Low temperature synthesis of NbC/C nano-composites as visible light photoactive catalyst

Abstract A facile carbothermal route was adopted to obtain niobium carbide nanoparticles (NPs) embedded in carbon network from Nb2O5 to study photocatalytic behavior. Optimization of synthesis parameters to obtain single phase NbC NPs has been successfully done. The phase identification, morphology...
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Autor*in:	Aayush Gupta [verfasserIn] Manish Mittal [verfasserIn] Mahesh Kumar Singh [verfasserIn] Steven L. Suib [verfasserIn] Om Prakash Pandey [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2018

Schlagwörter:	Multiple Oxidation States Carbon Network Niobium Carbide (NbC) Photo Catalyst Reduction Carburization

Übergeordnetes Werk:	In: Scientific Reports - Nature Portfolio, 2011, 8(2018), 1, Seite 17
Übergeordnetes Werk:	volume:8 ; year:2018 ; number:1 ; pages:17

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1038/s41598-018-31989-z

Katalog-ID:	DOAJ048448591

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author	Aayush Gupta
spellingShingle	Aayush Gupta misc Multiple Oxidation States misc Carbon Network misc Niobium Carbide (NbC) misc Photo Catalyst misc Reduction Carburization misc Medicine misc R misc Science misc Q Low temperature synthesis of NbC/C nano-composites as visible light photoactive catalyst
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topic_title	Low temperature synthesis of NbC/C nano-composites as visible light photoactive catalyst Multiple Oxidation States Carbon Network Niobium Carbide (NbC) Photo Catalyst Reduction Carburization
topic	misc Multiple Oxidation States misc Carbon Network misc Niobium Carbide (NbC) misc Photo Catalyst misc Reduction Carburization misc Medicine misc R misc Science misc Q
topic_unstemmed	misc Multiple Oxidation States misc Carbon Network misc Niobium Carbide (NbC) misc Photo Catalyst misc Reduction Carburization misc Medicine misc R misc Science misc Q
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title	Low temperature synthesis of NbC/C nano-composites as visible light photoactive catalyst
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title_full	Low temperature synthesis of NbC/C nano-composites as visible light photoactive catalyst
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title_sort	low temperature synthesis of nbc/c nano-composites as visible light photoactive catalyst
title_auth	Low temperature synthesis of NbC/C nano-composites as visible light photoactive catalyst
abstract	Abstract A facile carbothermal route was adopted to obtain niobium carbide nanoparticles (NPs) embedded in carbon network from Nb2O5 to study photocatalytic behavior. Optimization of synthesis parameters to obtain single phase NbC NPs has been successfully done. The phase identification, morphology and nature of carbon were determined with the help of X-ray diffraction, transmission electron microscopy (TEM) and Raman spectroscopy. X-ray photoelectron spectroscopy (XPS) suggested the presence of multiple oxidation states of Nb associated to NbC and NbCxOy centers on the surface of NPs. Due to the presence of NbCxOy on the surface of NPs, absorption under visible region of EM spectrum has been observed by UV-visible spectroscopy. Different organic dyes (RhB, MB and MO) were used to study the effect of holding time on the photocatalytic performance of as-synthesized samples. RhB dye was found to be the most sensitive organic molecule among all the considered dyes and degraded 78% in 120 min.
abstractGer	Abstract A facile carbothermal route was adopted to obtain niobium carbide nanoparticles (NPs) embedded in carbon network from Nb2O5 to study photocatalytic behavior. Optimization of synthesis parameters to obtain single phase NbC NPs has been successfully done. The phase identification, morphology and nature of carbon were determined with the help of X-ray diffraction, transmission electron microscopy (TEM) and Raman spectroscopy. X-ray photoelectron spectroscopy (XPS) suggested the presence of multiple oxidation states of Nb associated to NbC and NbCxOy centers on the surface of NPs. Due to the presence of NbCxOy on the surface of NPs, absorption under visible region of EM spectrum has been observed by UV-visible spectroscopy. Different organic dyes (RhB, MB and MO) were used to study the effect of holding time on the photocatalytic performance of as-synthesized samples. RhB dye was found to be the most sensitive organic molecule among all the considered dyes and degraded 78% in 120 min.
abstract_unstemmed	Abstract A facile carbothermal route was adopted to obtain niobium carbide nanoparticles (NPs) embedded in carbon network from Nb2O5 to study photocatalytic behavior. Optimization of synthesis parameters to obtain single phase NbC NPs has been successfully done. The phase identification, morphology and nature of carbon were determined with the help of X-ray diffraction, transmission electron microscopy (TEM) and Raman spectroscopy. X-ray photoelectron spectroscopy (XPS) suggested the presence of multiple oxidation states of Nb associated to NbC and NbCxOy centers on the surface of NPs. Due to the presence of NbCxOy on the surface of NPs, absorption under visible region of EM spectrum has been observed by UV-visible spectroscopy. Different organic dyes (RhB, MB and MO) were used to study the effect of holding time on the photocatalytic performance of as-synthesized samples. RhB dye was found to be the most sensitive organic molecule among all the considered dyes and degraded 78% in 120 min.
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title_short	Low temperature synthesis of NbC/C nano-composites as visible light photoactive catalyst
url	https://doi.org/10.1038/s41598-018-31989-z https://doaj.org/article/95734dc55e5c4468a074a200413ad3a3 https://doaj.org/toc/2045-2322
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Low temperature synthesis of NbC/C nano-composites as visible light photoactive catalyst

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