Extraction with Acidified Methanol—An Easy and Effective Method of Methyl Chlorogenate Formation, as Studied by ESI-MS
Among the different Hawthorn species, <i<Crataegus monogyna</i< seems to be one of the most often used in herbal medicine, and is commercially available. The methanolic extract and the acidified methanol extract of an herbal medicinal product based on <i<Crataegus monogyna</i<...
Ausführliche Beschreibung
Autor*in: |
Karolina Szymborska [verfasserIn] Rafał Frański [verfasserIn] Monika Beszterda-Buszczak [verfasserIn] |
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E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2022 |
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Übergeordnetes Werk: |
In: Molecules - MDPI AG, 2003, 27(2022), 21, p 7543 |
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Übergeordnetes Werk: |
volume:27 ; year:2022 ; number:21, p 7543 |
Links: |
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DOI / URN: |
10.3390/molecules27217543 |
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Katalog-ID: |
DOAJ020652518 |
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10.3390/molecules27217543 doi (DE-627)DOAJ020652518 (DE-599)DOAJ654bdababbd541a38508d415c31884bf DE-627 ger DE-627 rakwb eng QD241-441 Karolina Szymborska verfasserin aut Extraction with Acidified Methanol—An Easy and Effective Method of Methyl Chlorogenate Formation, as Studied by ESI-MS 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Among the different Hawthorn species, <i<Crataegus monogyna</i< seems to be one of the most often used in herbal medicine, and is commercially available. The methanolic extract and the acidified methanol extract of an herbal medicinal product based on <i<Crataegus monogyna</i< inflorescences were analyzed by using high-pressure liquid chromatography/electrospray ionization mass spectrometry (HPLC/ESI-MS). On the basis of <i<m/z</i< of [M-H]<sup<−</sup< ions and characteristic fragmentation patterns, a number of polyphenolic compounds, namely flavonoids and chlorogenic acids, were identified. It was found that the contents of the acid extract were enriched with methyl chlorogenates showing attractive biochemical properties. Analogous results were obtained for other plant materials, e.g., nectarine kernels. Apart from that, acid extraction had a minor influence on the polyphenolic compounds present in the plants, and thus it did not affect the natural antioxidant values of the plant extracts. <i<Crataegus monogyna</i< extraction liquid chromatography mass spectrometry methyl chlorogenate chlorogenic acids Organic chemistry Rafał Frański verfasserin aut Monika Beszterda-Buszczak verfasserin aut In Molecules MDPI AG, 2003 27(2022), 21, p 7543 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:27 year:2022 number:21, p 7543 https://doi.org/10.3390/molecules27217543 kostenfrei https://doaj.org/article/654bdababbd541a38508d415c31884bf kostenfrei https://www.mdpi.com/1420-3049/27/21/7543 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 27 2022 21, p 7543 |
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10.3390/molecules27217543 doi (DE-627)DOAJ020652518 (DE-599)DOAJ654bdababbd541a38508d415c31884bf DE-627 ger DE-627 rakwb eng QD241-441 Karolina Szymborska verfasserin aut Extraction with Acidified Methanol—An Easy and Effective Method of Methyl Chlorogenate Formation, as Studied by ESI-MS 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Among the different Hawthorn species, <i<Crataegus monogyna</i< seems to be one of the most often used in herbal medicine, and is commercially available. The methanolic extract and the acidified methanol extract of an herbal medicinal product based on <i<Crataegus monogyna</i< inflorescences were analyzed by using high-pressure liquid chromatography/electrospray ionization mass spectrometry (HPLC/ESI-MS). On the basis of <i<m/z</i< of [M-H]<sup<−</sup< ions and characteristic fragmentation patterns, a number of polyphenolic compounds, namely flavonoids and chlorogenic acids, were identified. It was found that the contents of the acid extract were enriched with methyl chlorogenates showing attractive biochemical properties. Analogous results were obtained for other plant materials, e.g., nectarine kernels. Apart from that, acid extraction had a minor influence on the polyphenolic compounds present in the plants, and thus it did not affect the natural antioxidant values of the plant extracts. <i<Crataegus monogyna</i< extraction liquid chromatography mass spectrometry methyl chlorogenate chlorogenic acids Organic chemistry Rafał Frański verfasserin aut Monika Beszterda-Buszczak verfasserin aut In Molecules MDPI AG, 2003 27(2022), 21, p 7543 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:27 year:2022 number:21, p 7543 https://doi.org/10.3390/molecules27217543 kostenfrei https://doaj.org/article/654bdababbd541a38508d415c31884bf kostenfrei https://www.mdpi.com/1420-3049/27/21/7543 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 27 2022 21, p 7543 |
