The synergetic relationship between the length and orientation of carbon nanotubes in direct spinning of high-strength carbon nanotube fibers
Floating catalytic chemical vapor deposition (FCCVD) is an attractive method for synthesizing carbon nanotube (CNT) fibers of high strength, toughness and electrical conductivity. During the process of CNT fibers synthesis, the assembly structure, such as the CNT orientation, CNT length, and the int...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Tao Zhou [verfasserIn] Yutao Niu [verfasserIn] Zhi Li [verfasserIn] Huifang Li [verfasserIn] Zhenzhong Yong [verfasserIn] Kunjie Wu [verfasserIn] Yongyi Zhang [verfasserIn] Qingwen Li [verfasserIn] |
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| Format: |
E-Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
2021 |
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| Übergeordnetes Werk: |
In: Materials & Design - Elsevier, 2019, 203(2021), Seite 109557- |
|---|---|
| Übergeordnetes Werk: |
volume:203 ; year:2021 ; pages:109557- |
| Links: |
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| DOI / URN: |
10.1016/j.matdes.2021.109557 |
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DOAJ053807537 |
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| 520 | |a Floating catalytic chemical vapor deposition (FCCVD) is an attractive method for synthesizing carbon nanotube (CNT) fibers of high strength, toughness and electrical conductivity. During the process of CNT fibers synthesis, the assembly structure, such as the CNT orientation, CNT length, and the inter-tube particle impurity inside the CNT fibers, are key factors to determine the mechanical properties of CNT fibers. However, the regulation mechanism of the assembly structure during the process of CNT fiber synthesis is still unclear. Herein, in order to obtain high-strength CNT fibers, we demonstrated the synergistic relationship between the orientation and length of CNT inside the CNT fibers during the FCCVD growth process by adjusting the winding rate (5–30 m/min) and the length of the high-temperature reaction zone (660–1060 mm). It also revealed that the particle impurities inside the fibers could greatly reduce mechanical strength of CNT fibers. By optimizing the assembly structure of CNT fibers, the stable and continuous synthesis was realized, with the specific tensile strength of 3.1 N/tex (~ 3.5 GPa) without any post-treatment process. | ||
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10.1016/j.matdes.2021.109557 doi (DE-627)DOAJ053807537 (DE-599)DOAJe34c737551604dcc9b3d11afb2a4ee76 DE-627 ger DE-627 rakwb eng TA401-492 Tao Zhou verfasserin aut The synergetic relationship between the length and orientation of carbon nanotubes in direct spinning of high-strength carbon nanotube fibers 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Floating catalytic chemical vapor deposition (FCCVD) is an attractive method for synthesizing carbon nanotube (CNT) fibers of high strength, toughness and electrical conductivity. During the process of CNT fibers synthesis, the assembly structure, such as the CNT orientation, CNT length, and the inter-tube particle impurity inside the CNT fibers, are key factors to determine the mechanical properties of CNT fibers. However, the regulation mechanism of the assembly structure during the process of CNT fiber synthesis is still unclear. Herein, in order to obtain high-strength CNT fibers, we demonstrated the synergistic relationship between the orientation and length of CNT inside the CNT fibers during the FCCVD growth process by adjusting the winding rate (5–30 m/min) and the length of the high-temperature reaction zone (660–1060 mm). It also revealed that the particle impurities inside the fibers could greatly reduce mechanical strength of CNT fibers. By optimizing the assembly structure of CNT fibers, the stable and continuous synthesis was realized, with the specific tensile strength of 3.1 N/tex (~ 3.5 GPa) without any post-treatment process. Materials of engineering and construction. Mechanics of materials Yutao Niu verfasserin aut Zhi Li verfasserin aut Huifang Li verfasserin aut Zhenzhong Yong verfasserin aut Kunjie Wu verfasserin aut Yongyi Zhang verfasserin aut Qingwen Li verfasserin aut In Materials & Design Elsevier, 2019 203(2021), Seite 109557- (DE-627)32052857X (DE-600)2015480-X 18734197 nnns volume:203 year:2021 pages:109557- https://doi.org/10.1016/j.matdes.2021.109557 kostenfrei https://doaj.org/article/e34c737551604dcc9b3d11afb2a4ee76 kostenfrei http://www.sciencedirect.com/science/article/pii/S0264127521001106 kostenfrei https://doaj.org/toc/0264-1275 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 203 2021 109557- |
