Effect of Sonification Time on Synthesisi and Corrosion Resistance of Epoxy-Clay Nanocomposite
In recent years many research works have been carried out on anti-corrosive nanocomposites coatings containing mineral reinforcements. The most important criteria in these attempts are polymerization method and the type of matrix and reinforcement of nanocomposites. In this regard, the physical and...
Ausführliche Beschreibung
Autor*in: |
Niloufar Bahrami Panah [verfasserIn] Iman Danaee [verfasserIn] Behrouz Moghadasibagha [verfasserIn] |
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E-Artikel |
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Sprache: |
Persisch |
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2016 |
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Übergeordnetes Werk: |
In: علوم و تکنولوژی پلیمر - Iran Polymer and Petrochemical Institute, 2018, 29(2016), 4, Seite 335-346 |
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Übergeordnetes Werk: |
volume:29 ; year:2016 ; number:4 ; pages:335-346 |
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Link aufrufen |
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DOI / URN: |
10.22063/jipst.2016.1407 |
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Katalog-ID: |
DOAJ076559947 |
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10.22063/jipst.2016.1407 doi (DE-627)DOAJ076559947 (DE-599)DOAJ63d583ab04954ec4add528d489078e3c DE-627 ger DE-627 rakwb per TP1080-1185 Niloufar Bahrami Panah verfasserin aut Effect of Sonification Time on Synthesisi and Corrosion Resistance of Epoxy-Clay Nanocomposite 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In recent years many research works have been carried out on anti-corrosive nanocomposites coatings containing mineral reinforcements. The most important criteria in these attempts are polymerization method and the type of matrix and reinforcement of nanocomposites. In this regard, the physical and mechanical properties of the polymers in which a small amount of filler is used can be improved. In this research, an epoxy-clay nanocomposite was synthesized by in-situ polymerization method using a resin matrix based on bisphenol-A type epoxy and montmorillonite clay (Closite 15A). The treatment was used at different ultrasonic stirring times to disperse 1-4 weight percentages of clay particles into the matrix. The structure of synthesized epoxy-clay nanocomposite was studied by scanning electron microscopy and X-ray diffraction techniques. The average size of clay particles was determined by X-ray diffraction measurement. Then, anti-corrosion properties of epoxy-clay coatings, prepared under different ultrasonic durations and applied on carbon steel panels, were investigated by Tafel and electrochemical impedance spectroscopy techniques. For this purpose, the carbon steel panels coated with these coatings were immersed in 3.5% sodium chloride solution and tested at different immersion times. The results indicated that a nanocomposite containing 1% clay, synthesized, stirred 60 min ultrasonically, produced smaller particle size, lower corrosion current density and higher coating corrosion resistance than the other composite formulations. This nanocomposite provided superior protection against corrosion in sodium chloride solution. nanocomposite epoxy clay anti-corrosive coating impedance Polymers and polymer manufacture Iman Danaee verfasserin aut Behrouz Moghadasibagha verfasserin aut In علوم و تکنولوژی پلیمر Iran Polymer and Petrochemical Institute, 2018 29(2016), 4, Seite 335-346 (DE-627)88394572X (DE-600)2890840-5 20080883 nnns volume:29 year:2016 number:4 pages:335-346 https://doi.org/10.22063/jipst.2016.1407 kostenfrei https://doaj.org/article/63d583ab04954ec4add528d489078e3c kostenfrei http://jips.ippi.ac.ir/article_1407_cbc42623297b54bcde12059b05c2a6b7.pdf kostenfrei https://doaj.org/toc/1016-3255 Journal toc kostenfrei https://doaj.org/toc/2008-0883 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 29 2016 4 335-346 |
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10.22063/jipst.2016.1407 doi (DE-627)DOAJ076559947 (DE-599)DOAJ63d583ab04954ec4add528d489078e3c DE-627 ger DE-627 rakwb per TP1080-1185 Niloufar Bahrami Panah verfasserin aut Effect of Sonification Time on Synthesisi and Corrosion Resistance of Epoxy-Clay Nanocomposite 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In recent years many research works have been carried out on anti-corrosive nanocomposites coatings containing mineral reinforcements. The most important criteria in these attempts are polymerization method and the type of matrix and reinforcement of nanocomposites. In this regard, the physical and mechanical properties of the polymers in which a small amount of filler is used can be improved. In this research, an epoxy-clay nanocomposite was synthesized by in-situ polymerization method using a resin matrix based on bisphenol-A type epoxy and montmorillonite clay (Closite 15A). The treatment was used at different ultrasonic stirring times to disperse 1-4 weight percentages of clay particles into the matrix. The structure of synthesized