Correlation between the surface characteristics of carbon supports and their electrochemical stability and performance in fuel cell cathodes
Abstract In this paper, an extensive characterisation of a range of carbon blacks (CB) with similar surface area but different surface chemistry is carried out by flow calorimetry, Raman spectroscopy, dynamic water vapour sorption, instrumental gas analysis, nitrogen adsorption/desorption and high p...
Ausführliche Beschreibung
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| Autor*in: |
Ignacio Jiménez‐Morales [verfasserIn] Alvaro Reyes‐Carmona [verfasserIn] Marc Dupont [verfasserIn] Sara Cavaliere [verfasserIn] Marlene Rodlert [verfasserIn] Flavio Mornaghini [verfasserIn] Mikkel J. Larsen [verfasserIn] Madeleine Odgaard [verfasserIn] Jerzy Zajac [verfasserIn] Deborah J. Jones [verfasserIn] Jacques Rozière [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
In: Carbon Energy - Wiley, 2020, 3(2021), 4, Seite 654-665 |
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| Übergeordnetes Werk: |
volume:3 ; year:2021 ; number:4 ; pages:654-665 |
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| DOI / URN: |
10.1002/cey2.109 |
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| Katalog-ID: |
DOAJ019065647 |
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| 650 | 4 | |a carbon black | |
| 650 | 4 | |a electrocatalyst support | |
| 650 | 4 | |a fuel cell cathodes | |
| 650 | 4 | |a surface properties | |
| 653 | 0 | |a Production of electric energy or power. Powerplants. Central stations | |
| 700 | 0 | |a Alvaro Reyes‐Carmona |e verfasserin |4 aut | |
| 700 | 0 | |a Marc Dupont |e verfasserin |4 aut | |
| 700 | 0 | |a Sara Cavaliere |e verfasserin |4 aut | |
| 700 | 0 | |a Marlene Rodlert |e verfasserin |4 aut | |
| 700 | 0 | |a Flavio Mornaghini |e verfasserin |4 aut | |
| 700 | 0 | |a Mikkel J. Larsen |e verfasserin |4 aut | |
| 700 | 0 | |a Madeleine Odgaard |e verfasserin |4 aut | |
| 700 | 0 | |a Jerzy Zajac |e verfasserin |4 aut | |
| 700 | 0 | |a Deborah J. Jones |e verfasserin |4 aut | |
| 700 | 0 | |a Jacques Rozière |e verfasserin |4 aut | |
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10.1002/cey2.109 doi (DE-627)DOAJ019065647 (DE-599)DOAJ144a63186a1a4950b28d35b010164398 DE-627 ger DE-627 rakwb eng TK1001-1841 Ignacio Jiménez‐Morales verfasserin aut Correlation between the surface characteristics of carbon supports and their electrochemical stability and performance in fuel cell cathodes 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this paper, an extensive characterisation of a range of carbon blacks (CB) with similar surface area but different surface chemistry is carried out by flow calorimetry, Raman spectroscopy, dynamic water vapour sorption, instrumental gas analysis, nitrogen adsorption/desorption and high potential chronoamperometry. Using these carbon materials as supports, Pt/CB electrocatalysts are prepared by microwave‐assisted polyol‐mediated synthesis in gram scale. Structural, morphological and electrochemical properties of the prepared electrocatalysts are evaluated by X‐ray diffraction, transmission electron microscopy, rotating disc electrode and in situ fuel cell characterisation of the corresponding membrane–electrode assemblies. The obtained results allow to establish a relationship between surface chemistry and electrochemical properties useful for the design of Pt/C catalyst layers with high performance and stability. carbon black electrocatalyst support fuel cell cathodes surface properties Production of electric energy or power. Powerplants. Central stations Alvaro Reyes‐Carmona verfasserin aut Marc Dupont verfasserin aut Sara Cavaliere verfasserin aut Marlene Rodlert verfasserin aut Flavio Mornaghini verfasserin aut Mikkel J. Larsen verfasserin aut Madeleine Odgaard verfasserin aut Jerzy Zajac verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Carbon Energy Wiley, 2020 3(2021), 4, Seite 654-665 (DE-627)1691003859 (DE-600)3009616-9 26379368 nnns volume:3 year:2021 number:4 pages:654-665 https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/article/144a63186a1a4950b28d35b010164398 kostenfrei https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/toc/2637-9368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 3 2021 4 654-665 |
