Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti

A combined chemical-electrochemical oxidation method to obtain porous bioactive TiO2 films on titanium is reported. In this case, a titanium chemical pre-etching followed by the micro-arc oxidation (MAO) treatment is proposed and optimized, to obtain a high-roughness and porous surface which benefit...
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Autor*in:	Ernesto Peláez-Abellán [verfasserIn] Laís Tereza Duarte [verfasserIn] Sonia Regina Biaggio [verfasserIn] Romeu Cardozo Rocha-Filho [verfasserIn] Nerilso Bocchi [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2012

Schlagwörter:	titanium anodization anodic oxide films micro-arc oxidation porous titanium oxide titanium oxide roughness

Übergeordnetes Werk:	In: Materials Research - Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol), 2004, 15(2012), 1, Seite 159-165
Übergeordnetes Werk:	volume:15 ; year:2012 ; number:1 ; pages:159-165

Links:	Link aufrufen Link aufrufen Journal toc

Katalog-ID:	DOAJ048330426

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allfields	(DE-627)DOAJ048330426 (DE-599)DOAJ66513a244e6d4e85bd69d92e328a6426 DE-627 ger DE-627 rakwb eng TA401-492 Ernesto Peláez-Abellán verfasserin aut Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A combined chemical-electrochemical oxidation method to obtain porous bioactive TiO2 films on titanium is reported. In this case, a titanium chemical pre-etching followed by the micro-arc oxidation (MAO) treatment is proposed and optimized, to obtain a high-roughness and porous surface which benefits the titanium/bone integration. The MAO treatment at various rates (different current densities) allowed to define the influence of the oxide growth rate on the surface morphology and to design the best features for each case. Titanium samples were pre-etched using a 2% HF solution as a function of the etching time, and then anodized by the MAO treatment in a 0.5 M H3PO4 solution at current densities in the 10 to 90 mA.cm-2 range. High porosity (0.5 to 1 µm-diameter pores) and higher phosphorous content for TiO2 films were achieved by first etching the Ti sample for 180 seconds in the HF solution, and then applying current densities in the 80 to 90 mA.cm-2 range for the micro-arc oxidation process. titanium anodization anodic oxide films micro-arc oxidation porous titanium oxide titanium oxide roughness Materials of engineering and construction. Mechanics of materials Laís Tereza Duarte verfasserin aut Sonia Regina Biaggio verfasserin aut Romeu Cardozo Rocha-Filho verfasserin aut Nerilso Bocchi verfasserin aut In Materials Research Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol), 2004 15(2012), 1, Seite 159-165 (DE-627)331755718 (DE-600)2053187-4 15161439 nnns volume:15 year:2012 number:1 pages:159-165 https://doaj.org/article/66513a244e6d4e85bd69d92e328a6426 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392012000100022 kostenfrei https://doaj.org/toc/1516-1439 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2012 1 159-165
spelling	(DE-627)DOAJ048330426 (DE-599)DOAJ66513a244e6d4e85bd69d92e328a6426 DE-627 ger DE-627 rakwb eng TA401-492 Ernesto Peláez-Abellán verfasserin aut Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A combined chemical-electrochemical oxidation method to obtain porous bioactive TiO2 films on titanium is reported. In this case, a titanium chemical pre-etching followed by the micro-arc oxidation (MAO) treatment is proposed and optimized, to obtain a high-roughness and porous surface which benefits the titanium/bone integration. The MAO treatment at various rates (different current densities) allowed to define the influence of the oxide growth rate on the surface morphology and to design the best features for each case. Titanium samples were pre-etched using a 2% HF solution as a function of the etching time, and then anodized by the MAO treatment in a 0.5 M H3PO4 solution at current densities in the 10 to 90 mA.cm-2 range. High porosity (0.5 to 1 µm-diameter pores) and higher phosphorous content for TiO2 films were achieved by first etching the Ti sample for 180 seconds in the HF solution, and then applying current densities in the 80 to 90 mA.cm-2 range for the micro-arc oxidation process. titanium anodization anodic oxide films micro-arc oxidation porous titanium oxide titanium oxide roughness Materials of engineering and construction. Mechanics of materials Laís Tereza Duarte verfasserin aut Sonia Regina Biaggio verfasserin aut Romeu Cardozo Rocha-Filho verfasserin aut Nerilso Bocchi verfasserin aut In Materials Research Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol), 2004 15(2012), 1, Seite 159-165 (DE-627)331755718 (DE-600)2053187-4 15161439 nnns volume:15 year:2012 number:1 pages:159-165 https://doaj.org/article/66513a244e6d4e85bd69d92e328a6426 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392012000100022 kostenfrei https://doaj.org/toc/1516-1439 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2012 1 159-165
