A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages
A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and...
Ausführliche Beschreibung
Autor*in: |
Cardoso Daniel R. [verfasserIn] Andrade Sobrinho Luiz G. [verfasserIn] Lima-Neto Benedito S. [verfasserIn] Franco Douglas W. [verfasserIn] |
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Englisch |
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2004 |
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In: Journal of the Brazilian Chemical Society - Sociedade Brasileira de Química, 2017, 15(2004), 2, Seite 277-281 |
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Übergeordnetes Werk: |
volume:15 ; year:2004 ; number:2 ; pages:277-281 |
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Katalog-ID: |
DOAJ044058756 |
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(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281 |
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(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281 |
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(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281 |
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(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281 |
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(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281 |
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QD1-999 A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages cachaça chromatography purge and trap dimethylsulphide GC-MS |
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A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages |
abstract |
A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. |
abstractGer |
A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. |
abstract_unstemmed |
A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. |
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|
score |
7.400075 |