Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite

Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplate...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Filippo Farina [verfasserIn] Giorgio Ercolano [verfasserIn] Sara Cavaliere [verfasserIn] Deborah J. Jones [verfasserIn] Jacques Rozière [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2018

Schlagwörter:	electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films

Übergeordnetes Werk:	In: Nanomaterials - MDPI AG, 2012, 8(2018), 9, p 721
Übergeordnetes Werk:	volume:8 ; year:2018 ; number:9, p 721

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/nano8090721

Katalog-ID:	DOAJ040554546

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520			\|a Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy.
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allfields	10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721
spelling	10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721
allfields_unstemmed	10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721
allfieldsGer	10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721
allfieldsSound	10.3390/nano8090721 doi (DE-627)DOAJ040554546 (DE-599)DOAJ508bf13684f14bf5a962c830221e07fc DE-627 ger DE-627 rakwb eng QD1-999 Filippo Farina verfasserin aut Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy. electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry Giorgio Ercolano verfasserin aut Sara Cavaliere verfasserin aut Deborah J. Jones verfasserin aut Jacques Rozière verfasserin aut In Nanomaterials MDPI AG, 2012 8(2018), 9, p 721 (DE-627)718627199 (DE-600)2662255-5 20794991 nnns volume:8 year:2018 number:9, p 721 https://doi.org/10.3390/nano8090721 kostenfrei https://doaj.org/article/508bf13684f14bf5a962c830221e07fc kostenfrei http://www.mdpi.com/2079-4991/8/9/721 kostenfrei https://doaj.org/toc/2079-4991 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 8 2018 9, p 721
language	English
source	In Nanomaterials 8(2018), 9, p 721 volume:8 year:2018 number:9, p 721
sourceStr	In Nanomaterials 8(2018), 9, p 721 volume:8 year:2018 number:9, p 721
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topic_facet	electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films Chemistry
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container_title	Nanomaterials
authorswithroles_txt_mv	Filippo Farina @@aut@@ Giorgio Ercolano @@aut@@ Sara Cavaliere @@aut@@ Deborah J. Jones @@aut@@ Jacques Rozière @@aut@@
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callnumber-first	Q - Science
author	Filippo Farina
spellingShingle	Filippo Farina misc QD1-999 misc electrodeposition misc platinum misc highly oriented pyrolytic graphite misc 2D growth misc thin films misc Chemistry Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite
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topic_title	QD1-999 Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite electrodeposition platinum highly oriented pyrolytic graphite 2D growth thin films
topic	misc QD1-999 misc electrodeposition misc platinum misc highly oriented pyrolytic graphite misc 2D growth misc thin films misc Chemistry
topic_unstemmed	misc QD1-999 misc electrodeposition misc platinum misc highly oriented pyrolytic graphite misc 2D growth misc thin films misc Chemistry
topic_browse	misc QD1-999 misc electrodeposition misc platinum misc highly oriented pyrolytic graphite misc 2D growth misc thin films misc Chemistry
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title	Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite
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title_full	Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite
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author_browse	Filippo Farina Giorgio Ercolano Sara Cavaliere Deborah J. Jones Jacques Rozière
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title_sort	surface-limited electrodeposition of continuous platinum networks on highly ordered pyrolytic graphite
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title_auth	Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite
abstract	Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy.
abstractGer	Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy.
abstract_unstemmed	Continuous thin platinum nanoplatelet networks and thin films were obtained on the flat surface of highly ordered pyrolytic graphite (HOPG) by high overpotential electrodeposition. By increasing the deposition time, the morphology of the Pt deposits can be progressively tuned from isolated nanoplatelets, interconnected nanostructures, and thin large flat islands. The deposition is surface-limited and the thickness of the deposits, equivalent to 5 to 12 Pt monolayers, is not time dependent. The presence of Pt (111) facets is confirmed by High Resolution Transmission Electron Microscopy (HRTEM) and evidence for the early formation of a platinum monolayer is provided by Scanning Transmission Electron Microscopy and Energy Dispersive X-rays Spectroscopy (STEM-EDX) and X-ray Photoelectron Spectroscopy (XPS) analysis. The electroactivity towards the oxygen reduction reaction of the 2D deposits is also assessed, demonstrating their great potential in energy conversion devices where ultra-low loading of Pt via extended surfaces is a reliable strategy.
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title_short	Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite
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Surface-Limited Electrodeposition of Continuous Platinum Networks on Highly Ordered Pyrolytic Graphite

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