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10.3390/molecules27217543 doi (DE-627)DOAJ020652518 (DE-599)DOAJ654bdababbd541a38508d415c31884bf DE-627 ger DE-627 rakwb eng QD241-441 Karolina Szymborska verfasserin aut Extraction with Acidified Methanol—An Easy and Effective Method of Methyl Chlorogenate Formation, as Studied by ESI-MS 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Among the different Hawthorn species, <i<Crataegus monogyna</i< seems to be one of the most often used in herbal medicine, and is commercially available. The methanolic extract and the acidified methanol extract of an herbal medicinal product based on <i<Crataegus monogyna</i< inflorescences were analyzed by using high-pressure liquid chromatography/electrospray ionization mass spectrometry (HPLC/ESI-MS). On the basis of <i<m/z</i< of [M-H]<sup<−</sup< ions and characteristic fragmentation patterns, a number of polyphenolic compounds, namely flavonoids and chlorogenic acids, were identified. It was found that the contents of the acid extract were enriched with methyl chlorogenates showing attractive biochemical properties. Analogous results were obtained for other plant materials, e.g., nectarine kernels. Apart from that, acid extraction had a minor influence on the polyphenolic compounds present in the plants, and thus it did not affect the natural antioxidant values of the plant extracts. <i<Crataegus monogyna</i< extraction liquid chromatography mass spectrometry methyl chlorogenate chlorogenic acids Organic chemistry Rafał Frański verfasserin aut Monika Beszterda-Buszczak verfasserin aut In Molecules MDPI AG, 2003 27(2022), 21, p 7543 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:27 year:2022 number:21, p 7543 https://doi.org/10.3390/molecules27217543 kostenfrei https://doaj.org/article/654bdababbd541a38508d415c31884bf kostenfrei https://www.mdpi.com/1420-3049/27/21/7543 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 27 2022 21, p 7543 |
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10.3390/molecules27217543 doi (DE-627)DOAJ020652518 (DE-599)DOAJ654bdababbd541a38508d415c31884bf DE-627 ger DE-627 rakwb eng QD241-441 Karolina Szymborska verfasserin aut Extraction with Acidified Methanol—An Easy and Effective Method of Methyl Chlorogenate Formation, as Studied by ESI-MS 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Among the different Hawthorn species, <i<Crataegus monogyna</i< seems to be one of the most often used in herbal medicine, and is commercially available. The methanolic extract and the acidified methanol extract of an herbal medicinal product based on <i<Crataegus monogyna</i< inflorescences were analyzed by using high-pressure liquid chromatography/electrospray ionization mass spectrometry (HPLC/ESI-MS). On the basis of <i<m/z</i< of [M-H]<sup<−</sup< ions and characteristic fragmentation patterns, a number of polyphenolic compounds, namely flavonoids and chlorogenic acids, were identified. It was found that the contents of the acid extract were enriched with methyl chlorogenates showing attractive biochemical properties. Analogous results were obtained for other plant materials, e.g., nectarine kernels. Apart from that, acid extraction had a minor influence on the polyphenolic compounds present in the plants, and thus it did not affect the natural antioxidant values of the plant extracts. <i<Crataegus monogyna</i< extraction liquid chromatography mass spectrometry methyl chlorogenate chlorogenic acids Organic chemistry Rafał Frański verfasserin aut Monika Beszterda-Buszczak verfasserin aut In Molecules MDPI AG, 2003 27(2022), 21, p 7543 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:27 year:2022 number:21, p 7543 https://doi.org/10.3390/molecules27217543 kostenfrei https://doaj.org/article/654bdababbd541a38508d415c31884bf kostenfrei https://www.mdpi.com/1420-3049/27/21/7543 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 27 2022 21, p 7543 |
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10.3390/molecules27217543 doi (DE-627)DOAJ020652518 (DE-599)DOAJ654bdababbd541a38508d415c31884bf DE-627 ger DE-627 rakwb eng QD241-441 Karolina Szymborska verfasserin aut Extraction with Acidified Methanol—An Easy and Effective Method of Methyl Chlorogenate Formation, as Studied by ESI-MS 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Among the different Hawthorn species, <i<Crataegus monogyna</i< seems to be one of the most often used in herbal medicine, and is commercially available. The methanolic extract and the acidified methanol extract of an herbal medicinal product based on <i<Crataegus monogyna</i< inflorescences were analyzed by using high-pressure liquid chromatography/electrospray ionization mass spectrometry (HPLC/ESI-MS). On the basis of <i<m/z</i< of [M-H]<sup<−</sup< ions and characteristic fragmentation patterns, a number of polyphenolic compounds, namely flavonoids and chlorogenic acids, were identified. It