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10.1002/cey2.109 doi (DE-627)DOAJ019065647 (DE-599)DOAJ144a63186a1a4950b28d35b010164398 DE-627 ger DE-627 rakwb eng TK1001-1841 Ignacio Jiménez‐Morales verfasserin aut Correlation between the surface characteristics of carbon supports and their electrochemical stability and performance in fuel cell cathodes 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this paper, an extensive characterisation of a range of carbon blacks (CB) with similar surface area but different surface chemistry is carried out by flow calorimetry, Raman spectroscopy, dynamic water vapour sorption, instrumental gas analysis, nitrogen adsorption/desorption and high potential chronoamperometry. Using these carbon materials as supports, Pt/CB electrocatalysts are prepared by microwave‐assisted polyol‐mediated synthesis in gram scale. Structural, morphological and electrochemical properties of the prepared electrocatalysts are evaluated by X‐ray diffraction, transmission electron microscopy, rotating disc electrode and in situ fuel cell characterisation of the corresponding membrane–electrode assemblies. The obtained results allow to establish a relationship between surface chemistry and electrochemical properties useful for the design of Pt/C catalyst layers with high performance and stability. carbon black electrocatalyst support fuel cell cathodes surface properties Production of electric energy or power. Powerplants. Central stations Alvaro Reyes‐Carmona verfasserin aut Marc Dupont verfasserin aut Sara Cavaliere verfasserin aut Marlene Rodlert verfasserin aut Flavio Mornaghini verfasserin aut Mikkel J. Larsen verfasserin aut Madeleine Odgaard verfasserin aut Jerzy Zajac verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Carbon Energy Wiley, 2020 3(2021), 4, Seite 654-665 (DE-627)1691003859 (DE-600)3009616-9 26379368 nnns volume:3 year:2021 number:4 pages:654-665 https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/article/144a63186a1a4950b28d35b010164398 kostenfrei https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/toc/2637-9368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 3 2021 4 654-665 |
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10.1002/cey2.109 doi (DE-627)DOAJ019065647 (DE-599)DOAJ144a63186a1a4950b28d35b010164398 DE-627 ger DE-627 rakwb eng TK1001-1841 Ignacio Jiménez‐Morales verfasserin aut Correlation between the surface characteristics of carbon supports and their electrochemical stability and performance in fuel cell cathodes 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this paper, an extensive characterisation of a range of carbon blacks (CB) with similar surface area but different surface chemistry is carried out by flow calorimetry, Raman spectroscopy, dynamic water vapour sorption, instrumental gas analysis, nitrogen adsorption/desorption and high potential chronoamperometry. Using these carbon materials as supports, Pt/CB electrocatalysts are prepared by microwave‐assisted polyol‐mediated synthesis in gram scale. Structural, morphological and electrochemical properties of the prepared electrocatalysts are evaluated by X‐ray diffraction, transmission electron microscopy, rotating disc electrode and in situ fuel cell characterisation of the corresponding membrane–electrode assemblies. The obtained results allow to establish a relationship between surface chemistry and electrochemical properties useful for the design of Pt/C catalyst layers with high performance and stability. carbon black electrocatalyst support fuel cell cathodes surface properties Production of electric energy or power. Powerplants. Central stations Alvaro Reyes‐Carmona verfasserin aut Marc Dupont verfasserin aut Sara Cavaliere verfasserin aut Marlene Rodlert verfasserin aut Flavio Mornaghini verfasserin aut Mikkel J. Larsen verfasserin aut Madeleine Odgaard verfasserin aut Jerzy Zajac verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Carbon Energy Wiley, 2020 3(2021), 4, Seite 654-665 (DE-627)1691003859 (DE-600)3009616-9 26379368 nnns volume:3 year:2021 number:4 pages:654-665 https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/article/144a63186a1a4950b28d35b010164398 kostenfrei https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/toc/2637-9368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 3 2021 4 654-665 |
