Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran

Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phen...
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Autor*in:	Muzzamal Hussain [verfasserIn] Farhan Saeed [verfasserIn] Bushra Niaz [verfasserIn] Ali Imran [verfasserIn] Tabussam Tufail [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2022

Schlagwörter:	arabinoxylans ferulic acid ferulated arabinoxylans HPLC FTIR maize bran

Übergeordnetes Werk:	In: Foods - MDPI AG, 2013, 11(2022), 21, p 3374
Übergeordnetes Werk:	volume:11 ; year:2022 ; number:21, p 3374

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/foods11213374

Katalog-ID:	DOAJ086492195

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520			\|a Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phenolic compounds) and structural characteristics (FTIR, SEM and XRD) as well as antioxidant activity. Results showed that contents of ferulated arabinoxylans were 8.1 ± 0.04% and 6.8 ± 0.02 in NMB and NNMB, respectively. Moreover, the purity of arabinoxylans was 60.1 ± 0.8% and 57.04 ± 0.7% in NMB and NNMB ferulated arabinoxylans. Furthermore, ferulated arabinoxylans have higher arabinose, xylose and ferulic acid contents. FTIR spectra of NMB and NNMB ferulated arabinoxylans depicted the presence of polysaccharide compounds and the corresponding band was observed at 993 cm<sup<−1</sup<, which is due to glycosidic bond vibration. In addition, absorbance regions of arabinoxylans between 900 cm<sup<−1</sup< to 1200 cm<sup<−1</sup< were observed. Moreover, SEM micrographs of ferulated arabinoxylans had visible rough and porous surface morphology. Further, ferulated arabinoxylans of NMB and NNMB did not exhibit any sharp peaks in XRD graphs, attributed to their amorphous nature. However, XRD 2θ showed peaks at 20.0°, which predominantly indicated that the material has an amorphous state with small crystalline regions in the sample, which shows the presence of xylans (small and narrow sharp peaks).
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allfields	10.3390/foods11213374 doi (DE-627)DOAJ086492195 (DE-599)DOAJdc6cf8bd8eaa436e9fa8b2a8a2f7031d DE-627 ger DE-627 rakwb eng TP1-1185 Muzzamal Hussain verfasserin aut Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phenolic compounds) and structural characteristics (FTIR, SEM and XRD) as well as antioxidant activity. Results showed that contents of ferulated arabinoxylans were 8.1 ± 0.04% and 6.8 ± 0.02 in NMB and NNMB, respectively. Moreover, the purity of arabinoxylans was 60.1 ± 0.8% and 57.04 ± 0.7% in NMB and NNMB ferulated arabinoxylans. Furthermore, ferulated arabinoxylans have higher arabinose, xylose and ferulic acid contents. FTIR spectra of NMB and NNMB ferulated arabinoxylans depicted the presence of polysaccharide compounds and the corresponding band was observed at 993 cm<sup<−1</sup<, which is due to glycosidic bond vibration. In addition, absorbance regions of arabinoxylans between 900 cm<sup<−1</sup< to 1200 cm<sup<−1</sup< were observed. Moreover, SEM micrographs of ferulated arabinoxylans had visible rough and porous surface morphology. Further, ferulated arabinoxylans of NMB and NNMB did not exhibit any sharp peaks in XRD graphs, attributed to their amorphous nature. However, XRD 2θ showed peaks at 20.0°, which predominantly indicated that the material has an amorphous state with small crystalline regions in the sample, which shows the presence of xylans (small and narrow sharp peaks). arabinoxylans ferulic acid ferulated arabinoxylans HPLC FTIR maize bran Chemical technology Farhan Saeed verfasserin aut Bushra Niaz verfasserin aut Ali Imran verfasserin aut Tabussam Tufail verfasserin aut In Foods MDPI AG, 2013 11(2022), 21, p 3374 (DE-627)737287632 (DE-600)2704223-6 23048158 nnns volume:11 year:2022 number:21, p 3374 https://doi.org/10.3390/foods11213374 kostenfrei https://doaj.org/article/dc6cf8bd8eaa436e9fa8b2a8a2f7031d kostenfrei https://www.mdpi.com/2304-8158/11/21/3374 kostenfrei https://doaj.org/toc/2304-8158 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 11 2022 21, p 3374
