Fast and Green Microwave-Assisted Conversion of Essential Oil Allylbenzenes into the Corresponding Aldehydes via Alkene Isomerization and Subsequent Potassium Permanganate Promoted Oxidative Alkene Group Cleavage

Essential oil allylbenzenes from have been converted quickly and efficiently into the corresponding benzaldehydes in good yields by a two-step “green” reaction pathway based on a solventless alkene group isomerization by KF/Al2O3 to form the corresponding 1-arylpropene and a subsequent solventless o...
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Autor*in:	Thi X. Thi Luu [verfasserIn] Trinh To Lam [verfasserIn] Thach Ngoc Le [verfasserIn] Fritz Duus [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2009

Schlagwörter:	microwave irradiation solvent-free reaction alkene isomerization alkene oxidation

Übergeordnetes Werk:	In: Molecules - MDPI AG, 2003, 14(2009), 9, Seite 3411-3424
Übergeordnetes Werk:	volume:14 ; year:2009 ; number:9 ; pages:3411-3424

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/molecules14093411

Katalog-ID:	DOAJ064686272

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520			\|a Essential oil allylbenzenes from have been converted quickly and efficiently into the corresponding benzaldehydes in good yields by a two-step “green” reaction pathway based on a solventless alkene group isomerization by KF/Al2O3 to form the corresponding 1-arylpropene and a subsequent solventless oxidation of the latter to the corresponding benzaldehyde by KMnO4/CuSO4·5H2O. The assistance by microwave irradiation results in very short reaction times (<15 minutes). The green conversion of eugenol (4-allyl-2-methoxyphenol) into vanillin (4-hydroxy-3-methoxybenzaldehyde) has been carried out in a similar way, requiring however two additional microwave-assisted synthetic steps for acetylation of the hydroxy group prior to the oxidation reaction, and for the final deacetylation of vanillin acetate (4-acetoxy-3-methoxybenzaldehyde) by KF/Al2O3 under solvent-free conditions, respectively.
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source	In Molecules 14(2009), 9, Seite 3411-3424 volume:14 year:2009 number:9 pages:3411-3424
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topic_facet	microwave irradiation solvent-free reaction alkene isomerization alkene oxidation Organic chemistry
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callnumber-first	Q - Science
author	Thi X. Thi Luu
spellingShingle	Thi X. Thi Luu misc QD241-441 misc microwave irradiation misc solvent-free reaction misc alkene isomerization misc alkene oxidation misc Organic chemistry Fast and Green Microwave-Assisted Conversion of Essential Oil Allylbenzenes into the Corresponding Aldehydes via Alkene Isomerization and Subsequent Potassium Permanganate Promoted Oxidative Alkene Group Cleavage
authorStr	Thi X. Thi Luu
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topic_title	QD241-441 Fast and Green Microwave-Assisted Conversion of Essential Oil Allylbenzenes into the Corresponding Aldehydes via Alkene Isomerization and Subsequent Potassium Permanganate Promoted Oxidative Alkene Group Cleavage microwave irradiation solvent-free reaction alkene isomerization alkene oxidation
topic	misc QD241-441 misc microwave irradiation misc solvent-free reaction misc alkene isomerization misc alkene oxidation misc Organic chemistry
topic_unstemmed	misc QD241-441 misc microwave irradiation misc solvent-free reaction misc alkene isomerization misc alkene oxidation misc Organic chemistry
topic_browse	misc QD241-441 misc microwave irradiation misc solvent-free reaction misc alkene isomerization misc alkene oxidation misc Organic chemistry
format_facet	Elektronische Aufsätze Aufsätze Elektronische Ressource
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title	Fast and Green Microwave-Assisted Conversion of Essential Oil Allylbenzenes into the Corresponding Aldehydes via Alkene Isomerization and Subsequent Potassium Permanganate Promoted Oxidative Alkene Group Cleavage
ctrlnum	(DE-627)DOAJ064686272 (DE-599)DOAJbd492d48f60a44b68ee9f1f81cd8988d
title_full	Fast and Green Microwave-Assisted Conversion of Essential Oil Allylbenzenes into the Corresponding Aldehydes via Alkene Isomerization and Subsequent Potassium Permanganate Promoted Oxidative Alkene Group Cleavage
author_sort	Thi X. Thi Luu
