Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate

The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by...
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Autor*in:	Jinliang Wang [verfasserIn] Huazhou Hu [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2020

Schlagwörter:	Lithium carbonate Lithium bicarbonate Pressure carbonation Microbubble Kinetics

Übergeordnetes Werk:	In: Journal of Materials Research and Technology - Elsevier, 2015, 9(2020), 5, Seite 9498-9505
Übergeordnetes Werk:	volume:9 ; year:2020 ; number:5 ; pages:9498-9505

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1016/j.jmrt.2020.06.089

Katalog-ID:	DOAJ016334795

Internformat


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520			\|a The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by 20–30% compared to that of conventional carbonation methods. The optimum conditions for CO2 carbonation are determined as follows: reaction temperature of 25 °C, pulp density of 60 g L−1, CO2 flow rate of 1.0 L min−1, CO2 partial pressure of 0.4 MPa, reaction time of 120 min, and stirring speed of 400 rpm. The carbonation kinetics of the material is shown to be controlled by surface chemical reactions, with an activation energy of −8.705 kJ mol−1 obtained at 25–55 °C. The mechanism of the surface chemical reactions is further corroborated by XRD patterns and SEM images of the material and the generated residues. Reprecipitation of 83.14% Li in the LiHCO3 solution with 99.99% pure Li2CO3 is achieved via purification and decomposition. This proves the process is possible and practical.
650		4	\|a Lithium carbonate
650		4	\|a Lithium bicarbonate
650		4	\|a Pressure carbonation
650		4	\|a Microbubble
650		4	\|a Kinetics
653		0	\|a Mining engineering. Metallurgy
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912			\|a GBV_ILN_4126
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912			\|a GBV_ILN_4249
912			\|a GBV_ILN_4251
912			\|a GBV_ILN_4305
912			\|a GBV_ILN_4306
912			\|a GBV_ILN_4307
912			\|a GBV_ILN_4313
912			\|a GBV_ILN_4322
912			\|a GBV_ILN_4323
912			\|a GBV_ILN_4324
912			\|a GBV_ILN_4325
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912			\|a GBV_ILN_4333
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912			\|a GBV_ILN_4338
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author_variant	j w jw h h hh
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publishDate	2020
allfields	10.1016/j.jmrt.2020.06.089 doi (DE-627)DOAJ016334795 (DE-599)DOAJ03099f563a4f41b28be7e0870bc65c4d DE-627 ger DE-627 rakwb eng TN1-997 Jinliang Wang verfasserin aut Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by 20–30% compared to that of conventional carbonation methods. The optimum conditions for CO2 carbonation are determined as follows: reaction temperature of 25 °C, pulp density of 60 g L−1, CO2 flow rate of 1.0 L min−1, CO2 partial pressure of 0.4 MPa, reaction time of 120 min, and stirring speed of 400 rpm. The carbonation kinetics of the material is shown to be controlled by surface chemical reactions, with an activation energy of −8.705 kJ mol−1 obtained at 25–55 °C. The mechanism of the surface chemical reactions is further corroborated by XRD patterns and SEM images of the material and the generated residues. Reprecipitation of 83.14% Li in the LiHCO3 solution with 99.99% pure Li2CO3 is achieved via purification and decomposition. This proves the process is possible and practical. Lithium carbonate Lithium bicarbonate Pressure carbonation Microbubble Kinetics Mining engineering. Metallurgy Huazhou Hu verfasserin aut In Journal of Materials Research and Technology Elsevier, 2015 9(2020), 5, Seite 9498-9505 (DE-627)768093163 (DE-600)2732709-7 22140697 nnns volume:9 year:2020 number:5 pages:9498-9505 https://doi.org/10.1016/j.jmrt.2020.06.089 kostenfrei https://doaj.org/article/03099f563a4f41b28be7e0870bc65c4d kostenfrei http://www.sciencedirect.com/science/article/pii/S2238785420314903 kostenfrei https://doaj.org/toc/2238-7854 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 9 2020 5 9498-9505