spelling	10.3390/foods11213374 doi (DE-627)DOAJ086492195 (DE-599)DOAJdc6cf8bd8eaa436e9fa8b2a8a2f7031d DE-627 ger DE-627 rakwb eng TP1-1185 Muzzamal Hussain verfasserin aut Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phenolic compounds) and structural characteristics (FTIR, SEM and XRD) as well as antioxidant activity. Results showed that contents of ferulated arabinoxylans were 8.1 ± 0.04% and 6.8 ± 0.02 in NMB and NNMB, respectively. Moreover, the purity of arabinoxylans was 60.1 ± 0.8% and 57.04 ± 0.7% in NMB and NNMB ferulated arabinoxylans. Furthermore, ferulated arabinoxylans have higher arabinose, xylose and ferulic acid contents. FTIR spectra of NMB and NNMB ferulated arabinoxylans depicted the presence of polysaccharide compounds and the corresponding band was observed at 993 cm<sup<−1</sup<, which is due to glycosidic bond vibration. In addition, absorbance regions of arabinoxylans between 900 cm<sup<−1</sup< to 1200 cm<sup<−1</sup< were observed. Moreover, SEM micrographs of ferulated arabinoxylans had visible rough and porous surface morphology. Further, ferulated arabinoxylans of NMB and NNMB did not exhibit any sharp peaks in XRD graphs, attributed to their amorphous nature. However, XRD 2θ showed peaks at 20.0°, which predominantly indicated that the material has an amorphous state with small crystalline regions in the sample, which shows the presence of xylans (small and narrow sharp peaks). arabinoxylans ferulic acid ferulated arabinoxylans HPLC FTIR maize bran Chemical technology Farhan Saeed verfasserin aut Bushra Niaz verfasserin aut Ali Imran verfasserin aut Tabussam Tufail verfasserin aut In Foods MDPI AG, 2013 11(2022), 21, p 3374 (DE-627)737287632 (DE-600)2704223-6 23048158 nnns volume:11 year:2022 number:21, p 3374 https://doi.org/10.3390/foods11213374 kostenfrei https://doaj.org/article/dc6cf8bd8eaa436e9fa8b2a8a2f7031d kostenfrei https://www.mdpi.com/2304-8158/11/21/3374 kostenfrei https://doaj.org/toc/2304-8158 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 11 2022 21, p 3374
allfields_unstemmed	10.3390/foods11213374 doi (DE-627)DOAJ086492195 (DE-599)DOAJdc6cf8bd8eaa436e9fa8b2a8a2f7031d DE-627 ger DE-627 rakwb eng TP1-1185 Muzzamal Hussain verfasserin aut Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phenolic compounds) and structural characteristics (FTIR, SEM and XRD) as well as antioxidant activity. Results showed that contents of ferulated arabinoxylans were 8.1 ± 0.04% and 6.8 ± 0.02 in NMB and NNMB, respectively. Moreover, the purity of arabinoxylans was 60.1 ± 0.8% and 57.04 ± 0.7% in NMB and NNMB ferulated arabinoxylans. Furthermore, ferulated arabinoxylans have higher arabinose, xylose and ferulic acid contents. FTIR spectra of NMB and NNMB ferulated arabinoxylans depicted the presence of polysaccharide compounds and the corresponding band was observed at 993 cm<sup<−1</sup<, which is due to glycosidic bond vibration. In addition, absorbance regions of arabinoxylans between 900 cm<sup<−1</sup< to 1200 cm<sup<−1</sup< were observed. Moreover, SEM micrographs of ferulated arabinoxylans had visible rough and porous surface morphology. Further, ferulated arabinoxylans of NMB and NNMB did not exhibit any sharp peaks in XRD graphs, attributed to their amorphous nature. However, XRD 2θ showed peaks at 20.0°, which predominantly indicated that the material has an amorphous state with small crystalline regions in the sample, which shows the presence of xylans (small and narrow sharp peaks). arabinoxylans ferulic acid ferulated arabinoxylans HPLC FTIR maize bran Chemical technology Farhan Saeed verfasserin aut Bushra Niaz verfasserin aut Ali Imran verfasserin aut Tabussam Tufail verfasserin aut In Foods MDPI AG, 2013 11(2022), 21, p 3374 (DE-627)737287632 (DE-600)2704223-6 23048158 nnns volume:11 year:2022 number:21, p 3374 https://doi.org/10.3390/foods11213374 kostenfrei https://doaj.org/article/dc6cf8bd8eaa436e9fa8b2a8a2f7031d kostenfrei https://www.mdpi.com/2304-8158/11/21/3374 kostenfrei https://doaj.org/toc/2304-8158 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 11 2022 21, p 3374
