The channel structure of trithallium pentaantimonate(V), Tl3Sb5O14
Single crystals of Tl3Sb5O14 were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K3Sb5O14, Rb3Sb5O14 and Cs3Sb5O14 analogues with orthorhombic Pbam symmetry and cell parameters a =...
Ausführliche Beschreibung
Autor*in: |
Paul Sicher [verfasserIn] Berthold Stöger [verfasserIn] |
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Sprache: |
Englisch |
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2022 |
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In: Acta Crystallographica Section E: Crystallographic Communications - International Union of Crystallography, 2015, 78(2022), 4, Seite 414-417 |
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Übergeordnetes Werk: |
volume:78 ; year:2022 ; number:4 ; pages:414-417 |
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DOI / URN: |
10.1107/S2056989022002869 |
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Katalog-ID: |
DOAJ026332507 |
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10.1107/S2056989022002869 doi (DE-627)DOAJ026332507 (DE-599)DOAJ22e1d41f269c4a6b9a2cfef7561f080f DE-627 ger DE-627 rakwb eng QD901-999 Paul Sicher verfasserin aut The channel structure of trithallium pentaantimonate(V), Tl3Sb5O14 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Single crystals of Tl3Sb5O14 were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K3Sb5O14, Rb3Sb5O14 and Cs3Sb5O14 analogues with orthorhombic Pbam symmetry and cell parameters a = 24.2899 (9) Å, b = 7.1931 (3) Å, c = 7.4182 (3) Å. The Sb atoms form irregular [SbO6] octahedra, which are linked via edges and corners into a triperiodic network. The Tl+ ions are located in distinct channels of the network extending along [010] and [001]. crystal structure channel structure antimonate(v) Crystallography Berthold Stöger verfasserin aut In Acta Crystallographica Section E: Crystallographic Communications International Union of Crystallography, 2015 78(2022), 4, Seite 414-417 (DE-627)845400835 (DE-600)2843762-7 20569890 nnns volume:78 year:2022 number:4 pages:414-417 https://doi.org/10.1107/S2056989022002869 kostenfrei https://doaj.org/article/22e1d41f269c4a6b9a2cfef7561f080f kostenfrei http://scripts.iucr.org/cgi-bin/paper?S2056989022002869 kostenfrei https://doaj.org/toc/2056-9890 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 78 2022 4 414-417 |
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10.1107/S2056989022002869 doi (DE-627)DOAJ026332507 (DE-599)DOAJ22e1d41f269c4a6b9a2cfef7561f080f DE-627 ger DE-627 rakwb eng QD901-999 Paul Sicher verfasserin aut The channel structure of trithallium pentaantimonate(V), Tl3Sb5O14 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Single crystals of Tl3Sb5O14 were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K3Sb5O14, Rb3Sb5O14 and Cs3Sb5O14 analogues with orthorhombic Pbam symmetry and cell parameters a = 24.2899 (9) Å, b = 7.1931 (3) Å, c = 7.4182 (3) Å. The Sb atoms form irregular [SbO6] octahedra, which are linked via edges and corners into a triperiodic network. The Tl+ ions are located in distinct channels of the network extending along [010] and [001]. crystal structure channel structure antimonate(v) Crystallography Berthold Stöger verfasserin aut In Acta Crystallographica Section E: Crystallographic Communications International Union of Crystallography, 2015 78(2022), 4, Seite 414-417 (DE-627)845400835 (DE-600)2843762-7 20569890 nnns volume:78 year:2022 number:4 pages:414-417 https://doi.org/10.1107/S2056989022002869 kostenfrei https://doaj.org/article/22e1d41f269c4a6b9a2cfef7561f080f kostenfrei http://scripts.iucr.org/cgi-bin/paper?S2056989022002869 kostenfrei https://doaj.org/toc/2056-9890 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 78 2022 4 414-417 |
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10.1107/S2056989022002869 doi (DE-627)DOAJ026332507 (DE-599)DOAJ22e1d41f269c4a6b9a2cfef7561f080f DE-627 ger DE-627 rakwb eng QD901-999 Paul Sicher verfasserin aut The channel structure of trithallium pentaantimonate(V), Tl3Sb5O14 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Single crystals of Tl3Sb5O14 were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K3Sb5O14, Rb3Sb5O14 and Cs3Sb5O14 analogues with orthorhombic Pbam symmetry and cell parameters a = 24.2899 (9) Å, b = 7.1931 (3) Å, c = 7.4182 (3) Å. The Sb atoms form irregular [SbO6] octahedra, which are linked via edges and corners into a triperiodic network. The Tl+ ions are located in distinct channels of the network extending along [010] and [001]. crystal structure channel structure antimonate(v) Crystallography Berthold Stöger verfasserin aut In Acta Crystallographica Section E: Crystallographic Communications International Union of Crystallography, 2015 78(2022), 4, Seite 414-417 (DE-627)845400835 (DE-600)2843762-7 20569890 nnns volume:78 year:2022 number:4 pages:414-417 https://doi.org/10.1107/S2056989022002869 kostenfrei https://doaj.org/article/22e1d41f269c4a6b9a2cfef7561f080f kostenfrei http://scripts.iucr.org/cgi-bin/paper?S2056989022002869 kostenfrei https://doaj.org/toc/2056-9890 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 78 2022 4 414-417 |
