Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate

The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate f...
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Gespeichert in:

Autor*in:	Zheng Fan [verfasserIn] Yan-Lan Huang [verfasserIn] Zhao Wang [verfasserIn] Han-Qi Guo [verfasserIn] Shang Shan [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2011

Übergeordnetes Werk:	In: Acta Crystallographica Section E - International Union of Crystallography, 2005, 67(2011), 11, Seite o3011-o3011
Übergeordnetes Werk:	volume:67 ; year:2011 ; number:11 ; pages:o3011-o3011

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1107/S1600536811042140

Katalog-ID:	DOAJ019696094

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520			\|a The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate fragment is approximately planar (r.m.s. deviation = 0.0052 Å); its mean plane is oriented at dihedral angles of 8.19 (15) and 85.70 (13)°, respectively, to the methoxyphenyl and phenyl rings. Intermolecular N—H...S hydrogen bonds and weak C—H...π interactions are observed in the crystal structure.
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allfields	10.1107/S1600536811042140 doi (DE-627)DOAJ019696094 (DE-599)DOAJ52ca930497d645168541383c45c8c61b DE-627 ger DE-627 rakwb eng QD901-999 Zheng Fan verfasserin aut Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate fragment is approximately planar (r.m.s. deviation = 0.0052 Å); its mean plane is oriented at dihedral angles of 8.19 (15) and 85.70 (13)°, respectively, to the methoxyphenyl and phenyl rings. Intermolecular N—H...S hydrogen bonds and weak C—H...π interactions are observed in the crystal structure. Crystallography Yan-Lan Huang verfasserin aut Zhao Wang verfasserin aut Han-Qi Guo verfasserin aut Shang Shan verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite o3011-o3011 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:o3011-o3011 https://doi.org/10.1107/S1600536811042140 kostenfrei https://doaj.org/article/52ca930497d645168541383c45c8c61b kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811042140 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 o3011-o3011
spelling	10.1107/S1600536811042140 doi (DE-627)DOAJ019696094 (DE-599)DOAJ52ca930497d645168541383c45c8c61b DE-627 ger DE-627 rakwb eng QD901-999 Zheng Fan verfasserin aut Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate fragment is approximately planar (r.m.s. deviation = 0.0052 Å); its mean plane is oriented at dihedral angles of 8.19 (15) and 85.70 (13)°, respectively, to the methoxyphenyl and phenyl rings. Intermolecular N—H...S hydrogen bonds and weak C—H...π interactions are observed in the crystal structure. Crystallography Yan-Lan Huang verfasserin aut Zhao Wang verfasserin aut Han-Qi Guo verfasserin aut Shang Shan verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite o3011-o3011 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:o3011-o3011 https://doi.org/10.1107/S1600536811042140 kostenfrei https://doaj.org/article/52ca930497d645168541383c45c8c61b kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811042140 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 o3011-o3011
allfields_unstemmed	10.1107/S1600536811042140 doi (DE-627)DOAJ019696094 (DE-599)DOAJ52ca930497d645168541383c45c8c61b DE-627 ger DE-627 rakwb eng QD901-999 Zheng Fan verfasserin aut Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate fragment is approximately planar (r.m.s. deviation = 0.0052 Å); its mean plane is oriented at dihedral angles of 8.19 (15) and 85.70 (13)°, respectively, to the methoxyphenyl and phenyl rings. Intermolecular N—H...S hydrogen bonds and weak C—H...π interactions are observed in the crystal structure. Crystallography Yan-Lan Huang verfasserin aut Zhao Wang verfasserin aut Han-Qi Guo verfasserin aut Shang Shan verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite o3011-o3011 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:o3011-o3011 https://doi.org/10.1107/S1600536811042140 kostenfrei https://doaj.org/article/52ca930497d645168541383c45c8c61b kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811042140 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 o3011-o3011
