New experimental studies on the phase relationship of the Bi–Pb–Te system

Knowledge of the phase relationships is crucial in developing thermoelectric materials and allows a better understanding of the properties of the relevant systems. In the present work, we present the liquidus projection of the Bi-Pb-Te system and phase equilibria of the BiTe-PbTe-Bi2Te3 portion at 4...
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Autor*in:	Dandan Huang [verfasserIn] Dechen Xia [verfasserIn] Tianfan Ye [verfasserIn] Toyohisa Fujita [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2022

Schlagwörter:	Bi–Pb–Te Phase diagram Liquidus projection Experimental investigation Thermoelectric materials system

Übergeordnetes Werk:	In: Materials & Design - Elsevier, 2019, 224(2022), Seite 111384-
Übergeordnetes Werk:	volume:224 ; year:2022 ; pages:111384-

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1016/j.matdes.2022.111384

Katalog-ID:	DOAJ024850829

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spelling	10.1016/j.matdes.2022.111384 doi (DE-627)DOAJ024850829 (DE-599)DOAJ4274915b5d6e49a997f8b4a9a1a8ccf1 DE-627 ger DE-627 rakwb eng TA401-492 Dandan Huang verfasserin aut New experimental studies on the phase relationship of the Bi–Pb–Te system 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Knowledge of the phase relationships is crucial in developing thermoelectric materials and allows a better understanding of the properties of the relevant systems. In the present work, we present the liquidus projection of the Bi-Pb-Te system and phase equilibria of the BiTe-PbTe-Bi2Te3 portion at 400 and 520 °C. Alloys were prepared by melting high-purity elements in cleaned quartz tubes and their microstructures were characterized by scanning electron microscopy, electron probe microanalysis, wavelength-dispersive X-ray spectrometer, X-ray diffractometry and differential scanning calorimetry. The binary compound BiTe extends up to 16.7 at.% Pb along BiTe-PbTe at 520 °C. The solubilities of Bi in PbTe were established to be 3.6, 3.8 and 10.8 at.% at 360, 400 and 520 °C, respectively. This work will help to understand the microstructure evolution during preparation and service and promote the designing of the Bi–Pb–Te-based high-performance materials. Bi–Pb–Te Phase diagram Liquidus projection Experimental investigation Thermoelectric materials system Materials of engineering and construction. Mechanics of materials Dechen Xia verfasserin aut Tianfan Ye verfasserin aut Toyohisa Fujita verfasserin aut In Materials & Design Elsevier, 2019 224(2022), Seite 111384- (DE-627)32052857X (DE-600)2015480-X 18734197 nnns volume:224 year:2022 pages:111384- https://doi.org/10.1016/j.matdes.2022.111384 kostenfrei https://doaj.org/article/4274915b5d6e49a997f8b4a9a1a8ccf1 kostenfrei http://www.sciencedirect.com/science/article/pii/S0264127522010061 kostenfrei https://doaj.org/toc/0264-1275 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 224 2022 111384-
allfields_unstemmed	10.1016/j.matdes.2022.111384 doi (DE-627)DOAJ024850829 (DE-599)DOAJ4274915b5d6e49a997f8b4a9a1a8ccf1 DE-627 ger DE-627 rakwb eng TA401-492 Dandan Huang verfasserin aut New experimental studies on the phase relationship of the Bi–Pb–Te system 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Knowledge of the phase relationships is crucial in developing thermoelectric materials and allows a better understanding of the properties of the relevant systems. In the present work, we present the liquidus projection of the Bi-Pb-Te system and phase equilibria of the BiTe-PbTe-Bi2Te3 portion at 400 and 520 °C. Alloys were prepared by melting high-purity elements in cleaned quartz tubes and their microstructures were characterized by scanning electron microscopy, electron probe microanalysis, wavelength-dispersive X-ray spectrometer, X-ray diffractometry and differential scanning calorimetry. The binary compound BiTe extends up to 16.7 at.% Pb along BiTe-PbTe at 520 °C. The solubilities of Bi in PbTe were established to be 3.6, 3.8 and 10.8 at.% at 360, 400 and 520 °C, respectively. This work will help to understand the microstructure evolution during preparation and service and promote the designing of the Bi–Pb–Te-based high-performance materials. Bi–Pb–Te Phase diagram Liquidus projection Experimental investigation Thermoelectric materials system Materials of engineering and construction. Mechanics of materials Dechen Xia verfasserin aut Tianfan Ye verfasserin aut Toyohisa Fujita verfasserin aut In Materials & Design Elsevier, 2019 224(2022), Seite 111384- (DE-627)32052857X (DE-600)2015480-X 18734197 nnns volume:224 year:2022 pages:111384- https://doi.org/10.1016/j.matdes.2022.111384 kostenfrei https://doaj.org/article/4274915b5d6e49a997f8b4a9a1a8ccf1 kostenfrei http://www.sciencedirect.com/science/article/pii/S0264127522010061 kostenfrei https://doaj.org/toc/0264-1275 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 224 2022 111384-