allfieldsGer	10.3390/foods11213374 doi (DE-627)DOAJ086492195 (DE-599)DOAJdc6cf8bd8eaa436e9fa8b2a8a2f7031d DE-627 ger DE-627 rakwb eng TP1-1185 Muzzamal Hussain verfasserin aut Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phenolic compounds) and structural characteristics (FTIR, SEM and XRD) as well as antioxidant activity. Results showed that contents of ferulated arabinoxylans were 8.1 ± 0.04% and 6.8 ± 0.02 in NMB and NNMB, respectively. Moreover, the purity of arabinoxylans was 60.1 ± 0.8% and 57.04 ± 0.7% in NMB and NNMB ferulated arabinoxylans. Furthermore, ferulated arabinoxylans have higher arabinose, xylose and ferulic acid contents. FTIR spectra of NMB and NNMB ferulated arabinoxylans depicted the presence of polysaccharide compounds and the corresponding band was observed at 993 cm<sup<−1</sup<, which is due to glycosidic bond vibration. In addition, absorbance regions of arabinoxylans between 900 cm<sup<−1</sup< to 1200 cm<sup<−1</sup< were observed. Moreover, SEM micrographs of ferulated arabinoxylans had visible rough and porous surface morphology. Further, ferulated arabinoxylans of NMB and NNMB did not exhibit any sharp peaks in XRD graphs, attributed to their amorphous nature. However, XRD 2θ showed peaks at 20.0°, which predominantly indicated that the material has an amorphous state with small crystalline regions in the sample, which shows the presence of xylans (small and narrow sharp peaks). arabinoxylans ferulic acid ferulated arabinoxylans HPLC FTIR maize bran Chemical technology Farhan Saeed verfasserin aut Bushra Niaz verfasserin aut Ali Imran verfasserin aut Tabussam Tufail verfasserin aut In Foods MDPI AG, 2013 11(2022), 21, p 3374 (DE-627)737287632 (DE-600)2704223-6 23048158 nnns volume:11 year:2022 number:21, p 3374 https://doi.org/10.3390/foods11213374 kostenfrei https://doaj.org/article/dc6cf8bd8eaa436e9fa8b2a8a2f7031d kostenfrei https://www.mdpi.com/2304-8158/11/21/3374 kostenfrei https://doaj.org/toc/2304-8158 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 11 2022 21, p 3374
allfieldsSound	10.3390/foods11213374 doi (DE-627)DOAJ086492195 (DE-599)DOAJdc6cf8bd8eaa436e9fa8b2a8a2f7031d DE-627 ger DE-627 rakwb eng TP1-1185 Muzzamal Hussain verfasserin aut Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phenolic compounds) and structural characteristics (FTIR, SEM and XRD) as well as antioxidant activity. Results showed that contents of ferulated arabinoxylans were 8.1 ± 0.04% and 6.8 ± 0.02 in NMB and NNMB, respectively. Moreover, the purity of arabinoxylans was 60.1 ± 0.8% and 57.04 ± 0.7% in NMB and NNMB ferulated arabinoxylans. Furthermore, ferulated arabinoxylans have higher arabinose, xylose and ferulic acid contents. FTIR spectra of NMB and NNMB ferulated arabinoxylans depicted the presence of polysaccharide compounds and the corresponding band was observed at 993 cm<sup<−1</sup<, which is due to glycosidic bond vibration. In addition, absorbance regions of arabinoxylans between 900 cm<sup<−1</sup< to 1200 cm<sup<−1</sup< were observed. Moreover, SEM micrographs of ferulated arabinoxylans had visible rough and porous surface morphology. Further, ferulated arabinoxylans of NMB and NNMB did not exhibit any sharp peaks in XRD graphs, attributed to their amorphous nature. However, XRD 2θ showed peaks at 20.0°, which predominantly indicated that the material has an amorphous state with small crystalline regions in the sample, which shows the presence of xylans (small and narrow sharp peaks). arabinoxylans ferulic acid ferulated arabinoxylans HPLC FTIR maize bran Chemical technology Farhan Saeed verfasserin aut Bushra Niaz verfasserin aut Ali Imran verfasserin aut Tabussam Tufail verfasserin aut In Foods MDPI AG, 2013 11(2022), 21, p 3374 (DE-627)737287632 (DE-600)2704223-6 23048158 nnns volume:11 year:2022 number:21, p 3374 https://doi.org/10.3390/foods11213374 kostenfrei https://doaj.org/article/dc6cf8bd8eaa436e9fa8b2a8a2f7031d kostenfrei https://www.mdpi.com/2304-8158/11/21/3374 kostenfrei https://doaj.org/toc/2304-8158 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 11 2022 21, p 3374
