Synthesis, spectral, antimicrobial, and antifertility studies of tetraaza macrocyclic complexes of tin(II)
A novel family of tetraazamacrocyclic complexes of Sn(II) has been synthesized by template condensation using 1,9-diaminononane with different dicarboxylic acids (malonic, succinic, glutaric, and adipic). The complexes were characterized by elemental analysis, conductivity measurements, molecular we...
Ausführliche Beschreibung
Autor*in: |
Bansal Nidhi [verfasserIn] Dave Saurabh [verfasserIn] |
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E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2013 |
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Übergeordnetes Werk: |
In: Main Group Metal Chemistry - De Gruyter, 2019, 36(2013), 3-4, Seite 101-107 |
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Übergeordnetes Werk: |
volume:36 ; year:2013 ; number:3-4 ; pages:101-107 |
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Link aufrufen |
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DOI / URN: |
10.1515/mgmc-2012-0074 |
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Katalog-ID: |
DOAJ060365188 |
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10.1515/mgmc-2012-0074 doi (DE-627)DOAJ060365188 (DE-599)DOAJaef93a256cf74784a149461ceb1cec7e DE-627 ger DE-627 rakwb eng QD1-999 Bansal Nidhi verfasserin aut Synthesis, spectral, antimicrobial, and antifertility studies of tetraaza macrocyclic complexes of tin(II) 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A novel family of tetraazamacrocyclic complexes of Sn(II) has been synthesized by template condensation using 1,9-diaminononane with different dicarboxylic acids (malonic, succinic, glutaric, and adipic). The complexes were characterized by elemental analysis, conductivity measurements, molecular weight determinations, infrared (IR), proton nuclear magnetic resonance (1H NMR), carbon nuclear magnetic resonance (13C NMR), and tin nuclear magnetic resonance (119Sn NMR) spectral studies. The compounds were found to be monomeric in nature, having an octahedral geometry. The in vitro antibacterial activity of macrocyclic complexes against Escherichia coli and Staphylococcus aureus were tested to assess their inhibiting activities. The antifungal activity of starting materials and their metal complexes were studied by screening the compounds against Fusarium oxysporum and Aspergillus niger. The testicular sperm density, sperm morphology, sperm motility, density of cauda epididymis, spermatozoa, and fertility in mating trials and the biochemical parameters of the reproductive organs of the rats were examined and are discussed. antibacterial activity macrocyclic complexes monomeric octahedral geometry Chemistry Dave Saurabh verfasserin aut In Main Group Metal Chemistry De Gruyter, 2019 36(2013), 3-4, Seite 101-107 (DE-627)656019840 (DE-600)2602433-0 21910219 nnns volume:36 year:2013 number:3-4 pages:101-107 https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/article/aef93a256cf74784a149461ceb1cec7e kostenfrei https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/toc/0792-1241 Journal toc kostenfrei https://doaj.org/toc/2191-0219 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_121 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_187 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_374 GBV_ILN_602 GBV_ILN_636 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2014 GBV_ILN_2891 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 36 2013 3-4 101-107 |
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10.1515/mgmc-2012-0074 doi (DE-627)DOAJ060365188 (DE-599)DOAJaef93a256cf74784a149461ceb1cec7e DE-627 ger DE-627 rakwb eng QD1-999 Bansal Nidhi verfasserin aut Synthesis, spectral, antimicrobial, and antifertility studies of tetraaza macrocyclic complexes of tin(II) 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A novel family of tetraazamacrocyclic complexes of Sn(II) has been synthesized by template condensation using 1,9-diaminononane with different dicarboxylic acids (malonic, succinic, glutaric, and adipic). The complexes were characterized by elemental analysis, conductivity measurements, molecular weight determinations, infrared (IR), proton nuclear magnetic resonance (1H NMR), carbon nuclear magnetic resonance (13C NMR), and tin nuclear magnetic resonance (119Sn NMR) spectral studies. The compounds were found to be monomeric in nature, having an octahedral geometry. The in vitro antibacterial activity of macrocyclic complexes against Escherichia coli and Staphylococcus aureus were tested to assess their inhibiting activities. The antifungal activity of starting materials and their metal complexes were studied by screening the compounds against Fusarium oxysporum and Aspergillus niger. The testicular sperm density, sperm morphology, sperm motility, density of cauda epididymis, spermatozoa, and fertility in mating trials and the biochemical parameters of the reproductive organs of the rats were examined and are discussed. antibacterial activity macrocyclic complexes monomeric octahedral geometry Chemistry Dave Saurabh verfasserin aut In Main Group Metal Chemistry De Gruyter, 2019 36(2013), 3-4, Seite 101-107 (DE-627)656019840 (DE-600)2602433-0 21910219 nnns volume:36 year:2013 number:3-4 pages:101-107 https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/article/aef93a256cf74784a149461ceb1cec7e kostenfrei https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/toc/0792-1241 Journal toc kostenfrei https://doaj.org/toc/2191-0219 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_121 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_187 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_374 GBV_ILN_602 GBV_ILN_636 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2014 GBV_ILN_2891 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 36 2013 3-4 101-107 |