spelling	10.1016/j.jmrt.2020.06.089 doi (DE-627)DOAJ016334795 (DE-599)DOAJ03099f563a4f41b28be7e0870bc65c4d DE-627 ger DE-627 rakwb eng TN1-997 Jinliang Wang verfasserin aut Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by 20–30% compared to that of conventional carbonation methods. The optimum conditions for CO2 carbonation are determined as follows: reaction temperature of 25 °C, pulp density of 60 g L−1, CO2 flow rate of 1.0 L min−1, CO2 partial pressure of 0.4 MPa, reaction time of 120 min, and stirring speed of 400 rpm. The carbonation kinetics of the material is shown to be controlled by surface chemical reactions, with an activation energy of −8.705 kJ mol−1 obtained at 25–55 °C. The mechanism of the surface chemical reactions is further corroborated by XRD patterns and SEM images of the material and the generated residues. Reprecipitation of 83.14% Li in the LiHCO3 solution with 99.99% pure Li2CO3 is achieved via purification and decomposition. This proves the process is possible and practical. Lithium carbonate Lithium bicarbonate Pressure carbonation Microbubble Kinetics Mining engineering. Metallurgy Huazhou Hu verfasserin aut In Journal of Materials Research and Technology Elsevier, 2015 9(2020), 5, Seite 9498-9505 (DE-627)768093163 (DE-600)2732709-7 22140697 nnns volume:9 year:2020 number:5 pages:9498-9505 https://doi.org/10.1016/j.jmrt.2020.06.089 kostenfrei https://doaj.org/article/03099f563a4f41b28be7e0870bc65c4d kostenfrei http://www.sciencedirect.com/science/article/pii/S2238785420314903 kostenfrei https://doaj.org/toc/2238-7854 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 9 2020 5 9498-9505
allfields_unstemmed	10.1016/j.jmrt.2020.06.089 doi (DE-627)DOAJ016334795 (DE-599)DOAJ03099f563a4f41b28be7e0870bc65c4d DE-627 ger DE-627 rakwb eng TN1-997 Jinliang Wang verfasserin aut Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by 20–30% compared to that of conventional carbonation methods. The optimum conditions for CO2 carbonation are determined as follows: reaction temperature of 25 °C, pulp density of 60 g L−1, CO2 flow rate of 1.0 L min−1, CO2 partial pressure of 0.4 MPa, reaction time of 120 min, and stirring speed of 400 rpm. The carbonation kinetics of the material is shown to be controlled by surface chemical reactions, with an activation energy of −8.705 kJ mol−1 obtained at 25–55 °C. The mechanism of the surface chemical reactions is further corroborated by XRD patterns and SEM images of the material and the generated residues. Reprecipitation of 83.14% Li in the LiHCO3 solution with 99.99% pure Li2CO3 is achieved via purification and decomposition. This proves the process is possible and practical. Lithium carbonate Lithium bicarbonate Pressure carbonation Microbubble Kinetics Mining engineering. Metallurgy Huazhou Hu verfasserin aut In Journal of Materials Research and Technology Elsevier, 2015 9(2020), 5, Seite 9498-9505 (DE-627)768093163 (DE-600)2732709-7 22140697 nnns volume:9 year:2020 number:5 pages:9498-9505 https://doi.org/10.1016/j.jmrt.2020.06.089 kostenfrei https://doaj.org/article/03099f563a4f41b28be7e0870bc65c4d kostenfrei http://www.sciencedirect.com/science/article/pii/S2238785420314903 kostenfrei https://doaj.org/toc/2238-7854 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 9 2020 5 9498-9505
allfieldsGer	10.1016/j.jmrt.2020.06.089 doi (DE-627)DOAJ016334795 (DE-599)DOAJ03099f563a4f41b28be7e0870bc65c4d DE-627 ger DE-627 rakwb eng TN1-997 Jinliang Wang verfasserin aut Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by 20–30% compared to that of conventional carbonation methods. The optimum conditions for CO2 carbonation are determined as follows: reaction temperature of 25 °C, pulp density of 60 g L−1, CO2 flow rate of 1.0 L min−1, CO2 partial pressure of 0.4 MPa, reaction time of 120 min, and stirring speed of 400 rpm. The carbonation kinetics of the material is shown to be controlled by surface chemical reactions, with an activation energy of −8.705 kJ mol−1 obtained at 25–55 °C. The mechanism of the surface chemical reactions is further corroborated by XRD patterns and SEM images of the material