allfields_unstemmed	(DE-627)DOAJ048330426 (DE-599)DOAJ66513a244e6d4e85bd69d92e328a6426 DE-627 ger DE-627 rakwb eng TA401-492 Ernesto Peláez-Abellán verfasserin aut Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A combined chemical-electrochemical oxidation method to obtain porous bioactive TiO2 films on titanium is reported. In this case, a titanium chemical pre-etching followed by the micro-arc oxidation (MAO) treatment is proposed and optimized, to obtain a high-roughness and porous surface which benefits the titanium/bone integration. The MAO treatment at various rates (different current densities) allowed to define the influence of the oxide growth rate on the surface morphology and to design the best features for each case. Titanium samples were pre-etched using a 2% HF solution as a function of the etching time, and then anodized by the MAO treatment in a 0.5 M H3PO4 solution at current densities in the 10 to 90 mA.cm-2 range. High porosity (0.5 to 1 µm-diameter pores) and higher phosphorous content for TiO2 films were achieved by first etching the Ti sample for 180 seconds in the HF solution, and then applying current densities in the 80 to 90 mA.cm-2 range for the micro-arc oxidation process. titanium anodization anodic oxide films micro-arc oxidation porous titanium oxide titanium oxide roughness Materials of engineering and construction. Mechanics of materials Laís Tereza Duarte verfasserin aut Sonia Regina Biaggio verfasserin aut Romeu Cardozo Rocha-Filho verfasserin aut Nerilso Bocchi verfasserin aut In Materials Research Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol), 2004 15(2012), 1, Seite 159-165 (DE-627)331755718 (DE-600)2053187-4 15161439 nnns volume:15 year:2012 number:1 pages:159-165 https://doaj.org/article/66513a244e6d4e85bd69d92e328a6426 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392012000100022 kostenfrei https://doaj.org/toc/1516-1439 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2012 1 159-165
allfieldsGer	(DE-627)DOAJ048330426 (DE-599)DOAJ66513a244e6d4e85bd69d92e328a6426 DE-627 ger DE-627 rakwb eng TA401-492 Ernesto Peláez-Abellán verfasserin aut Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A combined chemical-electrochemical oxidation method to obtain porous bioactive TiO2 films on titanium is reported. In this case, a titanium chemical pre-etching followed by the micro-arc oxidation (MAO) treatment is proposed and optimized, to obtain a high-roughness and porous surface which benefits the titanium/bone integration. The MAO treatment at various rates (different current densities) allowed to define the influence of the oxide growth rate on the surface morphology and to design the best features for each case. Titanium samples were pre-etched using a 2% HF solution as a function of the etching time, and then anodized by the MAO treatment in a 0.5 M H3PO4 solution at current densities in the 10 to 90 mA.cm-2 range. High porosity (0.5 to 1 µm-diameter pores) and higher phosphorous content for TiO2 films were achieved by first etching the Ti sample for 180 seconds in the HF solution, and then applying current densities in the 80 to 90 mA.cm-2 range for the micro-arc oxidation process. titanium anodization anodic oxide films micro-arc oxidation porous titanium oxide titanium oxide roughness Materials of engineering and construction. Mechanics of materials Laís Tereza Duarte verfasserin aut Sonia Regina Biaggio verfasserin aut Romeu Cardozo Rocha-Filho verfasserin aut Nerilso Bocchi verfasserin aut In Materials Research Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol), 2004 15(2012), 1, Seite 159-165 (DE-627)331755718 (DE-600)2053187-4 15161439 nnns volume:15 year:2012 number:1 pages:159-165 https://doaj.org/article/66513a244e6d4e85bd69d92e328a6426 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392012000100022 kostenfrei https://doaj.org/toc/1516-1439 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2012 1 159-165
allfieldsSound	(DE-627)DOAJ048330426 (DE-599)DOAJ66513a244e6d4e85bd69d92e328a6426 DE-627 ger DE-627 rakwb eng TA401-492 Ernesto Peláez-Abellán verfasserin aut Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A combined chemical-electrochemical oxidation method to obtain porous bioactive TiO2 films on titanium is reported. In this case, a titanium chemical pre-etching followed by the micro-arc oxidation (MAO) treatment is proposed and optimized, to obtain a high-roughness and porous surface which benefits the titanium/bone integration. The MAO treatment at various rates (different current densities) allowed to define the influence of the oxide growth rate on the surface morphology and to design the best features for each case. Titanium samples were pre-etched using a 2% HF solution as a function of the etching time, and then anodized by the MAO treatment in a 0.5 M H3PO4 solution at current densities in the 10 to 90 mA.cm-2 range. High porosity (0.5 to 1 µm-diameter pores) and higher phosphorous content for TiO2 films were achieved by first etching the Ti sample for 180 seconds in the HF solution, and then applying current densities in the 80 to 90 mA.cm-2 range for the micro-arc oxidation process. titanium anodization anodic oxide films micro-arc oxidation porous titanium oxide titanium oxide roughness Materials of engineering and construction. Mechanics of materials Laís Tereza Duarte verfasserin aut Sonia Regina Biaggio verfasserin aut Romeu Cardozo Rocha-Filho verfasserin aut Nerilso Bocchi verfasserin aut In Materials Research Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol), 2004 15(2012), 1, Seite 159-165 (DE-627)331755718 (DE-600)2053187-4 15161439 nnns volume:15 year:2012 number:1 pages:159-165 https://doaj.org/article/66513a244e6d4e85bd69d92e328a6426 kostenfrei http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392012000100022 kostenfrei https://doaj.org/toc/1516-1439 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2012 1 159-165