language	English
source	In Foods 11(2022), 21, p 3374 volume:11 year:2022 number:21, p 3374
sourceStr	In Foods 11(2022), 21, p 3374 volume:11 year:2022 number:21, p 3374
format_phy_str_mv	Article
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topic_facet	arabinoxylans ferulic acid ferulated arabinoxylans HPLC FTIR maize bran Chemical technology
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authorswithroles_txt_mv	Muzzamal Hussain @@aut@@ Farhan Saeed @@aut@@ Bushra Niaz @@aut@@ Ali Imran @@aut@@ Tabussam Tufail @@aut@@
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callnumber-first	T - Technology
author	Muzzamal Hussain
spellingShingle	Muzzamal Hussain misc TP1-1185 misc arabinoxylans misc ferulic acid misc ferulated arabinoxylans misc HPLC misc FTIR misc maize bran misc Chemical technology Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran
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topic_title	TP1-1185 Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran arabinoxylans ferulic acid ferulated arabinoxylans HPLC FTIR maize bran
topic	misc TP1-1185 misc arabinoxylans misc ferulic acid misc ferulated arabinoxylans misc HPLC misc FTIR misc maize bran misc Chemical technology
topic_unstemmed	misc TP1-1185 misc arabinoxylans misc ferulic acid misc ferulated arabinoxylans misc HPLC misc FTIR misc maize bran misc Chemical technology
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title	Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran
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title_full	Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran
author_sort	Muzzamal Hussain
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author_browse	Muzzamal Hussain Farhan Saeed Bushra Niaz Ali Imran Tabussam Tufail
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title_sort	biochemical and structural characterization of ferulated arabinoxylans extracted from nixtamalized and non-nixtamalized maize bran
callnumber	TP1-1185
title_auth	Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran
abstract	Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phenolic compounds) and structural characteristics (FTIR, SEM and XRD) as well as antioxidant activity. Results showed that contents of ferulated arabinoxylans were 8.1 ± 0.04% and 6.8 ± 0.02 in NMB and NNMB, respectively. Moreover, the purity of arabinoxylans was 60.1 ± 0.8% and 57.04 ± 0.7% in NMB and NNMB ferulated arabinoxylans. Furthermore, ferulated arabinoxylans have higher arabinose, xylose and ferulic acid contents. FTIR spectra of NMB and NNMB ferulated arabinoxylans depicted the presence of polysaccharide compounds and the corresponding band was observed at 993 cm<sup<−1</sup<, which is due to glycosidic bond vibration. In addition, absorbance regions of arabinoxylans between 900 cm<sup<−1</sup< to 1200 cm<sup<−1</sup< were observed. Moreover, SEM micrographs of ferulated arabinoxylans had visible rough and porous surface morphology. Further, ferulated arabinoxylans of NMB and NNMB did not exhibit any sharp peaks in XRD graphs, attributed to their amorphous nature. However, XRD 2θ showed peaks at 20.0°, which predominantly indicated that the material has an amorphous state with small crystalline regions in the sample, which shows the presence of xylans (small and narrow sharp peaks).
