Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography

Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing...
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Autor*in:	Xiangyan Li [verfasserIn] Bing Han [verfasserIn] Xuming Yang [verfasserIn] Zhipeng Deng [verfasserIn] Yucheng Zou [verfasserIn] Xiaobo Shi [verfasserIn] Liping Wang [verfasserIn] Yusheng Zhao [verfasserIn] Sudong Wu [verfasserIn] Meng Gu [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2021

Schlagwörter:	Energy materials Materials characterization Materials characterization techniques Materials chemistry Materials science

Übergeordnetes Werk:	In: iScience - Elsevier, 2019, 24(2021), 12, Seite 103418-
Übergeordnetes Werk:	volume:24 ; year:2021 ; number:12 ; pages:103418-

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1016/j.isci.2021.103418

Katalog-ID:	DOAJ015756971

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520			\|a Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing to the lack of 3D characterization techniques and the susceptibility of Li metal anode toward oxygen, moisture, as well as electron beam. Herein, we introduce a successful 3D presentation of deposited Li metal and SEI established via low-dose cryogenic electron microscopy tomography. The Li metal anode is imaged in low-dose mode at different tilt angles and then aligned and reconstructed into a 3D image through an expectation-maximization algorithm. The spherical Li deposits and SEI are confirmed in the 3D tomography of Li metal anode. It is also discovered that the Li metal corrodes and SEI turns concave owing to possible self-discharge after long-time rest.
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allfields	10.1016/j.isci.2021.103418 doi (DE-627)DOAJ015756971 (DE-599)DOAJ6db342749dfd44d7aae0ac938b0ff124 DE-627 ger DE-627 rakwb eng Xiangyan Li verfasserin aut Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing to the lack of 3D characterization techniques and the susceptibility of Li metal anode toward oxygen, moisture, as well as electron beam. Herein, we introduce a successful 3D presentation of deposited Li metal and SEI established via low-dose cryogenic electron microscopy tomography. The Li metal anode is imaged in low-dose mode at different tilt angles and then aligned and reconstructed into a 3D image through an expectation-maximization algorithm. The spherical Li deposits and SEI are confirmed in the 3D tomography of Li metal anode. It is also discovered that the Li metal corrodes and SEI turns concave owing to possible self-discharge after long-time rest. Energy materials Materials characterization Materials characterization techniques Materials chemistry Materials science Science Q Bing Han verfasserin aut Xuming Yang verfasserin aut Zhipeng Deng verfasserin aut Yucheng Zou verfasserin aut Xiaobo Shi verfasserin aut Liping Wang verfasserin aut Yusheng Zhao verfasserin aut Sudong Wu verfasserin aut Meng Gu verfasserin aut In iScience Elsevier, 2019 24(2021), 12, Seite 103418- (DE-627)1019532106 25890042 nnns volume:24 year:2021 number:12 pages:103418- https://doi.org/10.1016/j.isci.2021.103418 kostenfrei https://doaj.org/article/6db342749dfd44d7aae0ac938b0ff124 kostenfrei http://www.sciencedirect.com/science/article/pii/S2589004221013894 kostenfrei https://doaj.org/toc/2589-0042 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_171 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 24 2021 12 103418-
spelling	10.1016/j.isci.2021.103418 doi (DE-627)DOAJ015756971 (DE-599)DOAJ6db342749dfd44d7aae0ac938b0ff124 DE-627 ger DE-627 rakwb eng Xiangyan Li verfasserin aut Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing to the lack of 3D characterization techniques and the susceptibility of Li metal anode toward oxygen, moisture, as well as electron beam. Herein, we introduce a successful 3D presentation of deposited Li metal and SEI established via low-dose cryogenic electron microscopy tomography. The Li metal anode is imaged in low-dose mode at different tilt angles and then aligned and reconstructed into a 3D image through an expectation-maximization algorithm. The spherical Li deposits and SEI are confirmed in the 3D tomography of Li metal anode. It is also discovered that the Li metal corrodes and SEI turns concave owing to possible self-discharge after long-time rest. Energy materials Materials characterization Materials characterization techniques Materials chemistry Materials science Science Q Bing Han verfasserin aut Xuming Yang verfasserin aut Zhipeng Deng verfasserin aut Yucheng Zou verfasserin aut Xiaobo Shi verfasserin aut Liping Wang verfasserin aut Yusheng Zhao verfasserin aut Sudong Wu verfasserin aut Meng Gu verfasserin aut In iScience Elsevier, 2019 24(2021), 12, Seite 103418- (DE-627)1019532106 25890042 nnns volume:24 year:2021 number:12 pages:103418- https://doi.org/10.1016/j.isci.2021.103418 kostenfrei https://doaj.org/article/6db342749dfd44d7aae0ac938b0ff124 kostenfrei http://www.sciencedirect.com/science/article/pii/S2589004221013894 kostenfrei https://doaj.org/toc/2589-0042 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_171 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 24 2021 12 103418-
