Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi

A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was pe...
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Autor*in:	Carlos López [verfasserIn] Manuel Pastrana [verfasserIn] Alexandra Ríos [verfasserIn] Alvaro Cogollo [verfasserIn] Adriana Pabón [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2018

Schlagwörter:	canthin-6-one Picrolemma huberi Simaroubaceae antiplasmodial activity

Übergeordnetes Werk:	In: Molecules - MDPI AG, 2003, 23(2018), 4, p 934
Übergeordnetes Werk:	volume:23 ; year:2018 ; number:4, p 934

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/molecules23040934

Katalog-ID:	DOAJ052559823

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520			\|a A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was performed on a C18 column using acetonitrile/water (90:10, v/v) with 0.1% formic acid as the mobile phase. The structural elucidation was performed via spectroscopic methods, notably 1D- and 2D-NMR, UV, IR, MS and HRMS. The antiplasmodial activity of the compounds was studied.
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allfields	10.3390/molecules23040934 doi (DE-627)DOAJ052559823 (DE-599)DOAJ0a0f1ec9deb9445e83ac83b5733090a5 DE-627 ger DE-627 rakwb eng QD241-441 Carlos López verfasserin aut Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was performed on a C18 column using acetonitrile/water (90:10, v/v) with 0.1% formic acid as the mobile phase. The structural elucidation was performed via spectroscopic methods, notably 1D- and 2D-NMR, UV, IR, MS and HRMS. The antiplasmodial activity of the compounds was studied. canthin-6-one Picrolemma huberi Simaroubaceae antiplasmodial activity Organic chemistry Manuel Pastrana verfasserin aut Alexandra Ríos verfasserin aut Alvaro Cogollo verfasserin aut Adriana Pabón verfasserin aut In Molecules MDPI AG, 2003 23(2018), 4, p 934 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:23 year:2018 number:4, p 934 https://doi.org/10.3390/molecules23040934 kostenfrei https://doaj.org/article/0a0f1ec9deb9445e83ac83b5733090a5 kostenfrei http://www.mdpi.com/1420-3049/23/4/934 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 23 2018 4, p 934
spelling	10.3390/molecules23040934 doi (DE-627)DOAJ052559823 (DE-599)DOAJ0a0f1ec9deb9445e83ac83b5733090a5 DE-627 ger DE-627 rakwb eng QD241-441 Carlos López verfasserin aut Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was performed on a C18 column using acetonitrile/water (90:10, v/v) with 0.1% formic acid as the mobile phase. The structural elucidation was performed via spectroscopic methods, notably 1D- and 2D-NMR, UV, IR, MS and HRMS. The antiplasmodial activity of the compounds was studied. canthin-6-one Picrolemma huberi Simaroubaceae antiplasmodial activity Organic chemistry Manuel Pastrana verfasserin aut Alexandra Ríos verfasserin aut Alvaro Cogollo verfasserin aut Adriana Pabón verfasserin aut In Molecules MDPI AG, 2003 23(2018), 4, p 934 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:23 year:2018 number:4, p 934 https://doi.org/10.3390/molecules23040934 kostenfrei https://doaj.org/article/0a0f1ec9deb9445e83ac83b5733090a5 kostenfrei http://www.mdpi.com/1420-3049/23/4/934 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 23 2018 4, p 934
allfields_unstemmed	10.3390/molecules23040934 doi (DE-627)DOAJ052559823 (DE-599)DOAJ0a0f1ec9deb9445e83ac83b5733090a5 DE-627 ger DE-627 rakwb eng QD241-441 Carlos López verfasserin aut Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was performed on a C18 column using acetonitrile/water (90:10, v/v) with 0.1% formic acid as the mobile phase. The structural elucidation was performed via spectroscopic methods, notably 1D- and 2D-NMR, UV, IR, MS and HRMS. The antiplasmodial activity of the compounds was studied. canthin-6-one Picrolemma huberi Simaroubaceae antiplasmodial activity Organic chemistry Manuel Pastrana verfasserin aut Alexandra Ríos verfasserin aut Alvaro Cogollo verfasserin aut Adriana Pabón verfasserin aut In Molecules MDPI AG, 2003 23(2018), 4, p 934 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:23 year:2018 number:4, p 934 https://doi.org/10.3390/molecules23040934 kostenfrei https://doaj.org/article/0a0f1ec9deb9445e83ac83b5733090a5 kostenfrei http://www.mdpi.com/1420-3049/23/4/934 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 23 2018 4, p 934
