Investigating the effect of surface modification on the dispersion process of polymer nanocomposites

Achieving controlled nanoparticle dispersion through melt processing has been challenging as processing-structure rules for polymer nanocomposites are still not well-defined. This work focuses on developing a quantitative understanding of the filler–matrix compatibility and melt mixing parameters on...
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Autor*in:	Aditya Shanker Prasad [verfasserIn] Yixing Wang [verfasserIn] Xiaolin Li [verfasserIn] Akshay Iyer [verfasserIn] Wei Chen [verfasserIn] L. Catherine Brinson [verfasserIn] Linda S. Schadler [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2020

Schlagwörter:	polymer nanocomposites nanoparticle dispersion tem imaging image analysis surface modification

Übergeordnetes Werk:	In: Nanocomposites - Taylor & Francis Group, 2017, 6(2020), 3, Seite 111-124
Übergeordnetes Werk:	volume:6 ; year:2020 ; number:3 ; pages:111-124

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1080/20550324.2020.1809250

Katalog-ID:	DOAJ059696982

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520			\|a Achieving controlled nanoparticle dispersion through melt processing has been challenging as processing-structure rules for polymer nanocomposites are still not well-defined. This work focuses on developing a quantitative understanding of the filler–matrix compatibility and melt mixing parameters on the dispersion of nanoparticles. Filler-matrix compatibility was varied by surface modification of silica nanoparticles. A twin screw extruder was used to prepare the nanocomposites and TEM imaging and image analysis were used to quantitively characterize the microstructure. It was found that matrix–filler compatibility strongly affected the method of agglomerate breakdown and dispersion. Under similar conditions, compatible systems tended to disperse via rupture of agglomerates while incompatible systems were found to disperse via erosion. A map was created to predict the dispersion mechanism as a function of processing conditions and system compatibility and systems from this study and literature were found to be in good agreement with the map.
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language	English
source	In Nanocomposites 6(2020), 3, Seite 111-124 volume:6 year:2020 number:3 pages:111-124
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format_phy_str_mv	Article
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topic_facet	polymer nanocomposites nanoparticle dispersion tem imaging image analysis surface modification Materials of engineering and construction. Mechanics of materials Polymers and polymer manufacture
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container_title	Nanocomposites
authorswithroles_txt_mv	Aditya Shanker Prasad @@aut@@ Yixing Wang @@aut@@ Xiaolin Li @@aut@@ Akshay Iyer @@aut@@ Wei Chen @@aut@@ L. Catherine Brinson @@aut@@ Linda S. Schadler @@aut@@
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callnumber-first	T - Technology
author	Aditya Shanker Prasad
spellingShingle	Aditya Shanker Prasad misc TA401-492 misc TP1080-1185 misc polymer nanocomposites misc nanoparticle dispersion misc tem imaging misc image analysis misc surface modification misc Materials of engineering and construction. Mechanics of materials misc Polymers and polymer manufacture Investigating the effect of surface modification on the dispersion process of polymer nanocomposites
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topic_title	TA401-492 TP1080-1185 Investigating the effect of surface modification on the dispersion process of polymer nanocomposites polymer nanocomposites nanoparticle dispersion tem imaging image analysis surface modification
topic	misc TA401-492 misc TP1080-1185 misc polymer nanocomposites misc nanoparticle dispersion misc tem imaging misc image analysis misc surface modification misc Materials of engineering and construction. Mechanics of materials misc Polymers and polymer manufacture
topic_unstemmed	misc TA401-492 misc TP1080-1185 misc polymer nanocomposites misc nanoparticle dispersion misc tem imaging misc image analysis misc surface modification misc Materials of engineering and construction. Mechanics of materials misc Polymers and polymer manufacture
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title	Investigating the effect of surface modification on the dispersion process of polymer nanocomposites
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title_full	Investigating the effect of surface modification on the dispersion process of polymer nanocomposites
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title_sort	investigating the effect of surface modification on the dispersion process of polymer nanocomposites
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title_auth	Investigating the effect of surface modification on the dispersion process of polymer nanocomposites
abstract	Achieving controlled nanoparticle dispersion through melt processing has been challenging as processing-structure rules for polymer nanocomposites are still not well-defined. This work focuses on developing a quantitative understanding of the filler–matrix compatibility and melt mixing parameters on the dispersion of nanoparticles. Filler-matrix compatibility was varied by surface modification of silica nanoparticles. A twin screw extruder was used to prepare the nanocomposites and TEM imaging and image analysis were used to quantitively characterize the microstructure. It was found that matrix–filler compatibility strongly affected the method of agglomerate breakdown and dispersion. Under similar conditions, compatible systems tended to disperse via rupture of agglomerates while incompatible systems were found to disperse via erosion. A map was created to predict the dispersion mechanism as a function of processing conditions and system compatibility and systems from this study and literature were found to be in good agreement with the map.
abstractGer	Achieving controlled nanoparticle dispersion through melt processing has been challenging as processing-structure rules for polymer nanocomposites are still not well-defined. This work focuses on developing a quantitative understanding of the filler–matrix compatibility and melt mixing parameters on the dispersion of nanoparticles. Filler-matrix compatibility was varied by surface modification of silica nanoparticles. A twin screw extruder was used to prepare the nanocomposites and TEM imaging and image analysis were used to quantitively characterize the microstructure. It was found that matrix–filler compatibility strongly affected the method of agglomerate breakdown and dispersion. Under similar conditions, compatible systems tended to disperse via rupture of agglomerates while incompatible systems were found to disperse via erosion. A map was created to predict the dispersion mechanism as a function of processing conditions and system compatibility and systems from this study and literature were found to be in good agreement with the map.
abstract_unstemmed	Achieving controlled nanoparticle dispersion through melt processing has been challenging as processing-structure rules for polymer nanocomposites are still not well-defined. This work focuses on developing a quantitative understanding of the filler–matrix compatibility and melt mixing parameters on the dispersion of nanoparticles. Filler-matrix compatibility was varied by surface modification of silica nanoparticles. A twin screw extruder was used to prepare the nanocomposites and TEM imaging and image analysis were used to quantitively characterize the microstructure. It was found that matrix–filler compatibility strongly affected the method of agglomerate breakdown and dispersion. Under similar conditions, compatible systems tended to disperse via rupture of agglomerates while incompatible systems were found to disperse via erosion. A map was created to predict the dispersion mechanism as a function of processing conditions and system compatibility and systems from this study and literature were found to be in good agreement with the map.
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title_short	Investigating the effect of surface modification on the dispersion process of polymer nanocomposites
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Investigating the effect of surface modification on the dispersion process of polymer nanocomposites

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