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10.1016/j.matdes.2021.109557 doi (DE-627)DOAJ053807537 (DE-599)DOAJe34c737551604dcc9b3d11afb2a4ee76 DE-627 ger DE-627 rakwb eng TA401-492 Tao Zhou verfasserin aut The synergetic relationship between the length and orientation of carbon nanotubes in direct spinning of high-strength carbon nanotube fibers 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Floating catalytic chemical vapor deposition (FCCVD) is an attractive method for synthesizing carbon nanotube (CNT) fibers of high strength, toughness and electrical conductivity. During the process of CNT fibers synthesis, the assembly structure, such as the CNT orientation, CNT length, and the inter-tube particle impurity inside the CNT fibers, are key factors to determine the mechanical properties of CNT fibers. However, the regulation mechanism of the assembly structure during the process of CNT fiber synthesis is still unclear. Herein, in order to obtain high-strength CNT fibers, we demonstrated the synergistic relationship between the orientation and length of CNT inside the CNT fibers during the FCCVD growth process by adjusting the winding rate (5–30 m/min) and the length of the high-temperature reaction zone (660–1060 mm). It also revealed that the particle impurities inside the fibers could greatly reduce mechanical strength of CNT fibers. By optimizing the assembly structure of CNT fibers, the stable and continuous synthesis was realized, with the specific tensile strength of 3.1 N/tex (~ 3.5 GPa) without any post-treatment process. Materials of engineering and construction. Mechanics of materials Yutao Niu verfasserin aut Zhi Li verfasserin aut Huifang Li verfasserin aut Zhenzhong Yong verfasserin aut Kunjie Wu verfasserin aut Yongyi Zhang verfasserin aut Qingwen Li verfasserin aut In Materials & Design Elsevier, 2019 203(2021), Seite 109557- (DE-627)32052857X (DE-600)2015480-X 18734197 nnns volume:203 year:2021 pages:109557- https://doi.org/10.1016/j.matdes.2021.109557 kostenfrei https://doaj.org/article/e34c737551604dcc9b3d11afb2a4ee76 kostenfrei http://www.sciencedirect.com/science/article/pii/S0264127521001106 kostenfrei https://doaj.org/toc/0264-1275 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 203 2021 109557- |
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10.1016/j.matdes.2021.109557 doi (DE-627)DOAJ053807537 (DE-599)DOAJe34c737551604dcc9b3d11afb2a4ee76 DE-627 ger DE-627 rakwb eng TA401-492 Tao Zhou verfasserin aut The synergetic relationship between the length and orientation of carbon nanotubes in direct spinning of high-strength carbon nanotube fibers 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Floating catalytic chemical vapor deposition (FCCVD) is an attractive method for synthesizing carbon nanotube (CNT) fibers of high strength, toughness and electrical conductivity. During the process of CNT fibers synthesis, the assembly structure, such as the CNT orientation, CNT length, and the inter-tube particle impurity inside the CNT fibers, are key factors to determine the mechanical properties of CNT fibers. However, the regulation mechanism of the assembly structure during the process of CNT fiber synthesis is still unclear. Herein, in order to obtain high-strength CNT fibers, we demonstrated the synergistic relationship between the orientation and length of CNT inside the CNT fibers during the FCCVD growth process by adjusting the winding rate (5–30 m/min) and the length of the high-temperature reaction zone (660–1060 mm). It also revealed that the particle impurities inside the fibers could greatly reduce mechanical strength of CNT fibers. By optimizing the assembly structure of CNT fibers, the stable and continuous synthesis was realized, with the specific tensile strength of 3.1 N/tex (~ 3.5 GPa) without any post-treatment process. Materials of engineering and construction. Mechanics of materials Yutao Niu verfasserin aut Zhi Li verfasserin aut Huifang Li verfasserin aut Zhenzhong Yong verfasserin aut Kunjie Wu verfasserin aut Yongyi Zhang verfasserin aut Qingwen Li verfasserin aut In Materials & Design Elsevier, 2019 203(2021), Seite 109557- (DE-627)32052857X (DE-600)2015480-X 18734197 nnns volume:203 year:2021 pages:109557- https://doi.org/10.1016/j.matdes.2021.109557 kostenfrei https://doaj.org/article/e34c737551604dcc9b3d11afb2a4ee76 kostenfrei http://www.sciencedirect.com/science/article/pii/S0264127521001106 kostenfrei https://doaj.org/toc/0264-1275 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 203 2021 109557- |
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10.1016/j.matdes.2021.109557 doi (DE-627)DOAJ053807537 (DE-599)DOAJe34c737551604dcc9b3d11afb2a4ee76 DE-627 ger DE-627 rakwb eng TA401-492 Tao Zhou verfasserin aut The synergetic relationship between the length and orientation of carbon nanotubes in direct spinning of high-strength carbon nanotube fibers 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Floating catalytic chemical vapor deposition (FCCVD) is an attractive method for synthesizing carbon nanotube (CNT) fibers of high strength, toughness and electrical conductivity. During the process of CNT fibers synthesis, the assembly structure, such as the CNT orientation, CNT length, and the inter-tube particle impurity inside the CNT fibers, are key factors to determine the mechanical properties of CNT fibers. However, the regulation mechanism of the assembly structure during the process of CNT fiber synthesis is still unclear. Herein, in order to obtain high-strength CNT fibers, we demonstrated the synergistic relationship between the orientation and length of CNT inside the CNT fibers during the FCCVD growth process by adjusting the winding rate (5–30 m/min) and the length of the high-temperature reaction zone (660–1060 mm). It also revealed that the