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authorswithroles_txt_mv	Ernesto Peláez-Abellán @@aut@@ Laís Tereza Duarte @@aut@@ Sonia Regina Biaggio @@aut@@ Romeu Cardozo Rocha-Filho @@aut@@ Nerilso Bocchi @@aut@@
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callnumber-first	T - Technology
author	Ernesto Peláez-Abellán
spellingShingle	Ernesto Peláez-Abellán misc TA401-492 misc titanium anodization misc anodic oxide films misc micro-arc oxidation misc porous titanium oxide misc titanium oxide roughness misc Materials of engineering and construction. Mechanics of materials Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti
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topic_title	TA401-492 Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti titanium anodization anodic oxide films micro-arc oxidation porous titanium oxide titanium oxide roughness
topic	misc TA401-492 misc titanium anodization misc anodic oxide films misc micro-arc oxidation misc porous titanium oxide misc titanium oxide roughness misc Materials of engineering and construction. Mechanics of materials
topic_unstemmed	misc TA401-492 misc titanium anodization misc anodic oxide films misc micro-arc oxidation misc porous titanium oxide misc titanium oxide roughness misc Materials of engineering and construction. Mechanics of materials
topic_browse	misc TA401-492 misc titanium anodization misc anodic oxide films misc micro-arc oxidation misc porous titanium oxide misc titanium oxide roughness misc Materials of engineering and construction. Mechanics of materials
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title	Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti
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title_full	Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti
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author-letter	Ernesto Peláez-Abellán
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title_sort	modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp ti
callnumber	TA401-492
title_auth	Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti
abstract	A combined chemical-electrochemical oxidation method to obtain porous bioactive TiO2 films on titanium is reported. In this case, a titanium chemical pre-etching followed by the micro-arc oxidation (MAO) treatment is proposed and optimized, to obtain a high-roughness and porous surface which benefits the titanium/bone integration. The MAO treatment at various rates (different current densities) allowed to define the influence of the oxide growth rate on the surface morphology and to design the best features for each case. Titanium samples were pre-etched using a 2% HF solution as a function of the etching time, and then anodized by the MAO treatment in a 0.5 M H3PO4 solution at current densities in the 10 to 90 mA.cm-2 range. High porosity (0.5 to 1 µm-diameter pores) and higher phosphorous content for TiO2 films were achieved by first etching the Ti sample for 180 seconds in the HF solution, and then applying current densities in the 80 to 90 mA.cm-2 range for the micro-arc oxidation process.
abstractGer	A combined chemical-electrochemical oxidation method to obtain porous bioactive TiO2 films on titanium is reported. In this case, a titanium chemical pre-etching followed by the micro-arc oxidation (MAO) treatment is proposed and optimized, to obtain a high-roughness and porous surface which benefits the titanium/bone integration. The MAO treatment at various rates (different current densities) allowed to define the influence of the oxide growth rate on the surface morphology and to design the best features for each case. Titanium samples were pre-etched using a 2% HF solution as a function of the etching time, and then anodized by the MAO treatment in a 0.5 M H3PO4 solution at current densities in the 10 to 90 mA.cm-2 range. High porosity (0.5 to 1 µm-diameter pores) and higher phosphorous content for TiO2 films were achieved by first etching the Ti sample for 180 seconds in the HF solution, and then applying current densities in the 80 to 90 mA.cm-2 range for the micro-arc oxidation process.
abstract_unstemmed	A combined chemical-electrochemical oxidation method to obtain porous bioactive TiO2 films on titanium is reported. In this case, a titanium chemical pre-etching followed by the micro-arc oxidation (MAO) treatment is proposed and optimized, to obtain a high-roughness and porous surface which benefits the titanium/bone integration. The MAO treatment at various rates (different current densities) allowed to define the influence of the oxide growth rate on the surface morphology and to design the best features for each case. Titanium samples were pre-etched using a 2% HF solution as a function of the etching time, and then anodized by the MAO treatment in a 0.5 M H3PO4 solution at current densities in the 10 to 90 mA.cm-2 range. High porosity (0.5 to 1 µm-diameter pores) and higher phosphorous content for TiO2 films were achieved by first etching the Ti sample for 180 seconds in the HF solution, and then applying current densities in the 80 to 90 mA.cm-2 range for the micro-arc oxidation process.
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title_short	Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti
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Modification of the titanium oxide morphology and composition by a combined chemical-electrochemical treatment on cp Ti

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