epoxy-clay nanocomposite was studied by scanning electron microscopy and X-ray diffraction techniques. The average size of clay particles was determined by X-ray diffraction measurement. Then, anti-corrosion properties of epoxy-clay coatings, prepared under different ultrasonic durations and applied on carbon steel panels, were investigated by Tafel and electrochemical impedance spectroscopy techniques. For this purpose, the carbon steel panels coated with these coatings were immersed in 3.5% sodium chloride solution and tested at different immersion times. The results indicated that a nanocomposite containing 1% clay, synthesized, stirred 60 min ultrasonically, produced smaller particle size, lower corrosion current density and higher coating corrosion resistance than the other composite formulations. This nanocomposite provided superior protection against corrosion in sodium chloride solution. nanocomposite epoxy clay anti-corrosive coating impedance Polymers and polymer manufacture Iman Danaee verfasserin aut Behrouz Moghadasibagha verfasserin aut In علوم و تکنولوژی پلیمر Iran Polymer and Petrochemical Institute, 2018 29(2016), 4, Seite 335-346 (DE-627)88394572X (DE-600)2890840-5 20080883 nnns volume:29 year:2016 number:4 pages:335-346 https://doi.org/10.22063/jipst.2016.1407 kostenfrei https://doaj.org/article/63d583ab04954ec4add528d489078e3c kostenfrei http://jips.ippi.ac.ir/article_1407_cbc42623297b54bcde12059b05c2a6b7.pdf kostenfrei https://doaj.org/toc/1016-3255 Journal toc kostenfrei https://doaj.org/toc/2008-0883 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 29 2016 4 335-346 |
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10.22063/jipst.2016.1407 doi (DE-627)DOAJ076559947 (DE-599)DOAJ63d583ab04954ec4add528d489078e3c DE-627 ger DE-627 rakwb per TP1080-1185 Niloufar Bahrami Panah verfasserin aut Effect of Sonification Time on Synthesisi and Corrosion Resistance of Epoxy-Clay Nanocomposite 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In recent years many research works have been carried out on anti-corrosive nanocomposites coatings containing mineral reinforcements. The most important criteria in these attempts are polymerization method and the type of matrix and reinforcement of nanocomposites. In this regard, the physical and mechanical properties of the polymers in which a small amount of filler is used can be improved. In this research, an epoxy-clay nanocomposite was synthesized by in-situ polymerization method using a resin matrix based on bisphenol-A type epoxy and montmorillonite clay (Closite 15A). The treatment was used at different ultrasonic stirring times to disperse 1-4 weight percentages of clay particles into the matrix. The structure of synthesized epoxy-clay nanocomposite was studied by scanning electron microscopy and X-ray diffraction techniques. The average size of clay particles was determined by X-ray diffraction measurement. Then, anti-corrosion properties of epoxy-clay coatings, prepared under different ultrasonic durations and applied on carbon steel panels, were investigated by Tafel and electrochemical impedance spectroscopy techniques. For this purpose, the carbon steel panels coated with these coatings were immersed in 3.5% sodium chloride solution and tested at different immersion times. The results indicated that a nanocomposite containing 1% clay, synthesized, stirred 60 min ultrasonically, produced smaller particle size, lower corrosion current density and higher coating corrosion resistance than the other composite formulations. This nanocomposite provided superior protection against corrosion in sodium chloride solution. nanocomposite epoxy clay anti-corrosive coating impedance Polymers and polymer manufacture Iman Danaee verfasserin aut Behrouz Moghadasibagha verfasserin aut In علوم و تکنولوژی پلیمر Iran Polymer and Petrochemical Institute, 2018 29(2016), 4, Seite 335-346 (DE-627)88394572X (DE-600)2890840-5 20080883 nnns volume:29 year:2016 number:4 pages:335-346 https://doi.org/10.22063/jipst.2016.1407 kostenfrei https://doaj.org/article/63d583ab04954ec4add528d489078e3c kostenfrei http://jips.ippi.ac.ir/article_1407_cbc42623297b54bcde12059b05c2a6b7.pdf kostenfrei https://doaj.org/toc/1016-3255 Journal toc kostenfrei https://doaj.org/toc/2008-0883 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 29 2016 4 335-346 |
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10.22063/jipst.2016.1407 doi (DE-627)DOAJ076559947 (DE-599)DOAJ63d583ab04954ec4add528d489078e3c DE-627 ger DE-627 rakwb per TP1080-1185 Niloufar Bahrami Panah verfasserin aut Effect of Sonification Time on Synthesisi and Corrosion Resistance of Epoxy-Clay Nanocomposite 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In recent years many research works have been carried out on anti-corrosive nanocomposites coatings containing mineral reinforcements. The most important criteria in these attempts are polymerization method and the type of matrix and reinforcement of nanocomposites. In this regard, the physical and mechanical properties of the polymers in which a small amount of filler is used can be improved. In this research, an