Use of the Sol–Gel Method for the Preparation of Coatings of Titanium Substrates with Hydroxyapatite for Biomedical Application
Hydroxyapatite (HA) was coated onto the surface of commercially pure titanium grade 4 (a material generally used for implant application) by a dip coating method using HA sol. Hydroxyapatite sol was synthesized via sol−gel using Ca(NO<sub<3</sub<)<sub<2</sub<∙4H<sub<2&l...
Ausführliche Beschreibung
Autor*in: |
Michelina Catauro [verfasserIn] Federico Barrino [verfasserIn] Ignazio Blanco [verfasserIn] Simona Piccolella [verfasserIn] Severina Pacifico [verfasserIn] |
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E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2020 |
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Übergeordnetes Werk: |
In: Coatings - MDPI AG, 2012, 10(2020), 3, p 203 |
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Übergeordnetes Werk: |
volume:10 ; year:2020 ; number:3, p 203 |
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DOI / URN: |
10.3390/coatings10030203 |
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Katalog-ID: |
DOAJ068839766 |
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10.3390/coatings10030203 doi (DE-627)DOAJ068839766 (DE-599)DOAJd666516f20544f5290d519adad23c7e9 DE-627 ger DE-627 rakwb eng TA1-2040 Michelina Catauro verfasserin aut Use of the Sol–Gel Method for the Preparation of Coatings of Titanium Substrates with Hydroxyapatite for Biomedical Application 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Hydroxyapatite (HA) was coated onto the surface of commercially pure titanium grade 4 (a material generally used for implant application) by a dip coating method using HA sol. Hydroxyapatite sol was synthesized via sol−gel using Ca(NO<sub<3</sub<)<sub<2</sub<∙4H<sub<2</sub<O and P<sub<2</sub<O<sub<5</sub< as precursors. The surface of the HA coating was homogeneous, as determined by scanning electron microscopy (SEM), attenuated total reflectance Fourier transform infrared (ATR-FTIR), and X-ray diffraction (XRD), which allowed the materials to be characterized. The bioactivity of the synthesized materials and their efficiency for use as future bone implants was confirmed by observing the formation of a layer of hydroxyapatite on the surface of the samples soaked in a fluid simulating the composition of human blood plasma. To verify the biocompatibility of the obtained biomaterial, fibroblasts were grown on a glass surface and were tested for viability after 24 h. The results of the WST-8 analysis suggest that the HA systems, prepared by the sol−gel method, are most suitable for modifying the surface of titanium implants and improving their biocompatibility. sol–gel synthesis hydroxyapatite titanium substrate coating biocompatibility Engineering (General). Civil engineering (General) Federico Barrino verfasserin aut Ignazio Blanco verfasserin aut Simona Piccolella verfasserin aut Severina Pacifico verfasserin aut In Coatings MDPI AG, 2012 10(2020), 3, p 203 (DE-627)718627636 (DE-600)2662314-6 20796412 nnns volume:10 year:2020 number:3, p 203 https://doi.org/10.3390/coatings10030203 kostenfrei https://doaj.org/article/d666516f20544f5290d519adad23c7e9 kostenfrei https://www.mdpi.com/2079-6412/10/3/203 kostenfrei https://doaj.org/toc/2079-6412 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 10 2020 3, p 203 |
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10.3390/coatings10030203 doi (DE-627)DOAJ068839766 (DE-599)DOAJd666516f20544f5290d519adad23c7e9 DE-627 ger DE-627 rakwb eng TA1-2040 Michelina Catauro verfasserin aut Use of the Sol–Gel Method for the Preparation of Coatings of Titanium Substrates with Hydroxyapatite for Biomedical Application 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Hydroxyapatite (HA) was coated onto the surface of commercially pure titanium grade 4 (a material generally used for implant application) by a dip coating method using HA sol. Hydroxyapatite sol was synthesized via sol−gel using Ca(NO<sub<3</sub<)<sub<2</sub<∙4H<sub<2</sub<O and P<sub<2</sub<O<sub<5</sub< as precursors. The surface of the HA coating was homogeneous, as determined by scanning electron microscopy (SEM), attenuated total reflectance Fourier transform infrared (ATR-FTIR), and X-ray diffraction (XRD), which allowed the materials to be characterized. The bioactivity of the synthesized materials and their efficiency for use as future bone implants was confirmed by observing the formation of a layer of hydroxyapatite on the surface of the samples soaked in a fluid simulating the composition of human blood plasma. To verify the biocompatibility of the obtained biomaterial, fibroblasts were grown on a glass surface and were tested for viability after 24 h. The results of the WST-8 analysis suggest that the HA systems, prepared by the sol−gel method, are most suitable for modifying the surface of titanium implants and improving their biocompatibility. sol–gel synthesis hydroxyapatite titanium substrate coating biocompatibility Engineering (General). Civil engineering (General) Federico Barrino verfasserin aut Ignazio Blanco verfasserin aut Simona Piccolella verfasserin aut Severina Pacifico verfasserin aut In Coatings MDPI AG, 2012 10(2020), 3, p 203 (DE-627)718627636 (DE-600)2662314-6 20796412 nnns volume:10 year:2020 number:3, p 203 https://doi.org/10.3390/coatings10030203 kostenfrei https://doaj.org/article/d666516f20544f5290d519adad23c7e9 kostenfrei https://www.mdpi.com/2079-6412/10/3/203 kostenfrei https://doaj.org/toc/2079-6412 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 10 2020 3, p 203 |