allfieldsGer	10.1016/j.matdes.2022.111384 doi (DE-627)DOAJ024850829 (DE-599)DOAJ4274915b5d6e49a997f8b4a9a1a8ccf1 DE-627 ger DE-627 rakwb eng TA401-492 Dandan Huang verfasserin aut New experimental studies on the phase relationship of the Bi–Pb–Te system 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Knowledge of the phase relationships is crucial in developing thermoelectric materials and allows a better understanding of the properties of the relevant systems. In the present work, we present the liquidus projection of the Bi-Pb-Te system and phase equilibria of the BiTe-PbTe-Bi2Te3 portion at 400 and 520 °C. Alloys were prepared by melting high-purity elements in cleaned quartz tubes and their microstructures were characterized by scanning electron microscopy, electron probe microanalysis, wavelength-dispersive X-ray spectrometer, X-ray diffractometry and differential scanning calorimetry. The binary compound BiTe extends up to 16.7 at.% Pb along BiTe-PbTe at 520 °C. The solubilities of Bi in PbTe were established to be 3.6, 3.8 and 10.8 at.% at 360, 400 and 520 °C, respectively. This work will help to understand the microstructure evolution during preparation and service and promote the designing of the Bi–Pb–Te-based high-performance materials. Bi–Pb–Te Phase diagram Liquidus projection Experimental investigation Thermoelectric materials system Materials of engineering and construction. Mechanics of materials Dechen Xia verfasserin aut Tianfan Ye verfasserin aut Toyohisa Fujita verfasserin aut In Materials & Design Elsevier, 2019 224(2022), Seite 111384- (DE-627)32052857X (DE-600)2015480-X 18734197 nnns volume:224 year:2022 pages:111384- https://doi.org/10.1016/j.matdes.2022.111384 kostenfrei https://doaj.org/article/4274915b5d6e49a997f8b4a9a1a8ccf1 kostenfrei http://www.sciencedirect.com/science/article/pii/S0264127522010061 kostenfrei https://doaj.org/toc/0264-1275 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 224 2022 111384-
allfieldsSound	10.1016/j.matdes.2022.111384 doi (DE-627)DOAJ024850829 (DE-599)DOAJ4274915b5d6e49a997f8b4a9a1a8ccf1 DE-627 ger DE-627 rakwb eng TA401-492 Dandan Huang verfasserin aut New experimental studies on the phase relationship of the Bi–Pb–Te system 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Knowledge of the phase relationships is crucial in developing thermoelectric materials and allows a better understanding of the properties of the relevant systems. In the present work, we present the liquidus projection of the Bi-Pb-Te system and phase equilibria of the BiTe-PbTe-Bi2Te3 portion at 400 and 520 °C. Alloys were prepared by melting high-purity elements in cleaned quartz tubes and their microstructures were characterized by scanning electron microscopy, electron probe microanalysis, wavelength-dispersive X-ray spectrometer, X-ray diffractometry and differential scanning calorimetry. The binary compound BiTe extends up to 16.7 at.% Pb along BiTe-PbTe at 520 °C. The solubilities of Bi in PbTe were established to be 3.6, 3.8 and 10.8 at.% at 360, 400 and 520 °C, respectively. This work will help to understand the microstructure evolution during preparation and service and promote the designing of the Bi–Pb–Te-based high-performance materials. Bi–Pb–Te Phase diagram Liquidus projection Experimental investigation Thermoelectric materials system Materials of engineering and construction. Mechanics of materials Dechen Xia verfasserin aut Tianfan Ye verfasserin aut Toyohisa Fujita verfasserin aut In Materials & Design Elsevier, 2019 224(2022), Seite 111384- (DE-627)32052857X (DE-600)2015480-X 18734197 nnns volume:224 year:2022 pages:111384- https://doi.org/10.1016/j.matdes.2022.111384 kostenfrei https://doaj.org/article/4274915b5d6e49a997f8b4a9a1a8ccf1 kostenfrei http://www.sciencedirect.com/science/article/pii/S0264127522010061 kostenfrei https://doaj.org/toc/0264-1275 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 224 2022 111384-
language	English
source	In Materials & Design 224(2022), Seite 111384- volume:224 year:2022 pages:111384-
sourceStr	In Materials & Design 224(2022), Seite 111384- volume:224 year:2022 pages:111384-
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Bi–Pb–Te Phase diagram Liquidus projection Experimental investigation Thermoelectric materials system Materials of engineering and construction. Mechanics of materials
isfreeaccess_bool	true
container_title	Materials & Design
authorswithroles_txt_mv	Dandan Huang @@aut@@ Dechen Xia @@aut@@ Tianfan Ye @@aut@@ Toyohisa Fujita @@aut@@
publishDateDaySort_date	2022-01-01T00:00:00Z
hierarchy_top_id	32052857X
id	DOAJ024850829
language_de	englisch
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callnumber-first	T - Technology
author	Dandan Huang
spellingShingle	Dandan Huang misc TA401-492 misc Bi–Pb–Te misc Phase diagram misc Liquidus projection misc Experimental investigation misc Thermoelectric materials system misc Materials of engineering and construction. Mechanics of materials New experimental studies on the phase relationship of the Bi–Pb–Te system
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topic_title	TA401-492 New experimental studies on the phase relationship of the Bi–Pb–Te system Bi–Pb–Te Phase diagram Liquidus projection Experimental investigation Thermoelectric materials system
topic	misc TA401-492 misc Bi–Pb–Te misc Phase diagram misc Liquidus projection misc Experimental investigation misc Thermoelectric materials system misc Materials of engineering and construction. Mechanics of materials
