(1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate

The title compound, C17H24NO5S+·C18H13O8−, is the key intermediate during the preparation of lesatropane [systematic name (1R,3S,5R,6S)-6-acetoxy-3-(4-methylphenylsulfonyloxy)tropane], a potential antiglaucoma agent. The tertiary N atom of the tropane ring is involved in intermolecular N—H...O hydro...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Yang Lu [verfasserIn] Hong-Zhuan Chen [verfasserIn] Ya-Fang Gu [verfasserIn] Yi-Fan Xie [verfasserIn] Li-Min Yang [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2009

Übergeordnetes Werk:	In: Acta Crystallographica Section E - International Union of Crystallography, 2005, 65(2009), 5, Seite o1037-o1037
Übergeordnetes Werk:	volume:65 ; year:2009 ; number:5 ; pages:o1037-o1037

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1107/S1600536809012732

Katalog-ID:	DOAJ045464499

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allfields	10.1107/S1600536809012732 doi (DE-627)DOAJ045464499 (DE-599)DOAJca0fa8ace738460b83a0f63b4be44de4 DE-627 ger DE-627 rakwb eng QD901-999 Yang Lu verfasserin aut (1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C17H24NO5S+·C18H13O8−, is the key intermediate during the preparation of lesatropane [systematic name (1R,3S,5R,6S)-6-acetoxy-3-(4-methylphenylsulfonyloxy)tropane], a potential antiglaucoma agent. The tertiary N atom of the tropane ring is involved in intermolecular N—H...O hydrogen bonding, and the carboxylate groups are involved in intermolecular O—H...O hydrogen bonding. Crystallography Hong-Zhuan Chen verfasserin aut Ya-Fang Gu verfasserin aut Yi-Fan Xie verfasserin aut Li-Min Yang verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 65(2009), 5, Seite o1037-o1037 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:65 year:2009 number:5 pages:o1037-o1037 https://doi.org/10.1107/S1600536809012732 kostenfrei https://doaj.org/article/ca0fa8ace738460b83a0f63b4be44de4 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536809012732 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 65 2009 5 o1037-o1037
spelling	10.1107/S1600536809012732 doi (DE-627)DOAJ045464499 (DE-599)DOAJca0fa8ace738460b83a0f63b4be44de4 DE-627 ger DE-627 rakwb eng QD901-999 Yang Lu verfasserin aut (1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C17H24NO5S+·C18H13O8−, is the key intermediate during the preparation of lesatropane [systematic name (1R,3S,5R,6S)-6-acetoxy-3-(4-methylphenylsulfonyloxy)tropane], a potential antiglaucoma agent. The tertiary N atom of the tropane ring is involved in intermolecular N—H...O hydrogen bonding, and the carboxylate groups are involved in intermolecular O—H...O hydrogen bonding. Crystallography Hong-Zhuan Chen verfasserin aut Ya-Fang Gu verfasserin aut Yi-Fan Xie verfasserin aut Li-Min Yang verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 65(2009), 5, Seite o1037-o1037 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:65 year:2009 number:5 pages:o1037-o1037 https://doi.org/10.1107/S1600536809012732 kostenfrei https://doaj.org/article/ca0fa8ace738460b83a0f63b4be44de4 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536809012732 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 65 2009 5 o1037-o1037
allfields_unstemmed	10.1107/S1600536809012732 doi (DE-627)DOAJ045464499 (DE-599)DOAJca0fa8ace738460b83a0f63b4be44de4 DE-627 ger DE-627 rakwb eng QD901-999 Yang Lu verfasserin aut (1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C17H24NO5S+·C18H13O8−, is the key intermediate during the preparation of lesatropane [systematic name (1R,3S,5R,6S)-6-acetoxy-3-(4-methylphenylsulfonyloxy)tropane], a potential antiglaucoma agent. The tertiary N atom of the tropane ring is involved in intermolecular N—H...O hydrogen bonding, and the carboxylate groups are involved in intermolecular O—H...O hydrogen bonding. Crystallography Hong-Zhuan Chen verfasserin aut Ya-Fang Gu verfasserin aut Yi-Fan Xie verfasserin aut Li-Min Yang verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 65(2009), 5, Seite o1037-o1037 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:65 year:2009 number:5 pages:o1037-o1037 https://doi.org/10.1107/S1600536809012732 kostenfrei https://doaj.org/article/ca0fa8ace738460b83a0f63b4be44de4 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536809012732 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 65 2009 5 o1037-o1037
allfieldsGer	10.1107/S1600536809012732 doi (DE-627)DOAJ045464499 (DE-599)DOAJca0fa8ace738460b83a0f63b4be44de4 DE-627 ger DE-627 rakwb eng QD901-999 Yang Lu verfasserin aut (1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C17H24NO5S+·C18H13O8−, is the key intermediate during the preparation of lesatropane [systematic name (1R,3S,5R,6S)-6-acetoxy-3-(4-methylphenylsulfonyloxy)tropane], a potential antiglaucoma agent. The tertiary N atom of the tropane ring is involved in intermolecular N—H...O hydrogen bonding, and the carboxylate groups are involved in intermolecular O—H...O hydrogen bonding. Crystallography Hong-Zhuan Chen verfasserin aut Ya-Fang Gu verfasserin aut Yi-Fan Xie verfasserin aut Li-Min Yang verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 65(2009), 5, Seite o1037-o1037 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:65 year:2009 number:5 pages:o1037-o1037 https://doi.org/10.1107/S1600536809012732 kostenfrei https://doaj.org/article/ca0fa8ace738460b83a0f63b4be44de4 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536809012732 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 65 2009 5 o1037-o1037
