Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite
Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplate...
Ausführliche Beschreibung
Autor*in: |
Filippo Farina [verfasserIn] Giorgio Ercolano [verfasserIn] Sara Cavaliere [verfasserIn] Deborah J. Jones [verfasserIn] Jacques Rozière [verfasserIn] |
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E-Artikel |
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Englisch |
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2018 |
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In: Nanomaterials - MDPI AG, 2012, 8(2018), 9, p 721 |
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Übergeordnetes Werk: |
volume:8 ; year:2018 ; number:9, p 721 |
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DOI / URN: |
10.3390/nano8090721 |
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Katalog-ID: |
DOAJ040554546 |
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10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721 |
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10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721 |
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10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721 |
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10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721 |
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10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721 |
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Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite |
abstract |
Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. |
abstractGer |
Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. |
abstract_unstemmed |
Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. |
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