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10.1515/mgmc-2012-0074 doi (DE-627)DOAJ060365188 (DE-599)DOAJaef93a256cf74784a149461ceb1cec7e DE-627 ger DE-627 rakwb eng QD1-999 Bansal Nidhi verfasserin aut Synthesis, spectral, antimicrobial, and antifertility studies of tetraaza macrocyclic complexes of tin(II) 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A novel family of tetraazamacrocyclic complexes of Sn(II) has been synthesized by template condensation using 1,9-diaminononane with different dicarboxylic acids (malonic, succinic, glutaric, and adipic). The complexes were characterized by elemental analysis, conductivity measurements, molecular weight determinations, infrared (IR), proton nuclear magnetic resonance (1H NMR), carbon nuclear magnetic resonance (13C NMR), and tin nuclear magnetic resonance (119Sn NMR) spectral studies. The compounds were found to be monomeric in nature, having an octahedral geometry. The in vitro antibacterial activity of macrocyclic complexes against Escherichia coli and Staphylococcus aureus were tested to assess their inhibiting activities. The antifungal activity of starting materials and their metal complexes were studied by screening the compounds against Fusarium oxysporum and Aspergillus niger. The testicular sperm density, sperm morphology, sperm motility, density of cauda epididymis, spermatozoa, and fertility in mating trials and the biochemical parameters of the reproductive organs of the rats were examined and are discussed. antibacterial activity macrocyclic complexes monomeric octahedral geometry Chemistry Dave Saurabh verfasserin aut In Main Group Metal Chemistry De Gruyter, 2019 36(2013), 3-4, Seite 101-107 (DE-627)656019840 (DE-600)2602433-0 21910219 nnns volume:36 year:2013 number:3-4 pages:101-107 https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/article/aef93a256cf74784a149461ceb1cec7e kostenfrei https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/toc/0792-1241 Journal toc kostenfrei https://doaj.org/toc/2191-0219 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_121 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_187 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_374 GBV_ILN_602 GBV_ILN_636 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2014 GBV_ILN_2891 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 36 2013 3-4 101-107 |
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10.1515/mgmc-2012-0074 doi (DE-627)DOAJ060365188 (DE-599)DOAJaef93a256cf74784a149461ceb1cec7e DE-627 ger DE-627 rakwb eng QD1-999 Bansal Nidhi verfasserin aut Synthesis, spectral, antimicrobial, and antifertility studies of tetraaza macrocyclic complexes of tin(II) 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A novel family of tetraazamacrocyclic complexes of Sn(II) has been synthesized by template condensation using 1,9-diaminononane with different dicarboxylic acids (malonic, succinic, glutaric, and adipic). The complexes were characterized by elemental analysis, conductivity measurements, molecular weight determinations, infrared (IR), proton nuclear magnetic resonance (1H NMR), carbon nuclear magnetic resonance (13C NMR), and tin nuclear magnetic resonance (119Sn NMR) spectral studies. The compounds were found to be monomeric in nature, having an octahedral geometry. The in vitro antibacterial activity of macrocyclic complexes against Escherichia coli and Staphylococcus aureus were tested to assess their inhibiting activities. The antifungal activity of starting materials and their metal complexes were studied by screening the compounds against Fusarium oxysporum and Aspergillus niger. The testicular sperm density, sperm morphology, sperm motility, density of cauda epididymis, spermatozoa, and fertility in mating trials and the biochemical parameters of the reproductive organs of the rats were examined and are discussed. antibacterial activity macrocyclic complexes monomeric octahedral geometry Chemistry Dave Saurabh verfasserin aut In Main Group Metal Chemistry De Gruyter, 2019 36(2013), 3-4, Seite 101-107 (DE-627)656019840 (DE-600)2602433-0 21910219 nnns volume:36 year:2013 number:3-4 pages:101-107 https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/article/aef93a256cf74784a149461ceb1cec7e kostenfrei https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/toc/0792-1241 Journal toc kostenfrei https://doaj.org/toc/2191-0219 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_121 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_187 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_374 GBV_ILN_602 GBV_ILN_636 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2014 GBV_ILN_2891 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 36 2013 3-4 101-107 |