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10.1107/S2056989022002869 doi (DE-627)DOAJ026332507 (DE-599)DOAJ22e1d41f269c4a6b9a2cfef7561f080f DE-627 ger DE-627 rakwb eng QD901-999 Paul Sicher verfasserin aut The channel structure of trithallium pentaantimonate(V), Tl3Sb5O14 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Single crystals of Tl3Sb5O14 were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K3Sb5O14, Rb3Sb5O14 and Cs3Sb5O14 analogues with orthorhombic Pbam symmetry and cell parameters a = 24.2899 (9) Å, b = 7.1931 (3) Å, c = 7.4182 (3) Å. The Sb atoms form irregular [SbO6] octahedra, which are linked via edges and corners into a triperiodic network. The Tl+ ions are located in distinct channels of the network extending along [010] and [001]. crystal structure channel structure antimonate(v) Crystallography Berthold Stöger verfasserin aut In Acta Crystallographica Section E: Crystallographic Communications International Union of Crystallography, 2015 78(2022), 4, Seite 414-417 (DE-627)845400835 (DE-600)2843762-7 20569890 nnns volume:78 year:2022 number:4 pages:414-417 https://doi.org/10.1107/S2056989022002869 kostenfrei https://doaj.org/article/22e1d41f269c4a6b9a2cfef7561f080f kostenfrei http://scripts.iucr.org/cgi-bin/paper?S2056989022002869 kostenfrei https://doaj.org/toc/2056-9890 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 78 2022 4 414-417 |
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10.1107/S2056989022002869 doi (DE-627)DOAJ026332507 (DE-599)DOAJ22e1d41f269c4a6b9a2cfef7561f080f DE-627 ger DE-627 rakwb eng QD901-999 Paul Sicher verfasserin aut The channel structure of trithallium pentaantimonate(V), Tl3Sb5O14 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Single crystals of Tl3Sb5O14 were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K3Sb5O14, Rb3Sb5O14 and Cs3Sb5O14 analogues with orthorhombic Pbam symmetry and cell parameters a = 24.2899 (9) Å, b = 7.1931 (3) Å, c = 7.4182 (3) Å. The Sb atoms form irregular [SbO6] octahedra, which are linked via edges and corners into a triperiodic network. The Tl+ ions are located in distinct channels of the network extending along [010] and [001]. crystal structure channel structure antimonate(v) Crystallography Berthold Stöger verfasserin aut In Acta Crystallographica Section E: Crystallographic Communications International Union of Crystallography, 2015 78(2022), 4, Seite 414-417 (DE-627)845400835 (DE-600)2843762-7 20569890 nnns volume:78 year:2022 number:4 pages:414-417 https://doi.org/10.1107/S2056989022002869 kostenfrei https://doaj.org/article/22e1d41f269c4a6b9a2cfef7561f080f kostenfrei http://scripts.iucr.org/cgi-bin/paper?S2056989022002869 kostenfrei https://doaj.org/toc/2056-9890 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 78 2022 4 414-417 |
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The channel structure of trithallium pentaantimonate(V), Tl3Sb5O14 |
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Single crystals of Tl3Sb5O14 were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K3Sb5O14, Rb3Sb5O14 and Cs3Sb5O14 analogues with orthorhombic Pbam symmetry and cell parameters a = 24.2899 (9) Å, b = 7.1931 (3) Å, c = 7.4182 (3) Å. The Sb atoms form irregular [SbO6] octahedra, which are linked via edges and corners into a triperiodic network. The Tl+ ions are located in distinct channels of the network extending along [010] and [001]. |
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Single crystals of Tl3Sb5O14 were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K3Sb5O14, Rb3Sb5O14 and Cs3Sb5O14 analogues with orthorhombic Pbam symmetry and cell parameters a = 24.2899 (9) Å, b = 7.1931 (3) Å, c = 7.4182 (3) Å. The Sb atoms form irregular [SbO6] octahedra, which are linked via edges and corners into a triperiodic network. The Tl+ ions are located in distinct channels of the network extending along [010] and [001]. |
abstract_unstemmed |
Single crystals of Tl3Sb5O14 were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K3Sb5O14, Rb3Sb5O14 and Cs3Sb5O14 analogues with orthorhombic Pbam symmetry and cell parameters a = 24.2899 (9) Å, b = 7.1931 (3) Å, c = 7.4182 (3) Å. The Sb atoms form irregular [SbO6] octahedra, which are linked via edges and corners into a triperiodic network. The Tl+ ions are located in distinct channels of the network extending along [010] and [001]. |
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The channel structure of trithallium pentaantimonate(V), Tl3Sb5O14 |
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