Application and Validation of Analytical Software (SQX) for Semi-Quantitative Determination of the Main Chemical Composition of Solid, Bulk and Powder Fuel Samples by Wavelength Dispersive X-ray Fluorescence Technique

Determination of the content of chemical elements occurring in waste in large, small and trace amounts was performed using two instrumental analysis techniques: ICP-OES—Inductively Coupled Plasma Optical Emission Spectrometry and WDXRF—Wavelength Dispersive X-ray Fluorescence Spectrometry. Since suc...
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Gespeichert in:

Autor*in:	Adam Smoliński [verfasserIn] Marek Stempin [verfasserIn] Natalia Howaniec [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2022

Schlagwörter:	XRF WDXRF ICP-OES X-ray fluorescence spectrometry

Übergeordnetes Werk:	In: Energies - MDPI AG, 2008, 15(2022), 19, p 7311
Übergeordnetes Werk:	volume:15 ; year:2022 ; number:19, p 7311

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/en15197311

Katalog-ID:	DOAJ028315804

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author	Adam Smoliński
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topic_title	Application and Validation of Analytical Software (SQX) for Semi-Quantitative Determination of the Main Chemical Composition of Solid, Bulk and Powder Fuel Samples by Wavelength Dispersive X-ray Fluorescence Technique XRF WDXRF ICP-OES X-ray fluorescence spectrometry
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title	Application and Validation of Analytical Software (SQX) for Semi-Quantitative Determination of the Main Chemical Composition of Solid, Bulk and Powder Fuel Samples by Wavelength Dispersive X-ray Fluorescence Technique
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title_full	Application and Validation of Analytical Software (SQX) for Semi-Quantitative Determination of the Main Chemical Composition of Solid, Bulk and Powder Fuel Samples by Wavelength Dispersive X-ray Fluorescence Technique
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title_sort	application and validation of analytical software (sqx) for semi-quantitative determination of the main chemical composition of solid, bulk and powder fuel samples by wavelength dispersive x-ray fluorescence technique
title_auth	Application and Validation of Analytical Software (SQX) for Semi-Quantitative Determination of the Main Chemical Composition of Solid, Bulk and Powder Fuel Samples by Wavelength Dispersive X-ray Fluorescence Technique
abstract	Determination of the content of chemical elements occurring in waste in large, small and trace amounts was performed using two instrumental analysis techniques: ICP-OES—Inductively Coupled Plasma Optical Emission Spectrometry and WDXRF—Wavelength Dispersive X-ray Fluorescence Spectrometry. Since such analyses are expensive and time-consuming, the objective of the work presented in this paper was the development of a quick and inexpensive method for preliminary, scanning-based identification of the chemical composition of tested samples (solid, bulk or powder) using standardless, semi-quantitative analysis. An optimized method of preparing samples for X-ray measurements by pressing into a durable tablet, universal for all materials tested, was developed. Moreover, limits of quantification were determined, and the uncertainty of the results obtained was estimated by comparing them with the results acquired with the use of the accredited calibration method, employing standards and certified reference materials.
abstractGer	Determination of the content of chemical elements occurring in waste in large, small and trace amounts was performed using two instrumental analysis techniques: ICP-OES—Inductively Coupled Plasma Optical Emission Spectrometry and WDXRF—Wavelength Dispersive X-ray Fluorescence Spectrometry. Since such analyses are expensive and time-consuming, the objective of the work presented in this paper was the development of a quick and inexpensive method for preliminary, scanning-based identification of the chemical composition of tested samples (solid, bulk or powder) using standardless, semi-quantitative analysis. An optimized method of preparing samples for X-ray measurements by pressing into a durable tablet, universal for all materials tested, was developed. Moreover, limits of quantification were determined, and the uncertainty of the results obtained was estimated by comparing them with the results acquired with the use of the accredited calibration method, employing standards and certified reference materials.
abstract_unstemmed	Determination of the content of chemical elements occurring in waste in large, small and trace amounts was performed using two instrumental analysis techniques: ICP-OES—Inductively Coupled Plasma Optical Emission Spectrometry and WDXRF—Wavelength Dispersive X-ray Fluorescence Spectrometry. Since such analyses are expensive and time-consuming, the objective of the work presented in this paper was the development of a quick and inexpensive method for preliminary, scanning-based identification of the chemical composition of tested samples (solid, bulk or powder) using standardless, semi-quantitative analysis. An optimized method of preparing samples for X-ray measurements by pressing into a durable tablet, universal for all materials tested, was developed. Moreover, limits of quantification were determined, and the uncertainty of the results obtained was estimated by comparing them with the results acquired with the use of the accredited calibration method, employing standards and certified reference materials.
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title_short	Application and Validation of Analytical Software (SQX) for Semi-Quantitative Determination of the Main Chemical Composition of Solid, Bulk and Powder Fuel Samples by Wavelength Dispersive X-ray Fluorescence Technique
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Application and Validation of Analytical Software (SQX) for Semi-Quantitative Determination of the Main Chemical Composition of Solid, Bulk and Powder Fuel Samples by Wavelength Dispersive X-ray Fluorescence Technique

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