and the generated residues. Reprecipitation of 83.14% Li in the LiHCO3 solution with 99.99% pure Li2CO3 is achieved via purification and decomposition. This proves the process is possible and practical. Lithium carbonate Lithium bicarbonate Pressure carbonation Microbubble Kinetics Mining engineering. Metallurgy Huazhou Hu verfasserin aut In Journal of Materials Research and Technology Elsevier, 2015 9(2020), 5, Seite 9498-9505 (DE-627)768093163 (DE-600)2732709-7 22140697 nnns volume:9 year:2020 number:5 pages:9498-9505 https://doi.org/10.1016/j.jmrt.2020.06.089 kostenfrei https://doaj.org/article/03099f563a4f41b28be7e0870bc65c4d kostenfrei http://www.sciencedirect.com/science/article/pii/S2238785420314903 kostenfrei https://doaj.org/toc/2238-7854 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 9 2020 5 9498-9505
allfieldsSound	10.1016/j.jmrt.2020.06.089 doi (DE-627)DOAJ016334795 (DE-599)DOAJ03099f563a4f41b28be7e0870bc65c4d DE-627 ger DE-627 rakwb eng TN1-997 Jinliang Wang verfasserin aut Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by 20–30% compared to that of conventional carbonation methods. The optimum conditions for CO2 carbonation are determined as follows: reaction temperature of 25 °C, pulp density of 60 g L−1, CO2 flow rate of 1.0 L min−1, CO2 partial pressure of 0.4 MPa, reaction time of 120 min, and stirring speed of 400 rpm. The carbonation kinetics of the material is shown to be controlled by surface chemical reactions, with an activation energy of −8.705 kJ mol−1 obtained at 25–55 °C. The mechanism of the surface chemical reactions is further corroborated by XRD patterns and SEM images of the material and the generated residues. Reprecipitation of 83.14% Li in the LiHCO3 solution with 99.99% pure Li2CO3 is achieved via purification and decomposition. This proves the process is possible and practical. Lithium carbonate Lithium bicarbonate Pressure carbonation Microbubble Kinetics Mining engineering. Metallurgy Huazhou Hu verfasserin aut In Journal of Materials Research and Technology Elsevier, 2015 9(2020), 5, Seite 9498-9505 (DE-627)768093163 (DE-600)2732709-7 22140697 nnns volume:9 year:2020 number:5 pages:9498-9505 https://doi.org/10.1016/j.jmrt.2020.06.089 kostenfrei https://doaj.org/article/03099f563a4f41b28be7e0870bc65c4d kostenfrei http://www.sciencedirect.com/science/article/pii/S2238785420314903 kostenfrei https://doaj.org/toc/2238-7854 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 9 2020 5 9498-9505
language	English
source	In Journal of Materials Research and Technology 9(2020), 5, Seite 9498-9505 volume:9 year:2020 number:5 pages:9498-9505
sourceStr	In Journal of Materials Research and Technology 9(2020), 5, Seite 9498-9505 volume:9 year:2020 number:5 pages:9498-9505
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Lithium carbonate Lithium bicarbonate Pressure carbonation Microbubble Kinetics Mining engineering. Metallurgy
isfreeaccess_bool	true
container_title	Journal of Materials Research and Technology
authorswithroles_txt_mv	Jinliang Wang @@aut@@ Huazhou Hu @@aut@@
publishDateDaySort_date	2020-01-01T00:00:00Z
hierarchy_top_id	768093163
id	DOAJ016334795
language_de	englisch
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callnumber-first	T - Technology
author	Jinliang Wang
spellingShingle	Jinliang Wang misc TN1-997 misc Lithium carbonate misc Lithium bicarbonate misc Pressure carbonation misc Microbubble misc Kinetics misc Mining engineering. Metallurgy Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate
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topic_title	TN1-997 Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate Lithium carbonate Lithium bicarbonate Pressure carbonation Microbubble Kinetics
topic	misc TN1-997 misc Lithium carbonate misc Lithium bicarbonate misc Pressure carbonation misc Microbubble misc Kinetics misc Mining engineering. Metallurgy
topic_unstemmed	misc TN1-997 misc Lithium carbonate misc Lithium bicarbonate misc Pressure carbonation misc Microbubble misc Kinetics misc Mining engineering. Metallurgy