allfieldsGer	10.3390/molecules23040934 doi (DE-627)DOAJ052559823 (DE-599)DOAJ0a0f1ec9deb9445e83ac83b5733090a5 DE-627 ger DE-627 rakwb eng QD241-441 Carlos López verfasserin aut Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was performed on a C18 column using acetonitrile/water (90:10, v/v) with 0.1% formic acid as the mobile phase. The structural elucidation was performed via spectroscopic methods, notably 1D- and 2D-NMR, UV, IR, MS and HRMS. The antiplasmodial activity of the compounds was studied. canthin-6-one Picrolemma huberi Simaroubaceae antiplasmodial activity Organic chemistry Manuel Pastrana verfasserin aut Alexandra Ríos verfasserin aut Alvaro Cogollo verfasserin aut Adriana Pabón verfasserin aut In Molecules MDPI AG, 2003 23(2018), 4, p 934 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:23 year:2018 number:4, p 934 https://doi.org/10.3390/molecules23040934 kostenfrei https://doaj.org/article/0a0f1ec9deb9445e83ac83b5733090a5 kostenfrei http://www.mdpi.com/1420-3049/23/4/934 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 23 2018 4, p 934
allfieldsSound	10.3390/molecules23040934 doi (DE-627)DOAJ052559823 (DE-599)DOAJ0a0f1ec9deb9445e83ac83b5733090a5 DE-627 ger DE-627 rakwb eng QD241-441 Carlos López verfasserin aut Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was performed on a C18 column using acetonitrile/water (90:10, v/v) with 0.1% formic acid as the mobile phase. The structural elucidation was performed via spectroscopic methods, notably 1D- and 2D-NMR, UV, IR, MS and HRMS. The antiplasmodial activity of the compounds was studied. canthin-6-one Picrolemma huberi Simaroubaceae antiplasmodial activity Organic chemistry Manuel Pastrana verfasserin aut Alexandra Ríos verfasserin aut Alvaro Cogollo verfasserin aut Adriana Pabón verfasserin aut In Molecules MDPI AG, 2003 23(2018), 4, p 934 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:23 year:2018 number:4, p 934 https://doi.org/10.3390/molecules23040934 kostenfrei https://doaj.org/article/0a0f1ec9deb9445e83ac83b5733090a5 kostenfrei http://www.mdpi.com/1420-3049/23/4/934 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 23 2018 4, p 934
language	English
source	In Molecules 23(2018), 4, p 934 volume:23 year:2018 number:4, p 934
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institution	findex.gbv.de
topic_facet	canthin-6-one Picrolemma huberi Simaroubaceae antiplasmodial activity Organic chemistry
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container_title	Molecules
authorswithroles_txt_mv	Carlos López @@aut@@ Manuel Pastrana @@aut@@ Alexandra Ríos @@aut@@ Alvaro Cogollo @@aut@@ Adriana Pabón @@aut@@
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callnumber-first	Q - Science
author	Carlos López
spellingShingle	Carlos López misc QD241-441 misc canthin-6-one misc Picrolemma huberi misc Simaroubaceae misc antiplasmodial activity misc Organic chemistry Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi
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topic_title	QD241-441 Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi canthin-6-one Picrolemma huberi Simaroubaceae antiplasmodial activity
topic	misc QD241-441 misc canthin-6-one misc Picrolemma huberi misc Simaroubaceae misc antiplasmodial activity misc Organic chemistry
topic_unstemmed	misc QD241-441 misc canthin-6-one misc Picrolemma huberi misc Simaroubaceae misc antiplasmodial activity misc Organic chemistry
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title	Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi
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title_sort	huberine, a new canthin-6-one alkaloid from the bark of picrolemma huberi
callnumber	QD241-441
title_auth	Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi
abstract	A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was performed on a C18 column using acetonitrile/water (90:10, v/v) with 0.1% formic acid as the mobile phase. The structural elucidation was performed via spectroscopic methods, notably 1D- and 2D-NMR, UV, IR, MS and HRMS. The antiplasmodial activity of the compounds was studied.
abstractGer	A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was performed on a C18 column using acetonitrile/water (90:10, v/v) with 0.1% formic acid as the mobile phase. The structural elucidation was performed via spectroscopic methods, notably 1D- and 2D-NMR, UV, IR, MS and HRMS. The antiplasmodial activity of the compounds was studied.
abstract_unstemmed	A new alkaloid, Canthin-6-one, Huberine (1), together with three known compounds including 1-Hydroxy-canthin-6-one (2), Canthin-6-one (3) and stigma sterol (4), were isolated from the stem bark of Picrolemma huberi. The isolation was achieved by chromatographic techniques and the purification was performed on a C18 column using acetonitrile/water (90:10, v/v) with 0.1% formic acid as the mobile phase. The structural elucidation was performed via spectroscopic methods, notably 1D- and 2D-NMR, UV, IR, MS and HRMS. The antiplasmodial activity of the compounds was studied.
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title_short	Huberine, a New Canthin-6-One Alkaloid from the Bark of Picrolemma huberi
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