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10.3390/coatings10030203 doi (DE-627)DOAJ068839766 (DE-599)DOAJd666516f20544f5290d519adad23c7e9 DE-627 ger DE-627 rakwb eng TA1-2040 Michelina Catauro verfasserin aut Use of the Sol–Gel Method for the Preparation of Coatings of Titanium Substrates with Hydroxyapatite for Biomedical Application 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Hydroxyapatite (HA) was coated onto the surface of commercially pure titanium grade 4 (a material generally used for implant application) by a dip coating method using HA sol. Hydroxyapatite sol was synthesized via sol−gel using Ca(NO<sub<3</sub<)<sub<2</sub<∙4H<sub<2</sub<O and P<sub<2</sub<O<sub<5</sub< as precursors. The surface of the HA coating was homogeneous, as determined by scanning electron microscopy (SEM), attenuated total reflectance Fourier transform infrared (ATR-FTIR), and X-ray diffraction (XRD), which allowed the materials to be characterized. The bioactivity of the synthesized materials and their efficiency for use as future bone implants was confirmed by observing the formation of a layer of hydroxyapatite on the surface of the samples soaked in a fluid simulating the composition of human blood plasma. To verify the biocompatibility of the obtained biomaterial, fibroblasts were grown on a glass surface and were tested for viability after 24 h. The results of the WST-8 analysis suggest that the HA systems, prepared by the sol−gel method, are most suitable for modifying the surface of titanium implants and improving their biocompatibility. sol–gel synthesis hydroxyapatite titanium substrate coating biocompatibility Engineering (General). Civil engineering (General) Federico Barrino verfasserin aut Ignazio Blanco verfasserin aut Simona Piccolella verfasserin aut Severina Pacifico verfasserin aut In Coatings MDPI AG, 2012 10(2020), 3, p 203 (DE-627)718627636 (DE-600)2662314-6 20796412 nnns volume:10 year:2020 number:3, p 203 https://doi.org/10.3390/coatings10030203 kostenfrei https://doaj.org/article/d666516f20544f5290d519adad23c7e9 kostenfrei https://www.mdpi.com/2079-6412/10/3/203 kostenfrei https://doaj.org/toc/2079-6412 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 10 2020 3, p 203 |
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10.3390/coatings10030203 doi (DE-627)DOAJ068839766 (DE-599)DOAJd666516f20544f5290d519adad23c7e9 DE-627 ger DE-627 rakwb eng TA1-2040 Michelina Catauro verfasserin aut Use of the Sol–Gel Method for the Preparation of Coatings of Titanium Substrates with Hydroxyapatite for Biomedical Application 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Hydroxyapatite (HA) was coated onto the surface of commercially pure titanium grade 4 (a material generally used for implant application) by a dip coating method using HA sol. Hydroxyapatite sol was synthesized via sol−gel using Ca(NO<sub<3</sub<)<sub<2</sub<∙4H<sub<2</sub<O and P<sub<2</sub<O<sub<5</sub< as precursors. The surface of the HA coating was homogeneous, as determined by scanning electron microscopy (SEM), attenuated total reflectance Fourier transform infrared (ATR-FTIR), and X-ray diffraction (XRD), which allowed the materials to be characterized. The bioactivity of the synthesized materials and their efficiency for use as future bone implants was confirmed by observing the formation of a layer of hydroxyapatite on the surface of the samples soaked in a fluid simulating the composition of human blood plasma. To verify the biocompatibility of the obtained biomaterial, fibroblasts were grown on a glass surface and were tested for viability after 24 h. The results of the WST-8 analysis suggest that the HA systems, prepared by the sol−gel method, are most suitable for modifying the surface of titanium implants and improving their biocompatibility. sol–gel synthesis hydroxyapatite titanium substrate coating biocompatibility Engineering (General). Civil engineering (General) Federico Barrino verfasserin aut Ignazio Blanco verfasserin aut Simona Piccolella verfasserin aut Severina Pacifico verfasserin aut In Coatings MDPI AG, 2012 10(2020), 3, p 203 (DE-627)718627636 (DE-600)2662314-6 20796412 nnns volume:10 year:2020 number:3, p 203 https://doi.org/10.3390/coatings10030203 kostenfrei https://doaj.org/article/d666516f20544f5290d519adad23c7e9 kostenfrei https://www.mdpi.com/2079-6412/10/3/203 kostenfrei https://doaj.org/toc/2079-6412 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 10 2020 3, p 203 |
