New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation

The novel binuclear titanium(IV) complex [{TiCl(OPr i)2(HOPr i )}2(mu-OPr i)2], 1, and the first mononuclear vanadyl(IV) chloroalcoholate [VCl(O)(HOPr i)4]Cl, 2, have been prepared from 2:1:1 mixtures of [Ti(OPr i)4], KOPr i and VCl3. Products were characterised by elemental analysis, FTIR, EPR, NMR...
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Autor*in:	Nunes Giovana G. [verfasserIn] Reis Dayane M. [verfasserIn] Camargo Pedro H. C. [verfasserIn] Hitchcock Peter B. [verfasserIn] Hörner Manfredo [verfasserIn] Matos Robson M. [verfasserIn] Mangrich Antonio S. [verfasserIn] Sá Eduardo L. de [verfasserIn] Leigh G. Jeffery [verfasserIn] Soares Jaísa F. [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2003

Schlagwörter:	titanium(IV) vanadium(IV) alkoxides binuclear

Übergeordnetes Werk:	In: Journal of the Brazilian Chemical Society - Sociedade Brasileira de Química, 2017, 14(2003), 6, Seite 922-929
Übergeordnetes Werk:	volume:14 ; year:2003 ; number:6 ; pages:922-929

Links:	Link aufrufen Link aufrufen Journal toc

Katalog-ID:	DOAJ016900669

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allfields	(DE-627)DOAJ016900669 (DE-599)DOAJ8e46fa13ba8946b99427364475405e4e DE-627 ger DE-627 rakwb eng QD1-999 Nunes Giovana G. verfasserin aut New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation 2003 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The novel binuclear titanium(IV) complex [{TiCl(OPr i)2(HOPr i )}2(mu-OPr i)2], 1, and the first mononuclear vanadyl(IV) chloroalcoholate [VCl(O)(HOPr i)4]Cl, 2, have been prepared from 2:1:1 mixtures of [Ti(OPr i)4], KOPr i and VCl3. Products were characterised by elemental analysis, FTIR, EPR, NMR and electronic spectroscopies, magnetic susceptibility measurements and single crystal X-ray diffractometry. A third product was found to be polynuclear and to contain both titanium and vanadium. Semi-empirical quantum-mechanical calculations were carried out for the evaluation of the electronic structure of 1. titanium(IV) vanadium(IV) alkoxides binuclear Chemistry Reis Dayane M. verfasserin aut Camargo Pedro H. C. verfasserin aut Hitchcock Peter B. verfasserin aut Hörner Manfredo verfasserin aut Matos Robson M. verfasserin aut Mangrich Antonio S. verfasserin aut Sá Eduardo L. de verfasserin aut Leigh G. Jeffery verfasserin aut Soares Jaísa F. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 14(2003), 6, Seite 922-929 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:14 year:2003 number:6 pages:922-929 https://doaj.org/article/8e46fa13ba8946b99427364475405e4e kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000600009 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 14 2003 6 922-929
spelling	(DE-627)DOAJ016900669 (DE-599)DOAJ8e46fa13ba8946b99427364475405e4e DE-627 ger DE-627 rakwb eng QD1-999 Nunes Giovana G. verfasserin aut New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation 2003 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The novel binuclear titanium(IV) complex [{TiCl(OPr i)2(HOPr i )}2(mu-OPr i)2], 1, and the first mononuclear vanadyl(IV) chloroalcoholate [VCl(O)(HOPr i)4]Cl, 2, have been prepared from 2:1:1 mixtures of [Ti(OPr i)4], KOPr i and VCl3. Products were characterised by elemental analysis, FTIR, EPR, NMR and electronic spectroscopies, magnetic susceptibility measurements and single crystal X-ray diffractometry. A third product was found to be polynuclear and to contain both titanium and vanadium. Semi-empirical quantum-mechanical calculations were carried out for the evaluation of the electronic structure of 1. titanium(IV) vanadium(IV) alkoxides binuclear Chemistry Reis Dayane M. verfasserin aut Camargo Pedro H. C. verfasserin aut Hitchcock Peter B. verfasserin aut Hörner Manfredo verfasserin aut Matos Robson M. verfasserin aut Mangrich Antonio S. verfasserin aut Sá Eduardo L. de verfasserin aut Leigh G. Jeffery verfasserin aut Soares Jaísa F. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 14(2003), 6, Seite 922-929 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:14 year:2003 number:6 pages:922-929 https://doaj.org/article/8e46fa13ba8946b99427364475405e4e kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000600009 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 14 2003 6 922-929