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10.1002/cey2.109 doi (DE-627)DOAJ019065647 (DE-599)DOAJ144a63186a1a4950b28d35b010164398 DE-627 ger DE-627 rakwb eng TK1001-1841 Ignacio Jiménez‐Morales verfasserin aut Correlation between the surface characteristics of carbon supports and their electrochemical stability and performance in fuel cell cathodes 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this paper, an extensive characterisation of a range of carbon blacks (CB) with similar surface area but different surface chemistry is carried out by flow calorimetry, Raman spectroscopy, dynamic water vapour sorption, instrumental gas analysis, nitrogen adsorption/desorption and high potential chronoamperometry. Using these carbon materials as supports, Pt/CB electrocatalysts are prepared by microwave‐assisted polyol‐mediated synthesis in gram scale. Structural, morphological and electrochemical properties of the prepared electrocatalysts are evaluated by X‐ray diffraction, transmission electron microscopy, rotating disc electrode and in situ fuel cell characterisation of the corresponding membrane–electrode assemblies. The obtained results allow to establish a relationship between surface chemistry and electrochemical properties useful for the design of Pt/C catalyst layers with high performance and stability. carbon black electrocatalyst support fuel cell cathodes surface properties Production of electric energy or power. Powerplants. Central stations Alvaro Reyes‐Carmona verfasserin aut Marc Dupont verfasserin aut Sara Cavaliere verfasserin aut Marlene Rodlert verfasserin aut Flavio Mornaghini verfasserin aut Mikkel J. Larsen verfasserin aut Madeleine Odgaard verfasserin aut Jerzy Zajac verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Carbon Energy Wiley, 2020 3(2021), 4, Seite 654-665 (DE-627)1691003859 (DE-600)3009616-9 26379368 nnns volume:3 year:2021 number:4 pages:654-665 https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/article/144a63186a1a4950b28d35b010164398 kostenfrei https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/toc/2637-9368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 3 2021 4 654-665 |
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10.1002/cey2.109 doi (DE-627)DOAJ019065647 (DE-599)DOAJ144a63186a1a4950b28d35b010164398 DE-627 ger DE-627 rakwb eng TK1001-1841 Ignacio Jiménez‐Morales verfasserin aut Correlation between the surface characteristics of carbon supports and their electrochemical stability and performance in fuel cell cathodes 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this paper, an extensive characterisation of a range of carbon blacks (CB) with similar surface area but different surface chemistry is carried out by flow calorimetry, Raman spectroscopy, dynamic water vapour sorption, instrumental gas analysis, nitrogen adsorption/desorption and high potential chronoamperometry. Using these carbon materials as supports, Pt/CB electrocatalysts are prepared by microwave‐assisted polyol‐mediated synthesis in gram scale. Structural, morphological and electrochemical properties of the prepared electrocatalysts are evaluated by X‐ray diffraction, transmission electron microscopy, rotating disc electrode and in situ fuel cell characterisation of the corresponding membrane–electrode assemblies. The obtained results allow to establish a relationship between surface chemistry and electrochemical properties useful for the design of Pt/C catalyst layers with high performance and stability. carbon black electrocatalyst support fuel cell cathodes surface properties Production of electric energy or power. Powerplants. Central stations Alvaro Reyes‐Carmona verfasserin aut Marc Dupont verfasserin aut Sara Cavaliere verfasserin aut Marlene Rodlert verfasserin aut Flavio Mornaghini verfasserin aut Mikkel J. Larsen verfasserin aut Madeleine Odgaard verfasserin aut Jerzy Zajac verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Carbon Energy Wiley, 2020 3(2021), 4, Seite 654-665 (DE-627)1691003859 (DE-600)3009616-9 26379368 nnns volume:3 year:2021 number:4 pages:654-665 https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/article/144a63186a1a4950b28d35b010164398 kostenfrei https://doi.org/10.1002/cey2.109 kostenfrei https://doaj.org/toc/2637-9368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 3 2021 4 654-665 |
