O enfoque da metrologia química em análises toxicológicas na atividade turfística: validação de método analítico para determinação de cafeína em matrizes biológicas The chemical metrology approach for toxicological analysis in horseracing: validation of an analytical method for the determination of caffeine in biological matrices

<abstract language="eng"<This paper proposes an alternate method to detect forbidden doping substances present in biological matrices of horseracing. The method was fully validated for caffeine, identified as the most frequent forbidden substance in the analysis conducted by the Anti...
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Gespeichert in:

Autor*in:	India Maria H. de Lima [verfasserIn] Maurício N. Frota [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch ; Spanisch ; Portugiesisch

Erschienen:	2007

Schlagwörter:	metrological reliability toxicological analysis CG-MS

Übergeordnetes Werk:	In: Química Nova - Sociedade Brasileira de Química, 2004, 30(2007), 8, Seite 1820-1829
Übergeordnetes Werk:	volume:30 ; year:2007 ; number:8 ; pages:1820-1829

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc Journal toc

DOI / URN:	10.1590/S0100-40422007000800006

Katalog-ID:	DOAJ014737930

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language	English Spanish Portuguese
source	In Química Nova 30(2007), 8, Seite 1820-1829 volume:30 year:2007 number:8 pages:1820-1829
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authorswithroles_txt_mv	India Maria H. de Lima @@aut@@ Maurício N. Frota @@aut@@
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callnumber-first	Q - Science
author	India Maria H. de Lima
spellingShingle	India Maria H. de Lima misc QD1-999 misc metrological reliability misc toxicological analysis misc CG-MS misc Chemistry O enfoque da metrologia química em análises toxicológicas na atividade turfística: validação de método analítico para determinação de cafeína em matrizes biológicas The chemical metrology approach for toxicological analysis in horseracing: validation of an analytical method for the determination of caffeine in biological matrices
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topic_title	QD1-999 O enfoque da metrologia química em análises toxicológicas na atividade turfística: validação de método analítico para determinação de cafeína em matrizes biológicas The chemical metrology approach for toxicological analysis in horseracing: validation of an analytical method for the determination of caffeine in biological matrices metrological reliability toxicological analysis CG-MS
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title	O enfoque da metrologia química em análises toxicológicas na atividade turfística: validação de método analítico para determinação de cafeína em matrizes biológicas The chemical metrology approach for toxicological analysis in horseracing: validation of an analytical method for the determination of caffeine in biological matrices
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title_full	O enfoque da metrologia química em análises toxicológicas na atividade turfística: validação de método analítico para determinação de cafeína em matrizes biológicas The chemical metrology approach for toxicological analysis in horseracing: validation of an analytical method for the determination of caffeine in biological matrices
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title_sort	enfoque da metrologia química em análises toxicológicas na atividade turfística: validação de método analítico para determinação de cafeína em matrizes biológicas the chemical metrology approach for toxicological analysis in horseracing: validation of an analytical method for the determination of caffeine in biological matrices
callnumber	QD1-999
title_auth	O enfoque da metrologia química em análises toxicológicas na atividade turfística: validação de método analítico para determinação de cafeína em matrizes biológicas The chemical metrology approach for toxicological analysis in horseracing: validation of an analytical method for the determination of caffeine in biological matrices
abstract	<abstract language="eng"<This paper proposes an alternate method to detect forbidden doping substances present in biological matrices of horseracing. The method was fully validated for caffeine, identified as the most frequent forbidden substance in the analysis conducted by the Antidoping Laboratory of the Brazilian Jockey Club, which adopts a zero threshold limit according to national and international horseracing practices. The metrological reliability of the method applied to toxicological analysis in biological matrices is discussed. Although the analytical method proposed for detection of a zero threshold level of the doping substance is qualitative, it was validated for the determination of the limiting value (also known as quantification limit value) introducing a criterion that prevents the issuing of incorrect results ("false-positives" and "false-negatives").
abstractGer	<abstract language="eng"<This paper proposes an alternate method to detect forbidden doping substances present in biological matrices of horseracing. The method was fully validated for caffeine, identified as the most frequent forbidden substance in the analysis conducted by the Antidoping Laboratory of the Brazilian Jockey Club, which adopts a zero threshold limit according to national and international horseracing practices. The metrological reliability of the method applied to toxicological analysis in biological matrices is discussed. Although the analytical method proposed for detection of a zero threshold level of the doping substance is qualitative, it was validated for the determination of the limiting value (also known as quantification limit value) introducing a criterion that prevents the issuing of incorrect results ("false-positives" and "false-negatives").
abstract_unstemmed	<abstract language="eng"<This paper proposes an alternate method to detect forbidden doping substances present in biological matrices of horseracing. The method was fully validated for caffeine, identified as the most frequent forbidden substance in the analysis conducted by the Antidoping Laboratory of the Brazilian Jockey Club, which adopts a zero threshold limit according to national and international horseracing practices. The metrological reliability of the method applied to toxicological analysis in biological matrices is discussed. Although the analytical method proposed for detection of a zero threshold level of the doping substance is qualitative, it was validated for the determination of the limiting value (also known as quantification limit value) introducing a criterion that prevents the issuing of incorrect results ("false-positives" and "false-negatives").
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title_short	O enfoque da metrologia química em análises toxicológicas na atividade turfística: validação de método analítico para determinação de cafeína em matrizes biológicas The chemical metrology approach for toxicological analysis in horseracing: validation of an analytical method for the determination of caffeine in biological matrices
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score	7.400193

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