allfields_unstemmed	10.1016/j.isci.2021.103418 doi (DE-627)DOAJ015756971 (DE-599)DOAJ6db342749dfd44d7aae0ac938b0ff124 DE-627 ger DE-627 rakwb eng Xiangyan Li verfasserin aut Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing to the lack of 3D characterization techniques and the susceptibility of Li metal anode toward oxygen, moisture, as well as electron beam. Herein, we introduce a successful 3D presentation of deposited Li metal and SEI established via low-dose cryogenic electron microscopy tomography. The Li metal anode is imaged in low-dose mode at different tilt angles and then aligned and reconstructed into a 3D image through an expectation-maximization algorithm. The spherical Li deposits and SEI are confirmed in the 3D tomography of Li metal anode. It is also discovered that the Li metal corrodes and SEI turns concave owing to possible self-discharge after long-time rest. Energy materials Materials characterization Materials characterization techniques Materials chemistry Materials science Science Q Bing Han verfasserin aut Xuming Yang verfasserin aut Zhipeng Deng verfasserin aut Yucheng Zou verfasserin aut Xiaobo Shi verfasserin aut Liping Wang verfasserin aut Yusheng Zhao verfasserin aut Sudong Wu verfasserin aut Meng Gu verfasserin aut In iScience Elsevier, 2019 24(2021), 12, Seite 103418- (DE-627)1019532106 25890042 nnns volume:24 year:2021 number:12 pages:103418- https://doi.org/10.1016/j.isci.2021.103418 kostenfrei https://doaj.org/article/6db342749dfd44d7aae0ac938b0ff124 kostenfrei http://www.sciencedirect.com/science/article/pii/S2589004221013894 kostenfrei https://doaj.org/toc/2589-0042 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_171 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 24 2021 12 103418-
allfieldsGer	10.1016/j.isci.2021.103418 doi (DE-627)DOAJ015756971 (DE-599)DOAJ6db342749dfd44d7aae0ac938b0ff124 DE-627 ger DE-627 rakwb eng Xiangyan Li verfasserin aut Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing to the lack of 3D characterization techniques and the susceptibility of Li metal anode toward oxygen, moisture, as well as electron beam. Herein, we introduce a successful 3D presentation of deposited Li metal and SEI established via low-dose cryogenic electron microscopy tomography. The Li metal anode is imaged in low-dose mode at different tilt angles and then aligned and reconstructed into a 3D image through an expectation-maximization algorithm. The spherical Li deposits and SEI are confirmed in the 3D tomography of Li metal anode. It is also discovered that the Li metal corrodes and SEI turns concave owing to possible self-discharge after long-time rest. Energy materials Materials characterization Materials characterization techniques Materials chemistry Materials science Science Q Bing Han verfasserin aut Xuming Yang verfasserin aut Zhipeng Deng verfasserin aut Yucheng Zou verfasserin aut Xiaobo Shi verfasserin aut Liping Wang verfasserin aut Yusheng Zhao verfasserin aut Sudong Wu verfasserin aut Meng Gu verfasserin aut In iScience Elsevier, 2019 24(2021), 12, Seite 103418- (DE-627)1019532106 25890042 nnns volume:24 year:2021 number:12 pages:103418- https://doi.org/10.1016/j.isci.2021.103418 kostenfrei https://doaj.org/article/6db342749dfd44d7aae0ac938b0ff124 kostenfrei http://www.sciencedirect.com/science/article/pii/S2589004221013894 kostenfrei https://doaj.org/toc/2589-0042 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_171 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 24 2021 12 103418-
allfieldsSound	10.1016/j.isci.2021.103418 doi (DE-627)DOAJ015756971 (DE-599)DOAJ6db342749dfd44d7aae0ac938b0ff124 DE-627 ger DE-627 rakwb eng Xiangyan Li verfasserin aut Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing to the lack of 3D characterization techniques and the susceptibility of Li metal anode toward oxygen, moisture, as well as electron beam. Herein, we introduce a successful 3D presentation of deposited Li metal and SEI established via low-dose cryogenic electron microscopy tomography. The Li metal anode is imaged in low-dose mode at different tilt angles and then aligned and reconstructed into a 3D image through an expectation-maximization algorithm. The spherical Li deposits and SEI are confirmed in the 3D tomography of Li metal anode. It is also discovered that the Li metal corrodes and SEI turns concave owing to possible self-discharge after long-time rest. Energy materials Materials characterization Materials characterization techniques Materials chemistry Materials science Science Q Bing Han verfasserin aut Xuming Yang verfasserin aut Zhipeng Deng verfasserin aut Yucheng Zou verfasserin aut Xiaobo Shi verfasserin aut Liping Wang verfasserin aut Yusheng Zhao verfasserin aut Sudong Wu verfasserin aut Meng Gu verfasserin aut In iScience Elsevier, 2019 24(2021), 12, Seite 103418- (DE-627)1019532106 25890042 nnns volume:24 year:2021 number:12 pages:103418- https://doi.org/10.1016/j.isci.2021.103418 kostenfrei https://doaj.org/article/6db342749dfd44d7aae0ac938b0ff124 kostenfrei http://www.sciencedirect.com/science/article/pii/S2589004221013894 kostenfrei https://doaj.org/toc/2589-0042 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_171 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 24 2021 12 103418-