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Ignacio Jiménez‐Morales @@aut@@ Alvaro Reyes‐Carmona @@aut@@ Marc Dupont @@aut@@ Sara Cavaliere @@aut@@ Marlene Rodlert @@aut@@ Flavio Mornaghini @@aut@@ Mikkel J. Larsen @@aut@@ Madeleine Odgaard @@aut@@ Jerzy Zajac @@aut@@ Deborah J. Jones @@aut@@ Jacques Rozière @@aut@@ |
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Ignacio Jiménez‐Morales |
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TK1001-1841 Correlation between the surface characteristics of carbon supports and their electrochemical stability and performance in fuel cell cathodes carbon black electrocatalyst support fuel cell cathodes surface properties |
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Ignacio Jiménez‐Morales Alvaro Reyes‐Carmona Marc Dupont Sara Cavaliere Marlene Rodlert Flavio Mornaghini Mikkel J. Larsen Madeleine Odgaard Jerzy Zajac Deborah J. Jones Jacques Rozière |
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correlation between the surface characteristics of carbon supports and their electrochemical stability and performance in fuel cell cathodes |
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Correlation between the surface characteristics of carbon supports and their electrochemical stability and performance in fuel cell cathodes |
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Abstract In this paper, an extensive characterisation of a range of carbon blacks (CB) with similar surface area but different surface chemistry is carried out by flow calorimetry, Raman spectroscopy, dynamic water vapour sorption, instrumental gas analysis, nitrogen adsorption/desorption and high potential chronoamperometry. Using these carbon materials as supports, Pt/CB electrocatalysts are prepared by microwave‐assisted polyol‐mediated synthesis in gram scale. Structural, morphological and electrochemical properties of the prepared electrocatalysts are evaluated by X‐ray diffraction, transmission electron microscopy, rotating disc electrode and in situ fuel cell characterisation of the corresponding membrane–electrode assemblies. The obtained results allow to establish a relationship between surface chemistry and electrochemical properties useful for the design of Pt/C catalyst layers with high performance and stability. |
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Abstract In this paper, an extensive characterisation of a range of carbon blacks (CB) with similar surface area but different surface chemistry is carried out by flow calorimetry, Raman spectroscopy, dynamic water vapour sorption, instrumental gas analysis, nitrogen adsorption/desorption and high potential chronoamperometry. Using these carbon materials as supports, Pt/CB electrocatalysts are prepared by microwave‐assisted polyol‐mediated synthesis in gram scale. Structural, morphological and electrochemical properties of the prepared electrocatalysts are evaluated by X‐ray diffraction, transmission electron microscopy, rotating disc electrode and in situ fuel cell characterisation of the corresponding membrane–electrode assemblies. The obtained results allow to establish a relationship between surface chemistry and electrochemical properties useful for the design of Pt/C catalyst layers with high performance and stability. |
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Abstract In this paper, an extensive characterisation of a range of carbon blacks (CB) with similar surface area but different surface chemistry is carried out by flow calorimetry, Raman spectroscopy, dynamic water vapour sorption, instrumental gas analysis, nitrogen adsorption/desorption and high potential chronoamperometry. Using these carbon materials as supports, Pt/CB electrocatalysts are prepared by microwave‐assisted polyol‐mediated synthesis in gram scale. Structural, morphological and electrochemical properties of the prepared electrocatalysts are evaluated by X‐ray diffraction, transmission electron microscopy, rotating disc electrode and in situ fuel cell characterisation of the corresponding membrane–electrode assemblies. The obtained results allow to establish a relationship between surface chemistry and electrochemical properties useful for the design of Pt/C catalyst layers with high performance and stability. |
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