epoxy-clay nanocomposite was synthesized by in-situ polymerization method using a resin matrix based on bisphenol-A type epoxy and montmorillonite clay (Closite 15A). The treatment was used at different ultrasonic stirring times to disperse 1-4 weight percentages of clay particles into the matrix. The structure of synthesized epoxy-clay nanocomposite was studied by scanning electron microscopy and X-ray diffraction techniques. The average size of clay particles was determined by X-ray diffraction measurement. Then, anti-corrosion properties of epoxy-clay coatings, prepared under different ultrasonic durations and applied on carbon steel panels, were investigated by Tafel and electrochemical impedance spectroscopy techniques. For this purpose, the carbon steel panels coated with these coatings were immersed in 3.5% sodium chloride solution and tested at different immersion times. The results indicated that a nanocomposite containing 1% clay, synthesized, stirred 60 min ultrasonically, produced smaller particle size, lower corrosion current density and higher coating corrosion resistance than the other composite formulations. This nanocomposite provided superior protection against corrosion in sodium chloride solution. nanocomposite epoxy clay anti-corrosive coating impedance Polymers and polymer manufacture Iman Danaee verfasserin aut Behrouz Moghadasibagha verfasserin aut In علوم و تکنولوژی پلیمر Iran Polymer and Petrochemical Institute, 2018 29(2016), 4, Seite 335-346 (DE-627)88394572X (DE-600)2890840-5 20080883 nnns volume:29 year:2016 number:4 pages:335-346 https://doi.org/10.22063/jipst.2016.1407 kostenfrei https://doaj.org/article/63d583ab04954ec4add528d489078e3c kostenfrei http://jips.ippi.ac.ir/article_1407_cbc42623297b54bcde12059b05c2a6b7.pdf kostenfrei https://doaj.org/toc/1016-3255 Journal toc kostenfrei https://doaj.org/toc/2008-0883 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 29 2016 4 335-346 |
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10.22063/jipst.2016.1407 doi (DE-627)DOAJ076559947 (DE-599)DOAJ63d583ab04954ec4add528d489078e3c DE-627 ger DE-627 rakwb per TP1080-1185 Niloufar Bahrami Panah verfasserin aut Effect of Sonification Time on Synthesisi and Corrosion Resistance of Epoxy-Clay Nanocomposite 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In recent years many research works have been carried out on anti-corrosive nanocomposites coatings containing mineral reinforcements. The most important criteria in these attempts are polymerization method and the type of matrix and reinforcement of nanocomposites. In this regard, the physical and mechanical properties of the polymers in which a small amount of filler is used can be improved. In this research, an epoxy-clay nanocomposite was synthesized by in-situ polymerization method using a resin matrix based on bisphenol-A type epoxy and montmorillonite clay (Closite 15A). The treatment was used at different ultrasonic stirring times to disperse 1-4 weight percentages of clay particles into the matrix. The structure of synthesized epoxy-clay nanocomposite was studied by scanning electron microscopy and X-ray diffraction techniques. The average size of clay particles was determined by X-ray diffraction measurement. Then, anti-corrosion properties of epoxy-clay coatings, prepared under different ultrasonic durations and applied on carbon steel panels, were investigated by Tafel and electrochemical impedance spectroscopy techniques. For this purpose, the carbon steel panels coated with these coatings were immersed in 3.5% sodium chloride solution and tested at different immersion times. The results indicated that a nanocomposite containing 1% clay, synthesized, stirred 60 min ultrasonically, produced smaller particle size, lower corrosion current density and higher coating corrosion resistance than the other composite formulations. This nanocomposite provided superior protection against corrosion in sodium chloride solution. nanocomposite epoxy clay anti-corrosive coating impedance Polymers and polymer manufacture Iman Danaee verfasserin aut Behrouz Moghadasibagha verfasserin aut In علوم و تکنولوژی پلیمر Iran Polymer and Petrochemical Institute, 2018 29(2016), 4, Seite 335-346 (DE-627)88394572X (DE-600)2890840-5 20080883 nnns volume:29 year:2016 number:4 pages:335-346 https://doi.org/10.22063/jipst.2016.1407 kostenfrei https://doaj.org/article/63d583ab04954ec4add528d489078e3c kostenfrei http://jips.ippi.ac.ir/article_1407_cbc42623297b54bcde12059b05c2a6b7.pdf kostenfrei https://doaj.org/toc/1016-3255 Journal toc kostenfrei https://doaj.org/toc/2008-0883 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 29 2016 4 335-346 |
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TP1080-1185 Effect of Sonification Time on Synthesisi and Corrosion Resistance of Epoxy-Clay Nanocomposite nanocomposite epoxy clay anti-corrosive coating impedance |
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Effect of Sonification Time on Synthesisi and Corrosion Resistance of Epoxy-Clay Nanocomposite |