was found that the contents of the acid extract were enriched with methyl chlorogenates showing attractive biochemical properties. Analogous results were obtained for other plant materials, e.g., nectarine kernels. Apart from that, acid extraction had a minor influence on the polyphenolic compounds present in the plants, and thus it did not affect the natural antioxidant values of the plant extracts. <i<Crataegus monogyna</i< extraction liquid chromatography mass spectrometry methyl chlorogenate chlorogenic acids Organic chemistry Rafał Frański verfasserin aut Monika Beszterda-Buszczak verfasserin aut In Molecules MDPI AG, 2003 27(2022), 21, p 7543 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:27 year:2022 number:21, p 7543 https://doi.org/10.3390/molecules27217543 kostenfrei https://doaj.org/article/654bdababbd541a38508d415c31884bf kostenfrei https://www.mdpi.com/1420-3049/27/21/7543 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 27 2022 21, p 7543 |
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Karolina Szymborska misc QD241-441 misc <i<Crataegus monogyna</i< misc extraction misc liquid chromatography misc mass spectrometry misc methyl chlorogenate misc chlorogenic acids misc Organic chemistry Extraction with Acidified Methanol—An Easy and Effective Method of Methyl Chlorogenate Formation, as Studied by ESI-MS |
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QD241-441 Extraction with Acidified Methanol—An Easy and Effective Method of Methyl Chlorogenate Formation, as Studied by ESI-MS <i<Crataegus monogyna</i< extraction liquid chromatography mass spectrometry methyl chlorogenate chlorogenic acids |
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Extraction with Acidified Methanol—An Easy and Effective Method of Methyl Chlorogenate Formation, as Studied by ESI-MS |
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Among the different Hawthorn species, <i<Crataegus monogyna</i< seems to be one of the most often used in herbal medicine, and is commercially available. The methanolic extract and the acidified methanol extract of an herbal medicinal product based on <i<Crataegus monogyna</i< inflorescences were analyzed by using high-pressure liquid chromatography/electrospray ionization mass spectrometry (HPLC/ESI-MS). On the basis of <i<m/z</i< of [M-H]<sup<−</sup< ions and characteristic fragmentation patterns, a number of polyphenolic compounds, namely flavonoids and chlorogenic acids, were identified. It was found that the contents of the acid extract were enriched with methyl chlorogenates showing attractive biochemical properties. Analogous results were obtained for other plant materials, e.g., nectarine kernels. Apart from that, acid extraction had a minor influence on the polyphenolic compounds present in the plants, and thus it did not affect the natural antioxidant values of the plant extracts. |
abstractGer |
Among the different Hawthorn species, <i<Crataegus monogyna</i< seems to be one of the most often used in herbal medicine, and is commercially available. The methanolic extract and the acidified methanol extract of an herbal medicinal product based on <i<Crataegus monogyna</i< inflorescences were analyzed by using high-pressure liquid chromatography/electrospray ionization mass spectrometry (HPLC/ESI-MS). On the basis of <i<m/z</i< of [M-H]<sup<−</sup< ions and characteristic fragmentation patterns, a number of polyphenolic compounds, namely flavonoids and chlorogenic acids, were identified. It was found that the contents of the acid extract were enriched with methyl chlorogenates showing attractive biochemical properties. Analogous results were obtained for other plant materials, e.g., nectarine kernels. Apart from that, acid extraction had a minor influence on the polyphenolic compounds present in the plants, and thus it did not affect the natural antioxidant values of the plant extracts. |
abstract_unstemmed |
Among the different Hawthorn species, <i<Crataegus monogyna</i< seems to be one of the most often used in herbal medicine, and is commercially available. The methanolic extract and the acidified methanol extract of an herbal medicinal product based on <i<Crataegus monogyna</i< inflorescences were analyzed by using high-pressure liquid chromatography/electrospray ionization mass spectrometry (HPLC/ESI-MS). On the basis of <i<m/z</i< of [M-H]<sup<−</sup< ions and characteristic fragmentation patterns, a number of polyphenolic compounds, namely flavonoids and chlorogenic acids, were identified. It was found that the contents of the acid extract were enriched with methyl chlorogenates showing attractive biochemical properties. Analogous results were obtained for other plant materials, e.g., nectarine kernels. Apart from that, acid extraction had a minor influence on the polyphenolic compounds present in the plants, and thus it did not affect the natural antioxidant values of the plant extracts. |
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7.400075 |