphene nanostructures. We optimize a novel synthetic route based on aerosol preparation, which allows the simultaneous doping, crumpling, and reduction of graphene oxide (GO). Starting from aqueous solutions containing GO and the dopant precursors, we synthesize N- and N,S-dual-doped 3D graphene nanostructures (N-cGO and N,S-cGO). In the aerosol process, every aerosol droplet can be considered as a microreactor where dopant precursors undergo thermal decomposition and react with the GO flakes. Simultaneously, thanks to the relatively high temperature, GO undergoes crumpling and partial reduction. Using a combination of spectroscopic and microscopic characterization techniques, we investigate the morphology of the obtained materials and the chemical nature of the dopants within the crumpled graphene sheets. This study highlights the versatility of the aerosol process for the design of new CMG materials with tailored electrocatalytic properties. graphene chemically modified graphene crumpled graphene nitrogen doping sulfur doping dual doping aerosol synthesis Chemistry Mattia Cattelan verfasserin aut Marco Favaro verfasserin aut Laura Calvillo verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 6, p 406 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:6, p 406 https://doi.org/10.3390/nano8060406 kostenfrei https://doaj.org/article/ba5fb46b40cf483f9a24680dded63a1e kostenfrei http://www.mdpi.com/2079-4991/8/6/406 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 6, p 406
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allfieldsGer	10.3390/nano8060406 doi (DE-627)DOAJ01458588X (DE-599)DOAJba5fb46b40cf483f9a24680dded63a1e DE-627 ger DE-627 rakwb eng QD1-999 Francesco Carraro verfasserin aut Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Chemically modified graphene–based materials (CMG) are currently attracting a vast interest in their application in different fields. In particular, heteroatom-doped graphenes have revealed great potentialities in the field of electrocatalysis as substitutes of fuel cell noble metal–based catalysts. In this work, we investigate an innovative process for doping graphene nanostructures. We optimize a novel synthetic route based on aerosol preparation, which allows the simultaneous doping, crumpling, and reduction of graphene oxide (GO). Starting from aqueous solutions containing GO and the dopant precursors, we synthesize N- and N,S-dual-doped 3D graphene nanostructures (N-cGO and N,S-cGO). In the aerosol process, every aerosol droplet can be considered as a microreactor where dopant precursors undergo thermal decomposition and react with the GO flakes. Simultaneously, thanks to the relatively high temperature, GO undergoes crumpling and partial reduction. Using a combination of spectroscopic and microscopic characterization techniques, we investigate the morphology of the obtained materials and the chemical nature of the dopants within the crumpled graphene sheets. This study highlights the versatility of the aerosol process for the design of new CMG materials with tailored electrocatalytic properties. graphene chemically modified graphene crumpled graphene nitrogen doping sulfur doping dual doping aerosol synthesis Chemistry Mattia Cattelan verfasserin aut Marco Favaro verfasserin aut Laura Calvillo verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 6, p 406 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:6, p 406 https://doi.org/10.3390/nano8060406 kostenfrei https://doaj.org/article/ba5fb46b40cf483f9a24680dded63a1e kostenfrei http://www.mdpi.com/2079-4991/8/6/406 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 6, p 406
allfieldsSound	10.3390/nano8060406 doi (DE-627)DOAJ01458588X (DE-599)DOAJba5fb46b40cf483f9a24680dded63a1e DE-627 ger DE-627 rakwb eng QD1-999 Francesco Carraro verfasserin aut Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Chemically modified graphene–based materials (CMG) are currently attracting a vast interest in their application in different fields. In particular, heteroatom-doped graphenes have revealed great potentialities in the field of electrocatalysis as substitutes of fuel cell noble metal–based catalysts. In this work, we investigate an innovative process for doping graphene nanostructures. We optimize a novel synthetic route based on aerosol preparation, which allows the simultaneous doping, crumpling, and reduction of graphene oxide (GO). Starting from aqueous solutions containing GO and the dopant precursors, we synthesize N- and N,S-dual-doped 3D graphene nanostructures (N-cGO and N,S-cGO). In the aerosol process, every aerosol droplet can be considered as a microreactor where dopant precursors undergo thermal decomposition and react with the GO flakes. Simultaneously, thanks to the relatively high temperature, GO undergoes crumpling and partial reduction. Using a combination of spectroscopic and microscopic characterization techniques, we investigate the morphology of the obtained materials and the chemical nature of the dopants within the crumpled graphene sheets. This study highlights the versatility of the aerosol process for the design of new CMG materials with tailored electrocatalytic properties. graphene chemically modified graphene crumpled graphene nitrogen doping sulfur doping dual doping aerosol synthesis Chemistry Mattia Cattelan verfasserin aut Marco Favaro verfasserin aut Laura Calvillo verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 6, p 406 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:6, p 406 https://doi.org/10.3390/nano8060406 kostenfrei https://doaj.org/article/ba5fb46b40cf483f9a24680dded63a1e kostenfrei http://www.mdpi.com/2079-4991/8/6/406 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 6, p 406
language	English
source	In Nanomaterials 8(2018), 6, p 406 volume:8 year:2018 number:6, p 406
