Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium]

In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding ab...
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Autor*in:	Graham Smith [verfasserIn] Urs D. Wermuth [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2011

Übergeordnetes Werk:	In: Acta Crystallographica Section E - International Union of Crystallography, 2005, 67(2011), 11, Seite m1594-m1595
Übergeordnetes Werk:	volume:67 ; year:2011 ; number:11 ; pages:m1594-m1595

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1107/S1600536811043406

Katalog-ID:	DOAJ018526195

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520			\|a In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding about both the seven-coordinate cations is similar, comprising one monodentate water molecule together with three bridging water molecules and three carboxylate O-atom donors, two of which are bridging. The environments around the six-coordinate cations are also similar, comprising a monodentate nitro O-atom donor, a bridging water molecule and four bridging carboxylate O-atom donors [overall Rb—O range = 2.849 (2)–3.190 (2) Å]. The coordination leads to a two-dimensional polymeric structure extending parallel to (001), which is stabilized by interlayer water O—H...O hydrogen-bonding associations to water, carboxyl and nitro O-atom acceptors, together with weak inter-ring π–π interactions [minimum ring centroid–centroid separation = 3.5319 (19) Å].
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allfields	10.1107/S1600536811043406 doi (DE-627)DOAJ018526195 (DE-599)DOAJ1f753d3a6a6746d6a672d9ed873a6994 DE-627 ger DE-627 rakwb eng QD901-999 Graham Smith verfasserin aut Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium] 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding about both the seven-coordinate cations is similar, comprising one monodentate water molecule together with three bridging water molecules and three carboxylate O-atom donors, two of which are bridging. The environments around the six-coordinate cations are also similar, comprising a monodentate nitro O-atom donor, a bridging water molecule and four bridging carboxylate O-atom donors [overall Rb—O range = 2.849 (2)–3.190 (2) Å]. The coordination leads to a two-dimensional polymeric structure extending parallel to (001), which is stabilized by interlayer water O—H...O hydrogen-bonding associations to water, carboxyl and nitro O-atom acceptors, together with weak inter-ring π–π interactions [minimum ring centroid–centroid separation = 3.5319 (19) Å]. Crystallography Urs D. Wermuth verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite m1594-m1595 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:m1594-m1595 https://doi.org/10.1107/S1600536811043406 kostenfrei https://doaj.org/article/1f753d3a6a6746d6a672d9ed873a6994 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811043406 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 m1594-m1595
spelling	10.1107/S1600536811043406 doi (DE-627)DOAJ018526195 (DE-599)DOAJ1f753d3a6a6746d6a672d9ed873a6994 DE-627 ger DE-627 rakwb eng QD901-999 Graham Smith verfasserin aut Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium] 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding about both the seven-coordinate cations is similar, comprising one monodentate water molecule together with three bridging water molecules and three carboxylate O-atom donors, two of which are bridging. The environments around the six-coordinate cations are also similar, comprising a monodentate nitro O-atom donor, a bridging water molecule and four bridging carboxylate O-atom donors [overall Rb—O range = 2.849 (2)–3.190 (2) Å]. The coordination leads to a two-dimensional polymeric structure extending parallel to (001), which is stabilized by interlayer water O—H...O hydrogen-bonding associations to water, carboxyl and nitro O-atom acceptors, together with weak inter-ring π–π interactions [minimum ring centroid–centroid separation = 3.5319 (19) Å]. Crystallography Urs D. Wermuth verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite m1594-m1595 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:m1594-m1595 https://doi.org/10.1107/S1600536811043406 kostenfrei https://doaj.org/article/1f753d3a6a6746d6a672d9ed873a6994 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811043406 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 m1594-m1595
allfields_unstemmed	10.1107/S1600536811043406 doi (DE-627)DOAJ018526195 (DE-599)DOAJ1f753d3a6a6746d6a672d9ed873a6994 DE-627 ger DE-627 rakwb eng QD901-999 Graham Smith verfasserin aut Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium] 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding about both the seven-coordinate cations is similar, comprising one monodentate water molecule together with three bridging water molecules and three carboxylate O-atom donors, two of which are bridging. The environments around the six-coordinate cations are also similar, comprising a monodentate nitro O-atom donor, a bridging water molecule and four bridging carboxylate O-atom donors [overall Rb—O range = 2.849 (2)–3.190 (2) Å]. The coordination leads to a two-dimensional polymeric structure extending parallel to (001), which is stabilized by interlayer water O—H...O hydrogen-bonding associations to water, carboxyl and nitro O-atom acceptors, together with weak inter-ring π–π interactions [minimum ring centroid–centroid separation = 3.5319 (19) Å]. Crystallography Urs D. Wermuth verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite m1594-m1595 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:m1594-m1595 https://doi.org/10.1107/S1600536811043406 kostenfrei https://doaj.org/article/1f753d3a6a6746d6a672d9ed873a6994 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811043406 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 m1594-m1595
allfieldsGer	10.1107/S1600536811043406 doi (DE-627)DOAJ018526195 (DE-599)DOAJ1f753d3a6a6746d6a672d9ed873a6994 DE-627 ger DE-627 rakwb eng QD901-999 Graham Smith verfasserin aut Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium] 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding about both the seven-coordinate cations is similar, comprising one monodentate water molecule together with three bridging water molecules and three carboxylate O-atom donors, two of which are bridging. The environments around the six-coordinate cations are also similar, comprising a monodentate nitro O-atom donor, a bridging water molecule and four bridging carboxylate O-atom donors [overall Rb—O range = 2.849 (2)–3.190 (2) Å]. The coordination leads to a two-dimensional polymeric structure extending parallel to (001), which is stabilized by interlayer water O—H...O hydrogen-bonding associations to water, carboxyl and nitro O-atom acceptors, together with weak inter-ring π–π interactions [minimum ring centroid–centroid separation = 3.5319 (19) Å]. Crystallography Urs D. Wermuth verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite m1594-m1595 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:m1594-m1595 https://doi.org/10.1107/S1600536811043406 kostenfrei https://doaj.org/article/1f753d3a6a6746d6a672d9ed873a6994 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811043406 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 m1594-m1595
