Solid-phase synthesis of isoalloxazines using merrifield resin
The reaction of Merrifield resin bound diamino compounds with alloxan monohydrate gave 7-resin bound 10-substituted isoalloxazines that were characterized by solid phase fluorescence and IR spectroscopy. The resin was cleaved by 40% aqueous HF/DMF to give 7-carboxy-10-substituted isoalloxazines that...
Ausführliche Beschreibung
Autor*in: |
Geetanjali [verfasserIn] Singh Ram [verfasserIn] Chauhan S.M.S [verfasserIn] |
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Englisch |
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2006 |
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In: Journal of the Brazilian Chemical Society - Sociedade Brasileira de Química, 2017, 17(2006), 2, Seite 421-425 |
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Übergeordnetes Werk: |
volume:17 ; year:2006 ; number:2 ; pages:421-425 |
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Katalog-ID: |
DOAJ031213804 |
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(DE-627)DOAJ031213804 (DE-599)DOAJ7c48611de3ad430d847f358fe4606454 DE-627 ger DE-627 rakwb eng QD1-999 Geetanjali verfasserin aut Solid-phase synthesis of isoalloxazines using merrifield resin 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reaction of Merrifield resin bound diamino compounds with alloxan monohydrate gave 7-resin bound 10-substituted isoalloxazines that were characterized by solid phase fluorescence and IR spectroscopy. The resin was cleaved by 40% aqueous HF/DMF to give 7-carboxy-10-substituted isoalloxazines that were characterized by UV-vis., IR, ¹H NMR, fluorescence and elemental analysis isoalloxazines (or flavins) merrifield resin polymer-supported synthesis cyclocondensation alloxan monohydrate solid-state fluorescence Chemistry Singh Ram verfasserin aut Chauhan S.M.S verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 17(2006), 2, Seite 421-425 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:17 year:2006 number:2 pages:421-425 https://doaj.org/article/7c48611de3ad430d847f358fe4606454 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532006000200030 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei https://doaj.org/toc/1678-4790 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 17 2006 2 421-425 |
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(DE-627)DOAJ031213804 (DE-599)DOAJ7c48611de3ad430d847f358fe4606454 DE-627 ger DE-627 rakwb eng QD1-999 Geetanjali verfasserin aut Solid-phase synthesis of isoalloxazines using merrifield resin 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reaction of Merrifield resin bound diamino compounds with alloxan monohydrate gave 7-resin bound 10-substituted isoalloxazines that were characterized by solid phase fluorescence and IR spectroscopy. The resin was cleaved by 40% aqueous HF/DMF to give 7-carboxy-10-substituted isoalloxazines that were characterized by UV-vis., IR, ¹H NMR, fluorescence and elemental analysis isoalloxazines (or flavins) merrifield resin polymer-supported synthesis cyclocondensation alloxan monohydrate solid-state fluorescence Chemistry Singh Ram verfasserin aut Chauhan S.M.S verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 17(2006), 2, Seite 421-425 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:17 year:2006 number:2 pages:421-425 https://doaj.org/article/7c48611de3ad430d847f358fe4606454 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532006000200030 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei https://doaj.org/toc/1678-4790 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 17 2006 2 421-425 |
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(DE-627)DOAJ031213804 (DE-599)DOAJ7c48611de3ad430d847f358fe4606454 DE-627 ger DE-627 rakwb eng QD1-999 Geetanjali verfasserin aut Solid-phase synthesis of isoalloxazines using merrifield resin 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reaction of Merrifield resin bound diamino compounds with alloxan monohydrate gave 7-resin bound 10-substituted isoalloxazines that were characterized by solid phase fluorescence and IR spectroscopy. The resin was cleaved by 40% aqueous HF/DMF to give 7-carboxy-10-substituted isoalloxazines that were characterized by UV-vis., IR, ¹H NMR, fluorescence and elemental analysis isoalloxazines (or flavins) merrifield resin polymer-supported synthesis cyclocondensation alloxan monohydrate solid-state fluorescence Chemistry Singh Ram verfasserin aut Chauhan S.M.S verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 17(2006), 2, Seite 421-425 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:17 year:2006 number:2 pages:421-425 https://doaj.org/article/7c48611de3ad430d847f358fe4606454 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532006000200030 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei https://doaj.org/toc/1678-4790 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 17 2006 2 421-425 |