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In recent years many research works have been carried out on anti-corrosive nanocomposites coatings containing mineral reinforcements. The most important criteria in these attempts are polymerization method and the type of matrix and reinforcement of nanocomposites. In this regard, the physical and mechanical properties of the polymers in which a small amount of filler is used can be improved. In this research, an epoxy-clay nanocomposite was synthesized by in-situ polymerization method using a resin matrix based on bisphenol-A type epoxy and montmorillonite clay (Closite 15A). The treatment was used at different ultrasonic stirring times to disperse 1-4 weight percentages of clay particles into the matrix. The structure of synthesized epoxy-clay nanocomposite was studied by scanning electron microscopy and X-ray diffraction techniques. The average size of clay particles was determined by X-ray diffraction measurement. Then, anti-corrosion properties of epoxy-clay coatings, prepared under different ultrasonic durations and applied on carbon steel panels, were investigated by Tafel and electrochemical impedance spectroscopy techniques. For this purpose, the carbon steel panels coated with these coatings were immersed in 3.5% sodium chloride solution and tested at different immersion times. The results indicated that a nanocomposite containing 1% clay, synthesized, stirred 60 min ultrasonically, produced smaller particle size, lower corrosion current density and higher coating corrosion resistance than the other composite formulations. This nanocomposite provided superior protection against corrosion in sodium chloride solution. |
abstractGer |
In recent years many research works have been carried out on anti-corrosive nanocomposites coatings containing mineral reinforcements. The most important criteria in these attempts are polymerization method and the type of matrix and reinforcement of nanocomposites. In this regard, the physical and mechanical properties of the polymers in which a small amount of filler is used can be improved. In this research, an epoxy-clay nanocomposite was synthesized by in-situ polymerization method using a resin matrix based on bisphenol-A type epoxy and montmorillonite clay (Closite 15A). The treatment was used at different ultrasonic stirring times to disperse 1-4 weight percentages of clay particles into the matrix. The structure of synthesized epoxy-clay nanocomposite was studied by scanning electron microscopy and X-ray diffraction techniques. The average size of clay particles was determined by X-ray diffraction measurement. Then, anti-corrosion properties of epoxy-clay coatings, prepared under different ultrasonic durations and applied on carbon steel panels, were investigated by Tafel and electrochemical impedance spectroscopy techniques. For this purpose, the carbon steel panels coated with these coatings were immersed in 3.5% sodium chloride solution and tested at different immersion times. The results indicated that a nanocomposite containing 1% clay, synthesized, stirred 60 min ultrasonically, produced smaller particle size, lower corrosion current density and higher coating corrosion resistance than the other composite formulations. This nanocomposite provided superior protection against corrosion in sodium chloride solution. |
abstract_unstemmed |
In recent years many research works have been carried out on anti-corrosive nanocomposites coatings containing mineral reinforcements. The most important criteria in these attempts are polymerization method and the type of matrix and reinforcement of nanocomposites. In this regard, the physical and mechanical properties of the polymers in which a small amount of filler is used can be improved. In this research, an epoxy-clay nanocomposite was synthesized by in-situ polymerization method using a resin matrix based on bisphenol-A type epoxy and montmorillonite clay (Closite 15A). The treatment was used at different ultrasonic stirring times to disperse 1-4 weight percentages of clay particles into the matrix. The structure of synthesized epoxy-clay nanocomposite was studied by scanning electron microscopy and X-ray diffraction techniques. The average size of clay particles was determined by X-ray diffraction measurement. Then, anti-corrosion properties of epoxy-clay coatings, prepared under different ultrasonic durations and applied on carbon steel panels, were investigated by Tafel and electrochemical impedance spectroscopy techniques. For this purpose, the carbon steel panels coated with these coatings were immersed in 3.5% sodium chloride solution and tested at different immersion times. The results indicated that a nanocomposite containing 1% clay, synthesized, stirred 60 min ultrasonically, produced smaller particle size, lower corrosion current density and higher coating corrosion resistance than the other composite formulations. This nanocomposite provided superior protection against corrosion in sodium chloride solution. |
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Effect of Sonification Time on Synthesisi and Corrosion Resistance of Epoxy-Clay Nanocomposite |
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