allfieldsSound	10.1107/S1600536811043406 doi (DE-627)DOAJ018526195 (DE-599)DOAJ1f753d3a6a6746d6a672d9ed873a6994 DE-627 ger DE-627 rakwb eng QD901-999 Graham Smith verfasserin aut Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium] 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding about both the seven-coordinate cations is similar, comprising one monodentate water molecule together with three bridging water molecules and three carboxylate O-atom donors, two of which are bridging. The environments around the six-coordinate cations are also similar, comprising a monodentate nitro O-atom donor, a bridging water molecule and four bridging carboxylate O-atom donors [overall Rb—O range = 2.849 (2)–3.190 (2) Å]. The coordination leads to a two-dimensional polymeric structure extending parallel to (001), which is stabilized by interlayer water O—H...O hydrogen-bonding associations to water, carboxyl and nitro O-atom acceptors, together with weak inter-ring π–π interactions [minimum ring centroid–centroid separation = 3.5319 (19) Å]. Crystallography Urs D. Wermuth verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite m1594-m1595 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:m1594-m1595 https://doi.org/10.1107/S1600536811043406 kostenfrei https://doaj.org/article/1f753d3a6a6746d6a672d9ed873a6994 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811043406 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 m1594-m1595
language	English
source	In Acta Crystallographica Section E 67(2011), 11, Seite m1594-m1595 volume:67 year:2011 number:11 pages:m1594-m1595
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authorswithroles_txt_mv	Graham Smith @@aut@@ Urs D. Wermuth @@aut@@
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callnumber-first	Q - Science
author	Graham Smith
spellingShingle	Graham Smith misc QD901-999 misc Crystallography Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium]
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topic_title	QD901-999 Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium]
topic	misc QD901-999 misc Crystallography
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title	Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium]
ctrlnum	(DE-627)DOAJ018526195 (DE-599)DOAJ1f753d3a6a6746d6a672d9ed873a6994
title_full	Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium]
author_sort	Graham Smith
journal	Acta Crystallographica Section E
journalStr	Acta Crystallographica Section E
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author_browse	Graham Smith Urs D. Wermuth
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doi_str_mv	10.1107/S1600536811043406
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title_sort	poly[tetra-μ-aqua-diaquatetrakis[μ-(e)-2-nitrocinnamato]tetrarubidium]
callnumber	QD901-999
title_auth	Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium]
abstract	In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding about both the seven-coordinate cations is similar, comprising one monodentate water molecule together with three bridging water molecules and three carboxylate O-atom donors, two of which are bridging. The environments around the six-coordinate cations are also similar, comprising a monodentate nitro O-atom donor, a bridging water molecule and four bridging carboxylate O-atom donors [overall Rb—O range = 2.849 (2)–3.190 (2) Å]. The coordination leads to a two-dimensional polymeric structure extending parallel to (001), which is stabilized by interlayer water O—H...O hydrogen-bonding associations to water, carboxyl and nitro O-atom acceptors, together with weak inter-ring π–π interactions [minimum ring centroid–centroid separation = 3.5319 (19) Å].
abstractGer	In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding about both the seven-coordinate cations is similar, comprising one monodentate water molecule together with three bridging water molecules and three carboxylate O-atom donors, two of which are bridging. The environments around the six-coordinate cations are also similar, comprising a monodentate nitro O-atom donor, a bridging water molecule and four bridging carboxylate O-atom donors [overall Rb—O range = 2.849 (2)–3.190 (2) Å]. The coordination leads to a two-dimensional polymeric structure extending parallel to (001), which is stabilized by interlayer water O—H...O hydrogen-bonding associations to water, carboxyl and nitro O-atom acceptors, together with weak inter-ring π–π interactions [minimum ring centroid–centroid separation = 3.5319 (19) Å].
abstract_unstemmed	In the structure of the title compound, [Rb4(C9H6NO4)4(H2O)6]n, the asymmetric unit comprises four rubidium cations, two of which have an RbO7 coordination polyhedron with a monocapped distorted octahedral stereochemistry and two of which have a distorted RbO6 octahedral coordination. The bonding about both the seven-coordinate cations is similar, comprising one monodentate water molecule together with three bridging water molecules and three carboxylate O-atom donors, two of which are bridging. The environments around the six-coordinate cations are also similar, comprising a monodentate nitro O-atom donor, a bridging water molecule and four bridging carboxylate O-atom donors [overall Rb—O range = 2.849 (2)–3.190 (2) Å]. The coordination leads to a two-dimensional polymeric structure extending parallel to (001), which is stabilized by interlayer water O—H...O hydrogen-bonding associations to water, carboxyl and nitro O-atom acceptors, together with weak inter-ring π–π interactions [minimum ring centroid–centroid separation = 3.5319 (19) Å].
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container_issue	11
title_short	Poly[tetra-μ-aqua-diaquatetrakis[μ-(E)-2-nitrocinnamato]tetrarubidium]
url	https://doi.org/10.1107/S1600536811043406 https://doaj.org/article/1f753d3a6a6746d6a672d9ed873a6994 http://scripts.iucr.org/cgi-bin/paper?S1600536811043406 https://doaj.org/toc/1600-5368
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doi_str	10.1107/S1600536811043406
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up_date	2024-07-03T18:24:21.017Z
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