topic_browse	misc TN1-997 misc Lithium carbonate misc Lithium bicarbonate misc Pressure carbonation misc Microbubble misc Kinetics misc Mining engineering. Metallurgy
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title	Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate
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title_full	Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate
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doi_str_mv	10.1016/j.jmrt.2020.06.089
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title_sort	microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate
callnumber	TN1-997
title_auth	Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate
abstract	The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by 20–30% compared to that of conventional carbonation methods. The optimum conditions for CO2 carbonation are determined as follows: reaction temperature of 25 °C, pulp density of 60 g L−1, CO2 flow rate of 1.0 L min−1, CO2 partial pressure of 0.4 MPa, reaction time of 120 min, and stirring speed of 400 rpm. The carbonation kinetics of the material is shown to be controlled by surface chemical reactions, with an activation energy of −8.705 kJ mol−1 obtained at 25–55 °C. The mechanism of the surface chemical reactions is further corroborated by XRD patterns and SEM images of the material and the generated residues. Reprecipitation of 83.14% Li in the LiHCO3 solution with 99.99% pure Li2CO3 is achieved via purification and decomposition. This proves the process is possible and practical.
abstractGer	The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by 20–30% compared to that of conventional carbonation methods. The optimum conditions for CO2 carbonation are determined as follows: reaction temperature of 25 °C, pulp density of 60 g L−1, CO2 flow rate of 1.0 L min−1, CO2 partial pressure of 0.4 MPa, reaction time of 120 min, and stirring speed of 400 rpm. The carbonation kinetics of the material is shown to be controlled by surface chemical reactions, with an activation energy of −8.705 kJ mol−1 obtained at 25–55 °C. The mechanism of the surface chemical reactions is further corroborated by XRD patterns and SEM images of the material and the generated residues. Reprecipitation of 83.14% Li in the LiHCO3 solution with 99.99% pure Li2CO3 is achieved via purification and decomposition. This proves the process is possible and practical.
abstract_unstemmed	The direct carbonation of industrial grade Li2CO3 using pure CO2 induces the formation of impurity-free water-soluble LiHCO3. In this study, microbubble-assisted pressure carbonation using CO2 is performed on industrial grade Li2CO3 to facilitate LiHCO3 formation. The conversion rate is increased by 20–30% compared to that of conventional carbonation methods. The optimum conditions for CO2 carbonation are determined as follows: reaction temperature of 25 °C, pulp density of 60 g L−1, CO2 flow rate of 1.0 L min−1, CO2 partial pressure of 0.4 MPa, reaction time of 120 min, and stirring speed of 400 rpm. The carbonation kinetics of the material is shown to be controlled by surface chemical reactions, with an activation energy of −8.705 kJ mol−1 obtained at 25–55 °C. The mechanism of the surface chemical reactions is further corroborated by XRD patterns and SEM images of the material and the generated residues. Reprecipitation of 83.14% Li in the LiHCO3 solution with 99.99% pure Li2CO3 is achieved via purification and decomposition. This proves the process is possible and practical.
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title_short	Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate
url	https://doi.org/10.1016/j.jmrt.2020.06.089 https://doaj.org/article/03099f563a4f41b28be7e0870bc65c4d http://www.sciencedirect.com/science/article/pii/S2238785420314903 https://doaj.org/toc/2238-7854
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up_date	2024-07-03T20:23:17.090Z
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Microbubble-assisted pressure carbonation for preparation of high purity lithium carbonate

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