allfieldsGer	10.1107/S1600536811042140 doi (DE-627)DOAJ019696094 (DE-599)DOAJ52ca930497d645168541383c45c8c61b DE-627 ger DE-627 rakwb eng QD901-999 Zheng Fan verfasserin aut Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate fragment is approximately planar (r.m.s. deviation = 0.0052 Å); its mean plane is oriented at dihedral angles of 8.19 (15) and 85.70 (13)°, respectively, to the methoxyphenyl and phenyl rings. Intermolecular N—H...S hydrogen bonds and weak C—H...π interactions are observed in the crystal structure. Crystallography Yan-Lan Huang verfasserin aut Zhao Wang verfasserin aut Han-Qi Guo verfasserin aut Shang Shan verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite o3011-o3011 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:o3011-o3011 https://doi.org/10.1107/S1600536811042140 kostenfrei https://doaj.org/article/52ca930497d645168541383c45c8c61b kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811042140 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 o3011-o3011
allfieldsSound	10.1107/S1600536811042140 doi (DE-627)DOAJ019696094 (DE-599)DOAJ52ca930497d645168541383c45c8c61b DE-627 ger DE-627 rakwb eng QD901-999 Zheng Fan verfasserin aut Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate fragment is approximately planar (r.m.s. deviation = 0.0052 Å); its mean plane is oriented at dihedral angles of 8.19 (15) and 85.70 (13)°, respectively, to the methoxyphenyl and phenyl rings. Intermolecular N—H...S hydrogen bonds and weak C—H...π interactions are observed in the crystal structure. Crystallography Yan-Lan Huang verfasserin aut Zhao Wang verfasserin aut Han-Qi Guo verfasserin aut Shang Shan verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 67(2011), 11, Seite o3011-o3011 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:67 year:2011 number:11 pages:o3011-o3011 https://doi.org/10.1107/S1600536811042140 kostenfrei https://doaj.org/article/52ca930497d645168541383c45c8c61b kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536811042140 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 67 2011 11 o3011-o3011
language	English
source	In Acta Crystallographica Section E 67(2011), 11, Seite o3011-o3011 volume:67 year:2011 number:11 pages:o3011-o3011
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topic_facet	Crystallography
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container_title	Acta Crystallographica Section E
authorswithroles_txt_mv	Zheng Fan @@aut@@ Yan-Lan Huang @@aut@@ Zhao Wang @@aut@@ Han-Qi Guo @@aut@@ Shang Shan @@aut@@
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callnumber-first	Q - Science
author	Zheng Fan
spellingShingle	Zheng Fan misc QD901-999 misc Crystallography Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate
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topic_title	QD901-999 Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate
topic	misc QD901-999 misc Crystallography
topic_unstemmed	misc QD901-999 misc Crystallography
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title	Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate
ctrlnum	(DE-627)DOAJ019696094 (DE-599)DOAJ52ca930497d645168541383c45c8c61b
title_full	Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate
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title_sort	benzyl (e)-3-(4-methoxybenzylidene)dithiocarbazate
callnumber	QD901-999
title_auth	Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate
abstract	The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate fragment is approximately planar (r.m.s. deviation = 0.0052 Å); its mean plane is oriented at dihedral angles of 8.19 (15) and 85.70 (13)°, respectively, to the methoxyphenyl and phenyl rings. Intermolecular N—H...S hydrogen bonds and weak C—H...π interactions are observed in the crystal structure.
abstractGer	The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate fragment is approximately planar (r.m.s. deviation = 0.0052 Å); its mean plane is oriented at dihedral angles of 8.19 (15) and 85.70 (13)°, respectively, to the methoxyphenyl and phenyl rings. Intermolecular N—H...S hydrogen bonds and weak C—H...π interactions are observed in the crystal structure.
abstract_unstemmed	The title compound, C16H16N2OS2, was obtained from a condensation reaction of benzyl dithiocarbazate and 4-methoxybenzaldehyde. In the molecule, the methoxyphenyl ring and dithiocarbazate fragment are located on opposite sides of the C=N double bond, showing an E configuration. The dithiocarbazate fragment is approximately planar (r.m.s. deviation = 0.0052 Å); its mean plane is oriented at dihedral angles of 8.19 (15) and 85.70 (13)°, respectively, to the methoxyphenyl and phenyl rings. Intermolecular N—H...S hydrogen bonds and weak C—H...π interactions are observed in the crystal structure.
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title_short	Benzyl (E)-3-(4-methoxybenzylidene)dithiocarbazate
url	https://doi.org/10.1107/S1600536811042140 https://doaj.org/article/52ca930497d645168541383c45c8c61b http://scripts.iucr.org/cgi-bin/paper?S1600536811042140 https://doaj.org/toc/1600-5368
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