allfieldsSound	10.1107/S1600536809012732 doi (DE-627)DOAJ045464499 (DE-599)DOAJca0fa8ace738460b83a0f63b4be44de4 DE-627 ger DE-627 rakwb eng QD901-999 Yang Lu verfasserin aut (1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compound, C17H24NO5S+·C18H13O8−, is the key intermediate during the preparation of lesatropane [systematic name (1R,3S,5R,6S)-6-acetoxy-3-(4-methylphenylsulfonyloxy)tropane], a potential antiglaucoma agent. The tertiary N atom of the tropane ring is involved in intermolecular N—H...O hydrogen bonding, and the carboxylate groups are involved in intermolecular O—H...O hydrogen bonding. Crystallography Hong-Zhuan Chen verfasserin aut Ya-Fang Gu verfasserin aut Yi-Fan Xie verfasserin aut Li-Min Yang verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 65(2009), 5, Seite o1037-o1037 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:65 year:2009 number:5 pages:o1037-o1037 https://doi.org/10.1107/S1600536809012732 kostenfrei https://doaj.org/article/ca0fa8ace738460b83a0f63b4be44de4 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536809012732 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 65 2009 5 o1037-o1037
language	English
source	In Acta Crystallographica Section E 65(2009), 5, Seite o1037-o1037 volume:65 year:2009 number:5 pages:o1037-o1037
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callnumber-first	Q - Science
author	Yang Lu
spellingShingle	Yang Lu misc QD901-999 misc Crystallography (1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate
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issn	16005368
topic_title	QD901-999 (1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate
topic	misc QD901-999 misc Crystallography
topic_unstemmed	misc QD901-999 misc Crystallography
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format_facet	Elektronische Aufsätze Aufsätze Elektronische Ressource
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title	(1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate
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title_full	(1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate
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author_browse	Yang Lu Hong-Zhuan Chen Ya-Fang Gu Yi-Fan Xie Li-Min Yang
container_volume	65
class	QD901-999
format_se	Elektronische Aufsätze
author-letter	Yang Lu
doi_str_mv	10.1107/S1600536809012732
author2-role	verfasserin
title_sort	(1r,3s,5r,6s)-6-acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2r,3r)-2,3-bis(benzoyloxy)-3-carboxypropanoate
callnumber	QD901-999
title_auth	(1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate
abstract	The title compound, C17H24NO5S+·C18H13O8−, is the key intermediate during the preparation of lesatropane [systematic name (1R,3S,5R,6S)-6-acetoxy-3-(4-methylphenylsulfonyloxy)tropane], a potential antiglaucoma agent. The tertiary N atom of the tropane ring is involved in intermolecular N—H...O hydrogen bonding, and the carboxylate groups are involved in intermolecular O—H...O hydrogen bonding.
abstractGer	The title compound, C17H24NO5S+·C18H13O8−, is the key intermediate during the preparation of lesatropane [systematic name (1R,3S,5R,6S)-6-acetoxy-3-(4-methylphenylsulfonyloxy)tropane], a potential antiglaucoma agent. The tertiary N atom of the tropane ring is involved in intermolecular N—H...O hydrogen bonding, and the carboxylate groups are involved in intermolecular O—H...O hydrogen bonding.
abstract_unstemmed	The title compound, C17H24NO5S+·C18H13O8−, is the key intermediate during the preparation of lesatropane [systematic name (1R,3S,5R,6S)-6-acetoxy-3-(4-methylphenylsulfonyloxy)tropane], a potential antiglaucoma agent. The tertiary N atom of the tropane ring is involved in intermolecular N—H...O hydrogen bonding, and the carboxylate groups are involved in intermolecular O—H...O hydrogen bonding.
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container_issue	5
title_short	(1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate
url	https://doi.org/10.1107/S1600536809012732 https://doaj.org/article/ca0fa8ace738460b83a0f63b4be44de4 http://scripts.iucr.org/cgi-bin/paper?S1600536809012732 https://doaj.org/toc/1600-5368
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author2	Hong-Zhuan Chen Ya-Fang Gu Yi-Fan Xie Li-Min Yang
author2Str	Hong-Zhuan Chen Ya-Fang Gu Yi-Fan Xie Li-Min Yang
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doi_str	10.1107/S1600536809012732
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up_date	2024-07-03T15:07:32.502Z
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(1R,3S,5R,6S)-6-Acetoxy-8-methyl-3-(p-tolylsulfonyloxy)-8-azoniabicyclo[3.2.1]octane (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate

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