topic_unstemmed	misc TA401-492 misc Bi–Pb–Te misc Phase diagram misc Liquidus projection misc Experimental investigation misc Thermoelectric materials system misc Materials of engineering and construction. Mechanics of materials
topic_browse	misc TA401-492 misc Bi–Pb–Te misc Phase diagram misc Liquidus projection misc Experimental investigation misc Thermoelectric materials system misc Materials of engineering and construction. Mechanics of materials
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title	New experimental studies on the phase relationship of the Bi–Pb–Te system
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title_full	New experimental studies on the phase relationship of the Bi–Pb–Te system
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title_sort	new experimental studies on the phase relationship of the bi–pb–te system
callnumber	TA401-492
title_auth	New experimental studies on the phase relationship of the Bi–Pb–Te system
abstract	Knowledge of the phase relationships is crucial in developing thermoelectric materials and allows a better understanding of the properties of the relevant systems. In the present work, we present the liquidus projection of the Bi-Pb-Te system and phase equilibria of the BiTe-PbTe-Bi2Te3 portion at 400 and 520 °C. Alloys were prepared by melting high-purity elements in cleaned quartz tubes and their microstructures were characterized by scanning electron microscopy, electron probe microanalysis, wavelength-dispersive X-ray spectrometer, X-ray diffractometry and differential scanning calorimetry. The binary compound BiTe extends up to 16.7 at.% Pb along BiTe-PbTe at 520 °C. The solubilities of Bi in PbTe were established to be 3.6, 3.8 and 10.8 at.% at 360, 400 and 520 °C, respectively. This work will help to understand the microstructure evolution during preparation and service and promote the designing of the Bi–Pb–Te-based high-performance materials.
abstractGer	Knowledge of the phase relationships is crucial in developing thermoelectric materials and allows a better understanding of the properties of the relevant systems. In the present work, we present the liquidus projection of the Bi-Pb-Te system and phase equilibria of the BiTe-PbTe-Bi2Te3 portion at 400 and 520 °C. Alloys were prepared by melting high-purity elements in cleaned quartz tubes and their microstructures were characterized by scanning electron microscopy, electron probe microanalysis, wavelength-dispersive X-ray spectrometer, X-ray diffractometry and differential scanning calorimetry. The binary compound BiTe extends up to 16.7 at.% Pb along BiTe-PbTe at 520 °C. The solubilities of Bi in PbTe were established to be 3.6, 3.8 and 10.8 at.% at 360, 400 and 520 °C, respectively. This work will help to understand the microstructure evolution during preparation and service and promote the designing of the Bi–Pb–Te-based high-performance materials.
abstract_unstemmed	Knowledge of the phase relationships is crucial in developing thermoelectric materials and allows a better understanding of the properties of the relevant systems. In the present work, we present the liquidus projection of the Bi-Pb-Te system and phase equilibria of the BiTe-PbTe-Bi2Te3 portion at 400 and 520 °C. Alloys were prepared by melting high-purity elements in cleaned quartz tubes and their microstructures were characterized by scanning electron microscopy, electron probe microanalysis, wavelength-dispersive X-ray spectrometer, X-ray diffractometry and differential scanning calorimetry. The binary compound BiTe extends up to 16.7 at.% Pb along BiTe-PbTe at 520 °C. The solubilities of Bi in PbTe were established to be 3.6, 3.8 and 10.8 at.% at 360, 400 and 520 °C, respectively. This work will help to understand the microstructure evolution during preparation and service and promote the designing of the Bi–Pb–Te-based high-performance materials.
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title_short	New experimental studies on the phase relationship of the Bi–Pb–Te system
url	https://doi.org/10.1016/j.matdes.2022.111384 https://doaj.org/article/4274915b5d6e49a997f8b4a9a1a8ccf1 http://www.sciencedirect.com/science/article/pii/S0264127522010061 https://doaj.org/toc/0264-1275
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In the present work, we present the liquidus projection of the Bi-Pb-Te system and phase equilibria of the BiTe-PbTe-Bi2Te3 portion at 400 and 520 °C. Alloys were prepared by melting high-purity elements in cleaned quartz tubes and their microstructures were characterized by scanning electron microscopy, electron probe microanalysis, wavelength-dispersive X-ray spectrometer, X-ray diffractometry and differential scanning calorimetry. The binary compound BiTe extends up to 16.7 at.% Pb along BiTe-PbTe at 520 °C. The solubilities of Bi in PbTe were established to be 3.6, 3.8 and 10.8 at.% at 360, 400 and 520 °C, respectively. 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New experimental studies on the phase relationship of the Bi–Pb–Te system

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