allfields_unstemmed	(DE-627)DOAJ016900669 (DE-599)DOAJ8e46fa13ba8946b99427364475405e4e DE-627 ger DE-627 rakwb eng QD1-999 Nunes Giovana G. verfasserin aut New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation 2003 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The novel binuclear titanium(IV) complex [{TiCl(OPr i)2(HOPr i )}2(mu-OPr i)2], 1, and the first mononuclear vanadyl(IV) chloroalcoholate [VCl(O)(HOPr i)4]Cl, 2, have been prepared from 2:1:1 mixtures of [Ti(OPr i)4], KOPr i and VCl3. Products were characterised by elemental analysis, FTIR, EPR, NMR and electronic spectroscopies, magnetic susceptibility measurements and single crystal X-ray diffractometry. A third product was found to be polynuclear and to contain both titanium and vanadium. Semi-empirical quantum-mechanical calculations were carried out for the evaluation of the electronic structure of 1. titanium(IV) vanadium(IV) alkoxides binuclear Chemistry Reis Dayane M. verfasserin aut Camargo Pedro H. C. verfasserin aut Hitchcock Peter B. verfasserin aut Hörner Manfredo verfasserin aut Matos Robson M. verfasserin aut Mangrich Antonio S. verfasserin aut Sá Eduardo L. de verfasserin aut Leigh G. Jeffery verfasserin aut Soares Jaísa F. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 14(2003), 6, Seite 922-929 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:14 year:2003 number:6 pages:922-929 https://doaj.org/article/8e46fa13ba8946b99427364475405e4e kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000600009 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 14 2003 6 922-929
allfieldsGer	(DE-627)DOAJ016900669 (DE-599)DOAJ8e46fa13ba8946b99427364475405e4e DE-627 ger DE-627 rakwb eng QD1-999 Nunes Giovana G. verfasserin aut New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation 2003 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The novel binuclear titanium(IV) complex [{TiCl(OPr i)2(HOPr i )}2(mu-OPr i)2], 1, and the first mononuclear vanadyl(IV) chloroalcoholate [VCl(O)(HOPr i)4]Cl, 2, have been prepared from 2:1:1 mixtures of [Ti(OPr i)4], KOPr i and VCl3. Products were characterised by elemental analysis, FTIR, EPR, NMR and electronic spectroscopies, magnetic susceptibility measurements and single crystal X-ray diffractometry. A third product was found to be polynuclear and to contain both titanium and vanadium. Semi-empirical quantum-mechanical calculations were carried out for the evaluation of the electronic structure of 1. titanium(IV) vanadium(IV) alkoxides binuclear Chemistry Reis Dayane M. verfasserin aut Camargo Pedro H. C. verfasserin aut Hitchcock Peter B. verfasserin aut Hörner Manfredo verfasserin aut Matos Robson M. verfasserin aut Mangrich Antonio S. verfasserin aut Sá Eduardo L. de verfasserin aut Leigh G. Jeffery verfasserin aut Soares Jaísa F. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 14(2003), 6, Seite 922-929 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:14 year:2003 number:6 pages:922-929 https://doaj.org/article/8e46fa13ba8946b99427364475405e4e kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000600009 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 14 2003 6 922-929
allfieldsSound	(DE-627)DOAJ016900669 (DE-599)DOAJ8e46fa13ba8946b99427364475405e4e DE-627 ger DE-627 rakwb eng QD1-999 Nunes Giovana G. verfasserin aut New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation 2003 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The novel binuclear titanium(IV) complex [{TiCl(OPr i)2(HOPr i )}2(mu-OPr i)2], 1, and the first mononuclear vanadyl(IV) chloroalcoholate [VCl(O)(HOPr i)4]Cl, 2, have been prepared from 2:1:1 mixtures of [Ti(OPr i)4], KOPr i and VCl3. Products were characterised by elemental analysis, FTIR, EPR, NMR and electronic spectroscopies, magnetic susceptibility measurements and single crystal X-ray diffractometry. A third product was found to be polynuclear and to contain both titanium and vanadium. Semi-empirical quantum-mechanical calculations were carried out for the evaluation of the electronic structure of 1. titanium(IV) vanadium(IV) alkoxides binuclear Chemistry Reis Dayane M. verfasserin aut Camargo Pedro H. C. verfasserin aut Hitchcock Peter B. verfasserin aut Hörner Manfredo verfasserin aut Matos Robson M. verfasserin aut Mangrich Antonio S. verfasserin aut Sá Eduardo L. de verfasserin aut Leigh G. Jeffery verfasserin aut Soares Jaísa F. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 14(2003), 6, Seite 922-929 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:14 year:2003 number:6 pages:922-929 https://doaj.org/article/8e46fa13ba8946b99427364475405e4e kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000600009 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 14 2003 6 922-929