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author_browse	Thi X. Thi Luu Trinh To Lam Thach Ngoc Le Fritz Duus
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author-letter	Thi X. Thi Luu
doi_str_mv	10.3390/molecules14093411
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title_sort	fast and green microwave-assisted conversion of essential oil allylbenzenes into the corresponding aldehydes via alkene isomerization and subsequent potassium permanganate promoted oxidative alkene group cleavage
callnumber	QD241-441
title_auth	Fast and Green Microwave-Assisted Conversion of Essential Oil Allylbenzenes into the Corresponding Aldehydes via Alkene Isomerization and Subsequent Potassium Permanganate Promoted Oxidative Alkene Group Cleavage
abstract	Essential oil allylbenzenes from have been converted quickly and efficiently into the corresponding benzaldehydes in good yields by a two-step “green” reaction pathway based on a solventless alkene group isomerization by KF/Al2O3 to form the corresponding 1-arylpropene and a subsequent solventless oxidation of the latter to the corresponding benzaldehyde by KMnO4/CuSO4·5H2O. The assistance by microwave irradiation results in very short reaction times (<15 minutes). The green conversion of eugenol (4-allyl-2-methoxyphenol) into vanillin (4-hydroxy-3-methoxybenzaldehyde) has been carried out in a similar way, requiring however two additional microwave-assisted synthetic steps for acetylation of the hydroxy group prior to the oxidation reaction, and for the final deacetylation of vanillin acetate (4-acetoxy-3-methoxybenzaldehyde) by KF/Al2O3 under solvent-free conditions, respectively.
abstractGer	Essential oil allylbenzenes from have been converted quickly and efficiently into the corresponding benzaldehydes in good yields by a two-step “green” reaction pathway based on a solventless alkene group isomerization by KF/Al2O3 to form the corresponding 1-arylpropene and a subsequent solventless oxidation of the latter to the corresponding benzaldehyde by KMnO4/CuSO4·5H2O. The assistance by microwave irradiation results in very short reaction times (<15 minutes). The green conversion of eugenol (4-allyl-2-methoxyphenol) into vanillin (4-hydroxy-3-methoxybenzaldehyde) has been carried out in a similar way, requiring however two additional microwave-assisted synthetic steps for acetylation of the hydroxy group prior to the oxidation reaction, and for the final deacetylation of vanillin acetate (4-acetoxy-3-methoxybenzaldehyde) by KF/Al2O3 under solvent-free conditions, respectively.
abstract_unstemmed	Essential oil allylbenzenes from have been converted quickly and efficiently into the corresponding benzaldehydes in good yields by a two-step “green” reaction pathway based on a solventless alkene group isomerization by KF/Al2O3 to form the corresponding 1-arylpropene and a subsequent solventless oxidation of the latter to the corresponding benzaldehyde by KMnO4/CuSO4·5H2O. The assistance by microwave irradiation results in very short reaction times (<15 minutes). The green conversion of eugenol (4-allyl-2-methoxyphenol) into vanillin (4-hydroxy-3-methoxybenzaldehyde) has been carried out in a similar way, requiring however two additional microwave-assisted synthetic steps for acetylation of the hydroxy group prior to the oxidation reaction, and for the final deacetylation of vanillin acetate (4-acetoxy-3-methoxybenzaldehyde) by KF/Al2O3 under solvent-free conditions, respectively.
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container_issue	9
title_short	Fast and Green Microwave-Assisted Conversion of Essential Oil Allylbenzenes into the Corresponding Aldehydes via Alkene Isomerization and Subsequent Potassium Permanganate Promoted Oxidative Alkene Group Cleavage
url	https://doi.org/10.3390/molecules14093411 https://doaj.org/article/bd492d48f60a44b68ee9f1f81cd8988d http://www.mdpi.com/1420-3049/14/9/3411/ https://doaj.org/toc/1420-3049
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doi_str	10.3390/molecules14093411
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up_date	2024-07-03T23:58:04.020Z
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Fast and Green Microwave-Assisted Conversion of Essential Oil Allylbenzenes into the Corresponding Aldehydes via Alkene Isomerization and Subsequent Potassium Permanganate Promoted Oxidative Alkene Group Cleavage

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