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Michelina Catauro misc TA1-2040 misc sol–gel synthesis misc hydroxyapatite misc titanium substrate coating misc biocompatibility misc Engineering (General). Civil engineering (General) Use of the Sol–Gel Method for the Preparation of Coatings of Titanium Substrates with Hydroxyapatite for Biomedical Application |
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TA1-2040 Use of the Sol–Gel Method for the Preparation of Coatings of Titanium Substrates with Hydroxyapatite for Biomedical Application sol–gel synthesis hydroxyapatite titanium substrate coating biocompatibility |
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Use of the Sol–Gel Method for the Preparation of Coatings of Titanium Substrates with Hydroxyapatite for Biomedical Application |
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Hydroxyapatite (HA) was coated onto the surface of commercially pure titanium grade 4 (a material generally used for implant application) by a dip coating method using HA sol. Hydroxyapatite sol was synthesized via sol−gel using Ca(NO<sub<3</sub<)<sub<2</sub<∙4H<sub<2</sub<O and P<sub<2</sub<O<sub<5</sub< as precursors. The surface of the HA coating was homogeneous, as determined by scanning electron microscopy (SEM), attenuated total reflectance Fourier transform infrared (ATR-FTIR), and X-ray diffraction (XRD), which allowed the materials to be characterized. The bioactivity of the synthesized materials and their efficiency for use as future bone implants was confirmed by observing the formation of a layer of hydroxyapatite on the surface of the samples soaked in a fluid simulating the composition of human blood plasma. To verify the biocompatibility of the obtained biomaterial, fibroblasts were grown on a glass surface and were tested for viability after 24 h. The results of the WST-8 analysis suggest that the HA systems, prepared by the sol−gel method, are most suitable for modifying the surface of titanium implants and improving their biocompatibility. |
abstractGer |
Hydroxyapatite (HA) was coated onto the surface of commercially pure titanium grade 4 (a material generally used for implant application) by a dip coating method using HA sol. Hydroxyapatite sol was synthesized via sol−gel using Ca(NO<sub<3</sub<)<sub<2</sub<∙4H<sub<2</sub<O and P<sub<2</sub<O<sub<5</sub< as precursors. The surface of the HA coating was homogeneous, as determined by scanning electron microscopy (SEM), attenuated total reflectance Fourier transform infrared (ATR-FTIR), and X-ray diffraction (XRD), which allowed the materials to be characterized. The bioactivity of the synthesized materials and their efficiency for use as future bone implants was confirmed by observing the formation of a layer of hydroxyapatite on the surface of the samples soaked in a fluid simulating the composition of human blood plasma. To verify the biocompatibility of the obtained biomaterial, fibroblasts were grown on a glass surface and were tested for viability after 24 h. The results of the WST-8 analysis suggest that the HA systems, prepared by the sol−gel method, are most suitable for modifying the surface of titanium implants and improving their biocompatibility. |
abstract_unstemmed |
Hydroxyapatite (HA) was coated onto the surface of commercially pure titanium grade 4 (a material generally used for implant application) by a dip coating method using HA sol. Hydroxyapatite sol was synthesized via sol−gel using Ca(NO<sub<3</sub<)<sub<2</sub<∙4H<sub<2</sub<O and P<sub<2</sub<O<sub<5</sub< as precursors. The surface of the HA coating was homogeneous, as determined by scanning electron microscopy (SEM), attenuated total reflectance Fourier transform infrared (ATR-FTIR), and X-ray diffraction (XRD), which allowed the materials to be characterized. The bioactivity of the synthesized materials and their efficiency for use as future bone implants was confirmed by observing the formation of a layer of hydroxyapatite on the surface of the samples soaked in a fluid simulating the composition of human blood plasma. To verify the biocompatibility of the obtained biomaterial, fibroblasts were grown on a glass surface and were tested for viability after 24 h. The results of the WST-8 analysis suggest that the HA systems, prepared by the sol−gel method, are most suitable for modifying the surface of titanium implants and improving their biocompatibility. |
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Use of the Sol–Gel Method for the Preparation of Coatings of Titanium Substrates with Hydroxyapatite for Biomedical Application |
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