A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages

A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and...
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Gespeichert in:

Autor*in:	Cardoso Daniel R. [verfasserIn] Andrade Sobrinho Luiz G. [verfasserIn] Lima-Neto Benedito S. [verfasserIn] Franco Douglas W. [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2004

Schlagwörter:	cachaça chromatography purge and trap dimethylsulphide GC-MS

Übergeordnetes Werk:	In: Journal of the Brazilian Chemical Society - Sociedade Brasileira de Química, 2017, 15(2004), 2, Seite 277-281
Übergeordnetes Werk:	volume:15 ; year:2004 ; number:2 ; pages:277-281

Links:	Link aufrufen Link aufrufen Journal toc

Katalog-ID:	DOAJ044058756

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allfields	(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281
spelling	(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281
allfields_unstemmed	(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281
allfieldsGer	(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281
allfieldsSound	(DE-627)DOAJ044058756 (DE-599)DOAJf78609a5d3904bafa20f0ef2c37f55ac DE-627 ger DE-627 rakwb eng QD1-999 Cardoso Daniel R. verfasserin aut A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum. cachaça chromatography purge and trap dimethylsulphide GC-MS Chemistry Andrade Sobrinho Luiz G. verfasserin aut Lima-Neto Benedito S. verfasserin aut Franco Douglas W. verfasserin aut In Journal of the Brazilian Chemical Society Sociedade Brasileira de Química, 2017 15(2004), 2, Seite 277-281 (DE-627)32461330X (DE-600)2028738-0 16784790 nnns volume:15 year:2004 number:2 pages:277-281 https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 kostenfrei https://doaj.org/toc/0103-5053 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2004 2 277-281
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source	In Journal of the Brazilian Chemical Society 15(2004), 2, Seite 277-281 volume:15 year:2004 number:2 pages:277-281
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callnumber-first	Q - Science
author	Cardoso Daniel R.
spellingShingle	Cardoso Daniel R. misc QD1-999 misc cachaça misc chromatography misc purge and trap misc dimethylsulphide misc GC-MS misc Chemistry A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages
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topic_title	QD1-999 A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages cachaça chromatography purge and trap dimethylsulphide GC-MS
topic	misc QD1-999 misc cachaça misc chromatography misc purge and trap misc dimethylsulphide misc GC-MS misc Chemistry
topic_unstemmed	misc QD1-999 misc cachaça misc chromatography misc purge and trap misc dimethylsulphide misc GC-MS misc Chemistry
topic_browse	misc QD1-999 misc cachaça misc chromatography misc purge and trap misc dimethylsulphide misc GC-MS misc Chemistry
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title	A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages
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title_full	A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages
author_sort	Cardoso Daniel R.
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author_browse	Cardoso Daniel R. Andrade Sobrinho Luiz G. Lima-Neto Benedito S. Franco Douglas W.
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author-letter	Cardoso Daniel R.
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title_sort	rapid and sensitive method for dimethylsulphide analysis in brazilian sugar cane sugar spirits and other distilled beverages
callnumber	QD1-999
title_auth	A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages
abstract	A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum.
abstractGer	A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum.
abstract_unstemmed	A purge and trap concentrator coupled to gas chromatography was used to quantify dimethylsulphide in distilled beverages. A very good performance was obtained using a HP-FFAP column and a mass selective detector operating in SIM mode (m/z 62): detection limit 8 x 10-9 mol L-1; good repeatability and total time of analysis 25 minutes. The method has been applied for sixty samples of alcoholic beverages (cachaças, tiquiras, grappas, whiskies, brandies, vodkas, rum and a tequila). The cachaças exhibit the highest content of dimethylsulphide (median 3.16 x 10-4 mol L-1), followed by grappa (median 1.45 x 10-4 mol L-1). The presence of dimethylsulphide was not observed in the samples of rum.
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title_short	A rapid and sensitive method for dimethylsulphide analysis in Brazilian sugar cane sugar spirits and other distilled beverages
url	https://doaj.org/article/f78609a5d3904bafa20f0ef2c37f55ac http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200019 https://doaj.org/toc/0103-5053
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