One-Step Synthesis of High Pure Tris(8-hydroxyquinoline)aluminum for Optics and Photonics
A simple method of synthesis of high pure tris(8-hydroxyquinoline)aluminum (Alq<sub<3</sub<) from commercial available 5N Al<sub<2</sub<O<sub<3</sub< and 8-hydroxyquinolinol has been developed. One-step exchange chemical reaction has been conducted under controlle...
Ausführliche Beschreibung
Autor*in: |
Roman Avetisov [verfasserIn] Ksenya Kazmina [verfasserIn] Artem Barkanov [verfasserIn] Marina Zykova [verfasserIn] Andrew Khomyakov [verfasserIn] Alexander Pytchenko [verfasserIn] Igor Avetissov [verfasserIn] |
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E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2022 |
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Schlagwörter: |
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Übergeordnetes Werk: |
In: Materials - MDPI AG, 2009, 15(2022), 3, p 734 |
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Übergeordnetes Werk: |
volume:15 ; year:2022 ; number:3, p 734 |
Links: |
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DOI / URN: |
10.3390/ma15030734 |
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Katalog-ID: |
DOAJ016427173 |
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10.3390/ma15030734 doi (DE-627)DOAJ016427173 (DE-599)DOAJ2a692c2700a547c38247ec9cdd2ccb0d DE-627 ger DE-627 rakwb eng TK1-9971 TA1-2040 QH201-278.5 QC120-168.85 Roman Avetisov verfasserin aut One-Step Synthesis of High Pure Tris(8-hydroxyquinoline)aluminum for Optics and Photonics 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A simple method of synthesis of high pure tris(8-hydroxyquinoline)aluminum (Alq<sub<3</sub<) from commercial available 5N Al<sub<2</sub<O<sub<3</sub< and 8-hydroxyquinolinol has been developed. One-step exchange chemical reaction has been conducted under controlled 8-hydrixyquinoline vapor at a temperature of 190–240 °C with water removal by phosphorus anhydride. According to analysis of inductively coupled plasma mass-spectrometry, the chemical purity of synthesized Alq<sub<3</sub< was 99.998 wt%. Photoluminescence of the synthesized Alq<sub<3</sub< has been measured and slightly differed from those of Alq<sub<3</sub< obtained by traditional organic synthesis. tris(8-hydroxyquinoline)aluminum pure substance inductively coupled plasma mass spectrometry Technology T Electrical engineering. Electronics. Nuclear engineering Engineering (General). Civil engineering (General) Microscopy Descriptive and experimental mechanics Ksenya Kazmina verfasserin aut Artem Barkanov verfasserin aut Marina Zykova verfasserin aut Andrew Khomyakov verfasserin aut Alexander Pytchenko verfasserin aut Igor Avetissov verfasserin aut In Materials MDPI AG, 2009 15(2022), 3, p 734 (DE-627)595712649 (DE-600)2487261-1 19961944 nnns volume:15 year:2022 number:3, p 734 https://doi.org/10.3390/ma15030734 kostenfrei https://doaj.org/article/2a692c2700a547c38247ec9cdd2ccb0d kostenfrei https://www.mdpi.com/1996-1944/15/3/734 kostenfrei https://doaj.org/toc/1996-1944 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2022 3, p 734 |
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10.3390/ma15030734 doi (DE-627)DOAJ016427173 (DE-599)DOAJ2a692c2700a547c38247ec9cdd2ccb0d DE-627 ger DE-627 rakwb eng TK1-9971 TA1-2040 QH201-278.5 QC120-168.85 Roman Avetisov verfasserin aut One-Step Synthesis of High Pure Tris(8-hydroxyquinoline)aluminum for Optics and Photonics 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A simple method of synthesis of high pure tris(8-hydroxyquinoline)aluminum (Alq<sub<3</sub<) from commercial available 5N Al<sub<2</sub<O<sub<3</sub< and 8-hydroxyquinolinol has been developed. One-step exchange chemical reaction has been conducted under controlled 8-hydrixyquinoline vapor at a temperature of 190–240 °C with water removal by phosphorus anhydride. According to analysis of inductively coupled plasma mass-spectrometry, the chemical purity of synthesized Alq<sub<3</sub< was 99.998 wt%. Photoluminescence of the synthesized Alq<sub<3</sub< has been measured and slightly differed from those of Alq<sub<3</sub< obtained by traditional organic synthesis. tris(8-hydroxyquinoline)aluminum pure substance inductively coupled plasma mass spectrometry Technology T Electrical engineering. Electronics. Nuclear engineering Engineering (General). Civil engineering (General) Microscopy Descriptive and experimental mechanics Ksenya Kazmina verfasserin aut Artem Barkanov verfasserin aut Marina Zykova verfasserin aut Andrew Khomyakov verfasserin aut Alexander Pytchenko verfasserin aut Igor Avetissov verfasserin aut In Materials MDPI AG, 2009 15(2022), 3, p 734 (DE-627)595712649 (DE-600)2487261-1 19961944 nnns volume:15 year:2022 number:3, p 734 https://doi.org/10.3390/ma15030734 kostenfrei https://doaj.org/article/2a692c2700a547c38247ec9cdd2ccb0d kostenfrei https://www.mdpi.com/1996-1944/15/3/734 kostenfrei https://doaj.org/toc/1996-1944 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2022 3, p 734 |