language	English
source	In iScience 24(2021), 12, Seite 103418- volume:24 year:2021 number:12 pages:103418-
sourceStr	In iScience 24(2021), 12, Seite 103418- volume:24 year:2021 number:12 pages:103418-
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Energy materials Materials characterization Materials characterization techniques Materials chemistry Materials science Science Q
isfreeaccess_bool	true
container_title	iScience
authorswithroles_txt_mv	Xiangyan Li @@aut@@ Bing Han @@aut@@ Xuming Yang @@aut@@ Zhipeng Deng @@aut@@ Yucheng Zou @@aut@@ Xiaobo Shi @@aut@@ Liping Wang @@aut@@ Yusheng Zhao @@aut@@ Sudong Wu @@aut@@ Meng Gu @@aut@@
publishDateDaySort_date	2021-01-01T00:00:00Z
hierarchy_top_id	1019532106
id	DOAJ015756971
language_de	englisch
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author	Xiangyan Li
spellingShingle	Xiangyan Li misc Energy materials misc Materials characterization misc Materials characterization techniques misc Materials chemistry misc Materials science misc Science misc Q Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography
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topic_title	Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography Energy materials Materials characterization Materials characterization techniques Materials chemistry Materials science
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title	Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography
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title_full	Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography
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author_browse	Xiangyan Li Bing Han Xuming Yang Zhipeng Deng Yucheng Zou Xiaobo Shi Liping Wang Yusheng Zhao Sudong Wu Meng Gu
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title_sort	three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography
title_auth	Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography
abstract	Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing to the lack of 3D characterization techniques and the susceptibility of Li metal anode toward oxygen, moisture, as well as electron beam. Herein, we introduce a successful 3D presentation of deposited Li metal and SEI established via low-dose cryogenic electron microscopy tomography. The Li metal anode is imaged in low-dose mode at different tilt angles and then aligned and reconstructed into a 3D image through an expectation-maximization algorithm. The spherical Li deposits and SEI are confirmed in the 3D tomography of Li metal anode. It is also discovered that the Li metal corrodes and SEI turns concave owing to possible self-discharge after long-time rest.
abstractGer	Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing to the lack of 3D characterization techniques and the susceptibility of Li metal anode toward oxygen, moisture, as well as electron beam. Herein, we introduce a successful 3D presentation of deposited Li metal and SEI established via low-dose cryogenic electron microscopy tomography. The Li metal anode is imaged in low-dose mode at different tilt angles and then aligned and reconstructed into a 3D image through an expectation-maximization algorithm. The spherical Li deposits and SEI are confirmed in the 3D tomography of Li metal anode. It is also discovered that the Li metal corrodes and SEI turns concave owing to possible self-discharge after long-time rest.
abstract_unstemmed	Summary: The structure of lithium (Li) metal anode, including the Li metal and the solid electrolyte interphase (SEI), is critical to the investigation of cycle stability or decay mechanisms. The three-dimensional (3D) visualization of Li metal and SEI, however, has not been demonstrated yet, owing to the lack of 3D characterization techniques and the susceptibility of Li metal anode toward oxygen, moisture, as well as electron beam. Herein, we introduce a successful 3D presentation of deposited Li metal and SEI established via low-dose cryogenic electron microscopy tomography. The Li metal anode is imaged in low-dose mode at different tilt angles and then aligned and reconstructed into a 3D image through an expectation-maximization algorithm. The spherical Li deposits and SEI are confirmed in the 3D tomography of Li metal anode. It is also discovered that the Li metal corrodes and SEI turns concave owing to possible self-discharge after long-time rest.
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title_short	Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography
url	https://doi.org/10.1016/j.isci.2021.103418 https://doaj.org/article/6db342749dfd44d7aae0ac938b0ff124 http://www.sciencedirect.com/science/article/pii/S2589004221013894 https://doaj.org/toc/2589-0042
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Three-dimensional visualization of lithium metal anode via low-dose cryogenic electron microscopy tomography

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