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10.1515/mgmc-2012-0074 doi (DE-627)DOAJ060365188 (DE-599)DOAJaef93a256cf74784a149461ceb1cec7e DE-627 ger DE-627 rakwb eng QD1-999 Bansal Nidhi verfasserin aut Synthesis, spectral, antimicrobial, and antifertility studies of tetraaza macrocyclic complexes of tin(II) 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier A novel family of tetraazamacrocyclic complexes of Sn(II) has been synthesized by template condensation using 1,9-diaminononane with different dicarboxylic acids (malonic, succinic, glutaric, and adipic). The complexes were characterized by elemental analysis, conductivity measurements, molecular weight determinations, infrared (IR), proton nuclear magnetic resonance (1H NMR), carbon nuclear magnetic resonance (13C NMR), and tin nuclear magnetic resonance (119Sn NMR) spectral studies. The compounds were found to be monomeric in nature, having an octahedral geometry. The in vitro antibacterial activity of macrocyclic complexes against Escherichia coli and Staphylococcus aureus were tested to assess their inhibiting activities. The antifungal activity of starting materials and their metal complexes were studied by screening the compounds against Fusarium oxysporum and Aspergillus niger. The testicular sperm density, sperm morphology, sperm motility, density of cauda epididymis, spermatozoa, and fertility in mating trials and the biochemical parameters of the reproductive organs of the rats were examined and are discussed. antibacterial activity macrocyclic complexes monomeric octahedral geometry Chemistry Dave Saurabh verfasserin aut In Main Group Metal Chemistry De Gruyter, 2019 36(2013), 3-4, Seite 101-107 (DE-627)656019840 (DE-600)2602433-0 21910219 nnns volume:36 year:2013 number:3-4 pages:101-107 https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/article/aef93a256cf74784a149461ceb1cec7e kostenfrei https://doi.org/10.1515/mgmc-2012-0074 kostenfrei https://doaj.org/toc/0792-1241 Journal toc kostenfrei https://doaj.org/toc/2191-0219 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_121 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_187 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_374 GBV_ILN_602 GBV_ILN_636 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2014 GBV_ILN_2891 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 36 2013 3-4 101-107 |
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Synthesis, spectral, antimicrobial, and antifertility studies of tetraaza macrocyclic complexes of tin(II) |
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A novel family of tetraazamacrocyclic complexes of Sn(II) has been synthesized by template condensation using 1,9-diaminononane with different dicarboxylic acids (malonic, succinic, glutaric, and adipic). The complexes were characterized by elemental analysis, conductivity measurements, molecular weight determinations, infrared (IR), proton nuclear magnetic resonance (1H NMR), carbon nuclear magnetic resonance (13C NMR), and tin nuclear magnetic resonance (119Sn NMR) spectral studies. The compounds were found to be monomeric in nature, having an octahedral geometry. The in vitro antibacterial activity of macrocyclic complexes against Escherichia coli and Staphylococcus aureus were tested to assess their inhibiting activities. The antifungal activity of starting materials and their metal complexes were studied by screening the compounds against Fusarium oxysporum and Aspergillus niger. The testicular sperm density, sperm morphology, sperm motility, density of cauda epididymis, spermatozoa, and fertility in mating trials and the biochemical parameters of the reproductive organs of the rats were examined and are discussed. |
abstractGer |
A novel family of tetraazamacrocyclic complexes of Sn(II) has been synthesized by template condensation using 1,9-diaminononane with different dicarboxylic acids (malonic, succinic, glutaric, and adipic). The complexes were characterized by elemental analysis, conductivity measurements, molecular weight determinations, infrared (IR), proton nuclear magnetic resonance (1H NMR), carbon nuclear magnetic resonance (13C NMR), and tin nuclear magnetic resonance (119Sn NMR) spectral studies. The compounds were found to be monomeric in nature, having an octahedral geometry. The in vitro antibacterial activity of macrocyclic complexes against Escherichia coli and Staphylococcus aureus were tested to assess their inhibiting activities. The antifungal activity of starting materials and their metal complexes were studied by screening the compounds against Fusarium oxysporum and Aspergillus niger. The testicular sperm density, sperm morphology, sperm motility, density of cauda epididymis, spermatozoa, and fertility in mating trials and the biochemical parameters of the reproductive organs of the rats were examined and are discussed. |
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A novel family of tetraazamacrocyclic complexes of Sn(II) has been synthesized by template condensation using 1,9-diaminononane with different dicarboxylic acids (malonic, succinic, glutaric, and adipic). The complexes were characterized by elemental analysis, conductivity measurements, molecular weight determinations, infrared (IR), proton nuclear magnetic resonance (1H NMR), carbon nuclear magnetic resonance (13C NMR), and tin nuclear magnetic resonance (119Sn NMR) spectral studies. The compounds were found to be monomeric in nature, having an octahedral geometry. The in vitro antibacterial activity of macrocyclic complexes against Escherichia coli and Staphylococcus aureus were tested to assess their inhibiting activities. The antifungal activity of starting materials and their metal complexes were studied by screening the compounds against Fusarium oxysporum and Aspergillus niger. The testicular sperm density, sperm morphology, sperm motility, density of cauda epididymis, spermatozoa, and fertility in mating trials and the biochemical parameters of the reproductive organs of the rats were examined and are discussed. |
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