Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate

The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal,...
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Autor*in:	L.-J. Han [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2011

Übergeordnetes Werk:	In: Acta Crystallographica Section E - International Union of Crystallography, 2005, 67(2011), 4, Seite m514-m514
Übergeordnetes Werk:	volume:67 ; year:2011 ; number:4 ; pages:m514-m514

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1107/S1600536811011202

Katalog-ID:	DOAJ015218783

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520			\|a The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal, complex molecules are linked by Br...Br interactions [3.7049 (10) Å]. The disordered solvent molecule could not be satisfactorily modelled and was therefore eliminated from the final refinement.
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allfields	10.1107/S1600536811011202 doi (DE-627)DOAJ015218783 (DE-599)DOAJ0d274cdd3be5477583da3cebd163a76c DE-627 ger DE-627 rakwb eng QD901-999 L.-J. Han verfasserin aut Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal, complex molecules are linked by Br...Br interactions [3.7049 (10) Å]. The disordered solvent molecule could not be satisfactorily modelled and was therefore eliminated from the final refinement. Crystallography In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 4, Seite m514-m514 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:4 pages:m514-m514 https://doi.org/10.1107/S1600536811011202 kostenfrei https://doaj.org/article/0d274cdd3be5477583da3cebd163a76c kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811011202 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 4 m514-m514
spelling	10.1107/S1600536811011202 doi (DE-627)DOAJ015218783 (DE-599)DOAJ0d274cdd3be5477583da3cebd163a76c DE-627 ger DE-627 rakwb eng QD901-999 L.-J. Han verfasserin aut Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal, complex molecules are linked by Br...Br interactions [3.7049 (10) Å]. The disordered solvent molecule could not be satisfactorily modelled and was therefore eliminated from the final refinement. Crystallography In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 4, Seite m514-m514 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:4 pages:m514-m514 https://doi.org/10.1107/S1600536811011202 kostenfrei https://doaj.org/article/0d274cdd3be5477583da3cebd163a76c kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811011202 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 4 m514-m514
allfields_unstemmed	10.1107/S1600536811011202 doi (DE-627)DOAJ015218783 (DE-599)DOAJ0d274cdd3be5477583da3cebd163a76c DE-627 ger DE-627 rakwb eng QD901-999 L.-J. Han verfasserin aut Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal, complex molecules are linked by Br...Br interactions [3.7049 (10) Å]. The disordered solvent molecule could not be satisfactorily modelled and was therefore eliminated from the final refinement. Crystallography In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 4, Seite m514-m514 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:4 pages:m514-m514 https://doi.org/10.1107/S1600536811011202 kostenfrei https://doaj.org/article/0d274cdd3be5477583da3cebd163a76c kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811011202 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 4 m514-m514
allfieldsGer	10.1107/S1600536811011202 doi (DE-627)DOAJ015218783 (DE-599)DOAJ0d274cdd3be5477583da3cebd163a76c DE-627 ger DE-627 rakwb eng QD901-999 L.-J. Han verfasserin aut Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal, complex molecules are linked by Br...Br interactions [3.7049 (10) Å]. The disordered solvent molecule could not be satisfactorily modelled and was therefore eliminated from the final refinement. Crystallography In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 4, Seite m514-m514 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:4 pages:m514-m514 https://doi.org/10.1107/S1600536811011202 kostenfrei https://doaj.org/article/0d274cdd3be5477583da3cebd163a76c kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811011202 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 4 m514-m514
allfieldsSound	10.1107/S1600536811011202 doi (DE-627)DOAJ015218783 (DE-599)DOAJ0d274cdd3be5477583da3cebd163a76c DE-627 ger DE-627 rakwb eng QD901-999 L.-J. Han verfasserin aut Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal, complex molecules are linked by Br...Br interactions [3.7049 (10) Å]. The disordered solvent molecule could not be satisfactorily modelled and was therefore eliminated from the final refinement. Crystallography In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 4, Seite m514-m514 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:4 pages:m514-m514 https://doi.org/10.1107/S1600536811011202 kostenfrei https://doaj.org/article/0d274cdd3be5477583da3cebd163a76c kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811011202 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 4 m514-m514
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source	In Acta Crystallographica Section E 67(2011), 4, Seite m514-m514 volume:67 year:2011 number:4 pages:m514-m514
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callnumber-first	Q - Science
author	L.-J. Han
spellingShingle	L.-J. Han misc QD901-999 misc Crystallography Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate
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topic_title	QD901-999 Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate
topic	misc QD901-999 misc Crystallography
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title	Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate
ctrlnum	(DE-627)DOAJ015218783 (DE-599)DOAJ0d274cdd3be5477583da3cebd163a76c
title_full	Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate
author_sort	L.-J. Han
journal	Acta Crystallographica Section E
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author-letter	L.-J. Han
doi_str_mv	10.1107/S1600536811011202
title_sort	tetrakis[μ-n,n′-bis(4-bromophenyl)formamidinato-κ2n:n′]dimolybdenum(ii) tetrahydrofuran solvate
callnumber	QD901-999
title_auth	Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate
abstract	The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal, complex molecules are linked by Br...Br interactions [3.7049 (10) Å]. The disordered solvent molecule could not be satisfactorily modelled and was therefore eliminated from the final refinement.
abstractGer	The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal, complex molecules are linked by Br...Br interactions [3.7049 (10) Å]. The disordered solvent molecule could not be satisfactorily modelled and was therefore eliminated from the final refinement.
abstract_unstemmed	The title complex, [Mo2(C13H9N2Br2)4]·C4H8O, contains a quadruply bonded Mo24+ unit equatorially coordinated by four N,N′-bis(4-bromophenyl)formamidinate ligands, forming a dimetal paddlewheel complex. The centroid of the Mo—Mo bond is located on a special position with 2/m symmetry. In the crystal, complex molecules are linked by Br...Br interactions [3.7049 (10) Å]. The disordered solvent molecule could not be satisfactorily modelled and was therefore eliminated from the final refinement.
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container_issue	4
title_short	Tetrakis[μ-N,N′-bis(4-bromophenyl)formamidinato-κ2N:N′]dimolybdenum(II) tetrahydrofuran solvate
url	https://doi.org/10.1107/S1600536811011202 https://doaj.org/article/0d274cdd3be5477583da3cebd163a76c http://scripts.iucr.org/cgi-bin/paper?S1600536811011202 https://doaj.org/toc/1600-5368
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up_date	2024-07-03T13:41:51.160Z
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