language	English
source	In Journal of the Brazilian Chemical Society 14(2003), 6, Seite 922-929 volume:14 year:2003 number:6 pages:922-929
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topic_facet	titanium(IV) vanadium(IV) alkoxides binuclear Chemistry
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authorswithroles_txt_mv	Nunes Giovana G. @@aut@@ Reis Dayane M. @@aut@@ Camargo Pedro H. C. @@aut@@ Hitchcock Peter B. @@aut@@ Hörner Manfredo @@aut@@ Matos Robson M. @@aut@@ Mangrich Antonio S. @@aut@@ Sá Eduardo L. de @@aut@@ Leigh G. Jeffery @@aut@@ Soares Jaísa F. @@aut@@
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callnumber-first	Q - Science
author	Nunes Giovana G.
spellingShingle	Nunes Giovana G. misc QD1-999 misc titanium(IV) misc vanadium(IV) misc alkoxides misc binuclear misc Chemistry New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation
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topic_title	QD1-999 New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation titanium(IV) vanadium(IV) alkoxides binuclear
topic	misc QD1-999 misc titanium(IV) misc vanadium(IV) misc alkoxides misc binuclear misc Chemistry
topic_unstemmed	misc QD1-999 misc titanium(IV) misc vanadium(IV) misc alkoxides misc binuclear misc Chemistry
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title	New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation
ctrlnum	(DE-627)DOAJ016900669 (DE-599)DOAJ8e46fa13ba8946b99427364475405e4e
title_full	New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation
author_sort	Nunes Giovana G.
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author_browse	Nunes Giovana G. Reis Dayane M. Camargo Pedro H. C. Hitchcock Peter B. Hörner Manfredo Matos Robson M. Mangrich Antonio S. Sá Eduardo L. de Leigh G. Jeffery Soares Jaísa F.
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author-letter	Nunes Giovana G.
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title_sort	new titanium(iv) and vanadium(iv) haloalkoxides: synthetic route and structural characterisation
callnumber	QD1-999
title_auth	New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation
abstract	The novel binuclear titanium(IV) complex [{TiCl(OPr i)2(HOPr i )}2(mu-OPr i)2], 1, and the first mononuclear vanadyl(IV) chloroalcoholate [VCl(O)(HOPr i)4]Cl, 2, have been prepared from 2:1:1 mixtures of [Ti(OPr i)4], KOPr i and VCl3. Products were characterised by elemental analysis, FTIR, EPR, NMR and electronic spectroscopies, magnetic susceptibility measurements and single crystal X-ray diffractometry. A third product was found to be polynuclear and to contain both titanium and vanadium. Semi-empirical quantum-mechanical calculations were carried out for the evaluation of the electronic structure of 1.
abstractGer	The novel binuclear titanium(IV) complex [{TiCl(OPr i)2(HOPr i )}2(mu-OPr i)2], 1, and the first mononuclear vanadyl(IV) chloroalcoholate [VCl(O)(HOPr i)4]Cl, 2, have been prepared from 2:1:1 mixtures of [Ti(OPr i)4], KOPr i and VCl3. Products were characterised by elemental analysis, FTIR, EPR, NMR and electronic spectroscopies, magnetic susceptibility measurements and single crystal X-ray diffractometry. A third product was found to be polynuclear and to contain both titanium and vanadium. Semi-empirical quantum-mechanical calculations were carried out for the evaluation of the electronic structure of 1.
abstract_unstemmed	The novel binuclear titanium(IV) complex [{TiCl(OPr i)2(HOPr i )}2(mu-OPr i)2], 1, and the first mononuclear vanadyl(IV) chloroalcoholate [VCl(O)(HOPr i)4]Cl, 2, have been prepared from 2:1:1 mixtures of [Ti(OPr i)4], KOPr i and VCl3. Products were characterised by elemental analysis, FTIR, EPR, NMR and electronic spectroscopies, magnetic susceptibility measurements and single crystal X-ray diffractometry. A third product was found to be polynuclear and to contain both titanium and vanadium. Semi-empirical quantum-mechanical calculations were carried out for the evaluation of the electronic structure of 1.
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title_short	New titanium(IV) and vanadium(IV) haloalkoxides: synthetic route and structural characterisation
url	https://doaj.org/article/8e46fa13ba8946b99427364475405e4e http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000600009 https://doaj.org/toc/0103-5053
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up_date	2024-07-03T23:29:39.136Z
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