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(DE-627)DOAJ031213804 (DE-599)DOAJ7c48611de3ad430d847f358fe4606454 DE-627 ger DE-627 rakwb eng QD1-999 Geetanjali verfasserin aut Solid-phase synthesis of isoalloxazines using merrifield resin 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reaction of Merrifield resin bound diamino compounds with alloxan monohydrate gave 7-resin bound 10-substituted isoalloxazines that were characterized by solid phase fluorescence and IR spectroscopy. The resin was cleaved by 40% aqueous HF/DMF to give 7-carboxy-10-substituted isoalloxazines that were characterized by UV-vis., IR, ¹H NMR, fluorescence and elemental analysis isoalloxazines (or flavins) merrifield resin polymer-supported synthesis cyclocondensation alloxan monohydrate solid-state fluorescence Chemistry Singh Ram verfasserin aut Chauhan S.M.S verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 17(2006), 2, Seite 421-425 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:17 year:2006 number:2 pages:421-425 https://doaj.org/article/7c48611de3ad430d847f358fe4606454 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532006000200030 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei https://doaj.org/toc/1678-4790 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 17 2006 2 421-425 |
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(DE-627)DOAJ031213804 (DE-599)DOAJ7c48611de3ad430d847f358fe4606454 DE-627 ger DE-627 rakwb eng QD1-999 Geetanjali verfasserin aut Solid-phase synthesis of isoalloxazines using merrifield resin 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reaction of Merrifield resin bound diamino compounds with alloxan monohydrate gave 7-resin bound 10-substituted isoalloxazines that were characterized by solid phase fluorescence and IR spectroscopy. The resin was cleaved by 40% aqueous HF/DMF to give 7-carboxy-10-substituted isoalloxazines that were characterized by UV-vis., IR, ¹H NMR, fluorescence and elemental analysis isoalloxazines (or flavins) merrifield resin polymer-supported synthesis cyclocondensation alloxan monohydrate solid-state fluorescence Chemistry Singh Ram verfasserin aut Chauhan S.M.S verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 17(2006), 2, Seite 421-425 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:17 year:2006 number:2 pages:421-425 https://doaj.org/article/7c48611de3ad430d847f358fe4606454 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532006000200030 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei https://doaj.org/toc/1678-4790 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 17 2006 2 421-425 |
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QD1-999 Solid-phase synthesis of isoalloxazines using merrifield resin isoalloxazines (or flavins) merrifield resin polymer-supported synthesis cyclocondensation alloxan monohydrate solid-state fluorescence |
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Solid-phase synthesis of isoalloxazines using merrifield resin |
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Geetanjali Singh Ram Chauhan S.M.S |
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solid-phase synthesis of isoalloxazines using merrifield resin |
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Solid-phase synthesis of isoalloxazines using merrifield resin |
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The reaction of Merrifield resin bound diamino compounds with alloxan monohydrate gave 7-resin bound 10-substituted isoalloxazines that were characterized by solid phase fluorescence and IR spectroscopy. The resin was cleaved by 40% aqueous HF/DMF to give 7-carboxy-10-substituted isoalloxazines that were characterized by UV-vis., IR, ¹H NMR, fluorescence and elemental analysis |
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The reaction of Merrifield resin bound diamino compounds with alloxan monohydrate gave 7-resin bound 10-substituted isoalloxazines that were characterized by solid phase fluorescence and IR spectroscopy. The resin was cleaved by 40% aqueous HF/DMF to give 7-carboxy-10-substituted isoalloxazines that were characterized by UV-vis., IR, ¹H NMR, fluorescence and elemental analysis |
abstract_unstemmed |
The reaction of Merrifield resin bound diamino compounds with alloxan monohydrate gave 7-resin bound 10-substituted isoalloxazines that were characterized by solid phase fluorescence and IR spectroscopy. The resin was cleaved by 40% aqueous HF/DMF to give 7-carboxy-10-substituted isoalloxazines that were characterized by UV-vis., IR, ¹H NMR, fluorescence and elemental analysis |
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Solid-phase synthesis of isoalloxazines using merrifield resin |
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