sourceStr	In Nanomaterials 8(2018), 6, p 406 volume:8 year:2018 number:6, p 406
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	graphene chemically modified graphene crumpled graphene nitrogen doping sulfur doping dual doping aerosol synthesis Chemistry
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container_title	Nanomaterials
authorswithroles_txt_mv	Francesco Carraro @@aut@@ Mattia Cattelan @@aut@@ Marco Favaro @@aut@@ Laura Calvillo @@aut@@
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callnumber-first	Q - Science
author	Francesco Carraro
spellingShingle	Francesco Carraro misc QD1-999 misc graphene misc chemically modified graphene misc crumpled graphene misc nitrogen doping misc sulfur doping misc dual doping misc aerosol synthesis misc Chemistry Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures
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topic	misc QD1-999 misc graphene misc chemically modified graphene misc crumpled graphene misc nitrogen doping misc sulfur doping misc dual doping misc aerosol synthesis misc Chemistry
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title	Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures
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title_full	Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures
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title_sort	aerosol synthesis of n and n-s doped and crumpled graphene nanostructures
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title_auth	Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures
abstract	Chemically modified graphene–based materials (CMG) are currently attracting a vast interest in their application in different fields. In particular, heteroatom-doped graphenes have revealed great potentialities in the field of electrocatalysis as substitutes of fuel cell noble metal–based catalysts. In this work, we investigate an innovative process for doping graphene nanostructures. We optimize a novel synthetic route based on aerosol preparation, which allows the simultaneous doping, crumpling, and reduction of graphene oxide (GO). Starting from aqueous solutions containing GO and the dopant precursors, we synthesize N- and N,S-dual-doped 3D graphene nanostructures (N-cGO and N,S-cGO). In the aerosol process, every aerosol droplet can be considered as a microreactor where dopant precursors undergo thermal decomposition and react with the GO flakes. Simultaneously, thanks to the relatively high temperature, GO undergoes crumpling and partial reduction. Using a combination of spectroscopic and microscopic characterization techniques, we investigate the morphology of the obtained materials and the chemical nature of the dopants within the crumpled graphene sheets. This study highlights the versatility of the aerosol process for the design of new CMG materials with tailored electrocatalytic properties.
abstractGer	Chemically modified graphene–based materials (CMG) are currently attracting a vast interest in their application in different fields. In particular, heteroatom-doped graphenes have revealed great potentialities in the field of electrocatalysis as substitutes of fuel cell noble metal–based catalysts. In this work, we investigate an innovative process for doping graphene nanostructures. We optimize a novel synthetic route based on aerosol preparation, which allows the simultaneous doping, crumpling, and reduction of graphene oxide (GO). Starting from aqueous solutions containing GO and the dopant precursors, we synthesize N- and N,S-dual-doped 3D graphene nanostructures (N-cGO and N,S-cGO). In the aerosol process, every aerosol droplet can be considered as a microreactor where dopant precursors undergo thermal decomposition and react with the GO flakes. Simultaneously, thanks to the relatively high temperature, GO undergoes crumpling and partial reduction. Using a combination of spectroscopic and microscopic characterization techniques, we investigate the morphology of the obtained materials and the chemical nature of the dopants within the crumpled graphene sheets. This study highlights the versatility of the aerosol process for the design of new CMG materials with tailored electrocatalytic properties.
abstract_unstemmed	Chemically modified graphene–based materials (CMG) are currently attracting a vast interest in their application in different fields. In particular, heteroatom-doped graphenes have revealed great potentialities in the field of electrocatalysis as substitutes of fuel cell noble metal–based catalysts. In this work, we investigate an innovative process for doping graphene nanostructures. We optimize a novel synthetic route based on aerosol preparation, which allows the simultaneous doping, crumpling, and reduction of graphene oxide (GO). Starting from aqueous solutions containing GO and the dopant precursors, we synthesize N- and N,S-dual-doped 3D graphene nanostructures (N-cGO and N,S-cGO). In the aerosol process, every aerosol droplet can be considered as a microreactor where dopant precursors undergo thermal decomposition and react with the GO flakes. Simultaneously, thanks to the relatively high temperature, GO undergoes crumpling and partial reduction. Using a combination of spectroscopic and microscopic characterization techniques, we investigate the morphology of the obtained materials and the chemical nature of the dopants within the crumpled graphene sheets. This study highlights the versatility of the aerosol process for the design of new CMG materials with tailored electrocatalytic properties.
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container_issue	6, p 406
title_short	Aerosol Synthesis of N and N-S Doped and Crumpled Graphene Nanostructures
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