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10.3390/ma15030734 doi (DE-627)DOAJ016427173 (DE-599)DOAJ2a692c2700a547c38247ec9cdd2ccb0d DE-627 ger DE-627 rakwb eng TK1-9971 TA1-2040 QH201-278.5 QC120-168.85 Roman Avetisov verfasserin aut One-Step Synthesis of High Pure Tris(8-hydroxyquinoline)aluminum for Optics and Photonics 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A simple method of synthesis of high pure tris(8-hydroxyquinoline)aluminum (Alq<sub<3</sub<) from commercial available 5N Al<sub<2</sub<O<sub<3</sub< and 8-hydroxyquinolinol has been developed. One-step exchange chemical reaction has been conducted under controlled 8-hydrixyquinoline vapor at a temperature of 190–240 °C with water removal by phosphorus anhydride. According to analysis of inductively coupled plasma mass-spectrometry, the chemical purity of synthesized Alq<sub<3</sub< was 99.998 wt%. Photoluminescence of the synthesized Alq<sub<3</sub< has been measured and slightly differed from those of Alq<sub<3</sub< obtained by traditional organic synthesis. tris(8-hydroxyquinoline)aluminum pure substance inductively coupled plasma mass spectrometry Technology T Electrical engineering. Electronics. Nuclear engineering Engineering (General). Civil engineering (General) Microscopy Descriptive and experimental mechanics Ksenya Kazmina verfasserin aut Artem Barkanov verfasserin aut Marina Zykova verfasserin aut Andrew Khomyakov verfasserin aut Alexander Pytchenko verfasserin aut Igor Avetissov verfasserin aut In Materials MDPI AG, 2009 15(2022), 3, p 734 (DE-627)595712649 (DE-600)2487261-1 19961944 nnns volume:15 year:2022 number:3, p 734 https://doi.org/10.3390/ma15030734 kostenfrei https://doaj.org/article/2a692c2700a547c38247ec9cdd2ccb0d kostenfrei https://www.mdpi.com/1996-1944/15/3/734 kostenfrei https://doaj.org/toc/1996-1944 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2022 3, p 734 |
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Roman Avetisov misc TK1-9971 misc TA1-2040 misc QH201-278.5 misc QC120-168.85 misc tris(8-hydroxyquinoline)aluminum misc pure substance misc inductively coupled plasma mass spectrometry misc Technology misc T misc Electrical engineering. Electronics. Nuclear engineering misc Engineering (General). Civil engineering (General) misc Microscopy misc Descriptive and experimental mechanics One-Step Synthesis of High Pure Tris(8-hydroxyquinoline)aluminum for Optics and Photonics |
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TK1-9971 TA1-2040 QH201-278.5 QC120-168.85 One-Step Synthesis of High Pure Tris(8-hydroxyquinoline)aluminum for Optics and Photonics tris(8-hydroxyquinoline)aluminum pure substance inductively coupled plasma mass spectrometry |
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One-Step Synthesis of High Pure Tris(8-hydroxyquinoline)aluminum for Optics and Photonics |
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A simple method of synthesis of high pure tris(8-hydroxyquinoline)aluminum (Alq<sub<3</sub<) from commercial available 5N Al<sub<2</sub<O<sub<3</sub< and 8-hydroxyquinolinol has been developed. One-step exchange chemical reaction has been conducted under controlled 8-hydrixyquinoline vapor at a temperature of 190–240 °C with water removal by phosphorus anhydride. According to analysis of inductively coupled plasma mass-spectrometry, the chemical purity of synthesized Alq<sub<3</sub< was 99.998 wt%. Photoluminescence of the synthesized Alq<sub<3</sub< has been measured and slightly differed from those of Alq<sub<3</sub< obtained by traditional organic synthesis. |
abstractGer |
A simple method of synthesis of high pure tris(8-hydroxyquinoline)aluminum (Alq<sub<3</sub<) from commercial available 5N Al<sub<2</sub<O<sub<3</sub< and 8-hydroxyquinolinol has been developed. One-step exchange chemical reaction has been conducted under controlled 8-hydrixyquinoline vapor at a temperature of 190–240 °C with water removal by phosphorus anhydride. According to analysis of inductively coupled plasma mass-spectrometry, the chemical purity of synthesized Alq<sub<3</sub< was 99.998 wt%. Photoluminescence of the synthesized Alq<sub<3</sub< has been measured and slightly differed from those of Alq<sub<3</sub< obtained by traditional organic synthesis. |
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A simple method of synthesis of high pure tris(8-hydroxyquinoline)aluminum (Alq<sub<3</sub<) from commercial available 5N Al<sub<2</sub<O<sub<3</sub< and 8-hydroxyquinolinol has been developed. One-step exchange chemical reaction has been conducted under controlled 8-hydrixyquinoline vapor at a temperature of 190–240 °C with water removal by phosphorus anhydride. According to analysis of inductively coupled plasma mass-spectrometry, the chemical purity of synthesized Alq<sub<3</sub< was 99.998 wt%. Photoluminescence of the synthesized Alq<sub<3</sub< has been measured and slightly differed from those of Alq<sub<3</sub< obtained by traditional organic synthesis. |
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