particle impurities inside the fibers could greatly reduce mechanical strength of CNT fibers. By optimizing the assembly structure of CNT fibers, the stable and continuous synthesis was realized, with the specific tensile strength of 3.1 N/tex (~ 3.5 GPa) without any post-treatment process. Materials of engineering and construction. Mechanics of materials Yutao Niu verfasserin aut Zhi Li verfasserin aut Huifang Li verfasserin aut Zhenzhong Yong verfasserin aut Kunjie Wu verfasserin aut Yongyi Zhang verfasserin aut Qingwen Li verfasserin aut In Materials & Design Elsevier, 2019 203(2021), Seite 109557- (DE-627)32052857X (DE-600)2015480-X 18734197 nnns volume:203 year:2021 pages:109557- https://doi.org/10.1016/j.matdes.2021.109557 kostenfrei https://doaj.org/article/e34c737551604dcc9b3d11afb2a4ee76 kostenfrei http://www.sciencedirect.com/science/article/pii/S0264127521001106 kostenfrei https://doaj.org/toc/0264-1275 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_165 GBV_ILN_170 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 203 2021 109557- |
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synergetic relationship between the length and orientation of carbon nanotubes in direct spinning of high-strength carbon nanotube fibers |
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The synergetic relationship between the length and orientation of carbon nanotubes in direct spinning of high-strength carbon nanotube fibers |
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Floating catalytic chemical vapor deposition (FCCVD) is an attractive method for synthesizing carbon nanotube (CNT) fibers of high strength, toughness and electrical conductivity. During the process of CNT fibers synthesis, the assembly structure, such as the CNT orientation, CNT length, and the inter-tube particle impurity inside the CNT fibers, are key factors to determine the mechanical properties of CNT fibers. However, the regulation mechanism of the assembly structure during the process of CNT fiber synthesis is still unclear. Herein, in order to obtain high-strength CNT fibers, we demonstrated the synergistic relationship between the orientation and length of CNT inside the CNT fibers during the FCCVD growth process by adjusting the winding rate (5–30 m/min) and the length of the high-temperature reaction zone (660–1060 mm). It also revealed that the particle impurities inside the fibers could greatly reduce mechanical strength of CNT fibers. By optimizing the assembly structure of CNT fibers, the stable and continuous synthesis was realized, with the specific tensile strength of 3.1 N/tex (~ 3.5 GPa) without any post-treatment process. |
| abstractGer |
Floating catalytic chemical vapor deposition (FCCVD) is an attractive method for synthesizing carbon nanotube (CNT) fibers of high strength, toughness and electrical conductivity. During the process of CNT fibers synthesis, the assembly structure, such as the CNT orientation, CNT length, and the inter-tube particle impurity inside the CNT fibers, are key factors to determine the mechanical properties of CNT fibers. However, the regulation mechanism of the assembly structure during the process of CNT fiber synthesis is still unclear. Herein, in order to obtain high-strength CNT fibers, we demonstrated the synergistic relationship between the orientation and length of CNT inside the CNT fibers during the FCCVD growth process by adjusting the winding rate (5–30 m/min) and the length of the high-temperature reaction zone (660–1060 mm). It also revealed that the particle impurities inside the fibers could greatly reduce mechanical strength of CNT fibers. By optimizing the assembly structure of CNT fibers, the stable and continuous synthesis was realized, with the specific tensile strength of 3.1 N/tex (~ 3.5 GPa) without any post-treatment process. |
| abstract_unstemmed |
Floating catalytic chemical vapor deposition (FCCVD) is an attractive method for synthesizing carbon nanotube (CNT) fibers of high strength, toughness and electrical conductivity. During the process of CNT fibers synthesis, the assembly structure, such as the CNT orientation, CNT length, and the inter-tube particle impurity inside the CNT fibers, are key factors to determine the mechanical properties of CNT fibers. However, the regulation mechanism of the assembly structure during the process of CNT fiber synthesis is still unclear. Herein, in order to obtain high-strength CNT fibers, we demonstrated the synergistic relationship between the orientation and length of CNT inside the CNT fibers during the FCCVD growth process by adjusting the winding rate (5–30 m/min) and the length of the high-temperature reaction zone (660–1060 mm). It also revealed that the particle impurities inside the fibers could greatly reduce mechanical strength of CNT fibers. By optimizing the assembly structure of CNT fibers, the stable and continuous synthesis was realized, with the specific tensile strength of 3.1 N/tex (~ 3.5 GPa) without any post-treatment process. |
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The synergetic relationship between the length and orientation of carbon nanotubes in direct spinning of high-strength carbon nanotube fibers |
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