abstractGer	Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phenolic compounds) and structural characteristics (FTIR, SEM and XRD) as well as antioxidant activity. Results showed that contents of ferulated arabinoxylans were 8.1 ± 0.04% and 6.8 ± 0.02 in NMB and NNMB, respectively. Moreover, the purity of arabinoxylans was 60.1 ± 0.8% and 57.04 ± 0.7% in NMB and NNMB ferulated arabinoxylans. Furthermore, ferulated arabinoxylans have higher arabinose, xylose and ferulic acid contents. FTIR spectra of NMB and NNMB ferulated arabinoxylans depicted the presence of polysaccharide compounds and the corresponding band was observed at 993 cm<sup<−1</sup<, which is due to glycosidic bond vibration. In addition, absorbance regions of arabinoxylans between 900 cm<sup<−1</sup< to 1200 cm<sup<−1</sup< were observed. Moreover, SEM micrographs of ferulated arabinoxylans had visible rough and porous surface morphology. Further, ferulated arabinoxylans of NMB and NNMB did not exhibit any sharp peaks in XRD graphs, attributed to their amorphous nature. However, XRD 2θ showed peaks at 20.0°, which predominantly indicated that the material has an amorphous state with small crystalline regions in the sample, which shows the presence of xylans (small and narrow sharp peaks).
abstract_unstemmed	Maize bran is a good source of non-starch polysaccharides, having various bioactive compounds. In the current research, we extracted the ferulated arabinoxylans from nixtamalized maize bran (NMB) and non-nixtamalized maize bran (NNMB) and explored their biochemical composition (monosaccharides, phenolic compounds) and structural characteristics (FTIR, SEM and XRD) as well as antioxidant activity. Results showed that contents of ferulated arabinoxylans were 8.1 ± 0.04% and 6.8 ± 0.02 in NMB and NNMB, respectively. Moreover, the purity of arabinoxylans was 60.1 ± 0.8% and 57.04 ± 0.7% in NMB and NNMB ferulated arabinoxylans. Furthermore, ferulated arabinoxylans have higher arabinose, xylose and ferulic acid contents. FTIR spectra of NMB and NNMB ferulated arabinoxylans depicted the presence of polysaccharide compounds and the corresponding band was observed at 993 cm<sup<−1</sup<, which is due to glycosidic bond vibration. In addition, absorbance regions of arabinoxylans between 900 cm<sup<−1</sup< to 1200 cm<sup<−1</sup< were observed. Moreover, SEM micrographs of ferulated arabinoxylans had visible rough and porous surface morphology. Further, ferulated arabinoxylans of NMB and NNMB did not exhibit any sharp peaks in XRD graphs, attributed to their amorphous nature. However, XRD 2θ showed peaks at 20.0°, which predominantly indicated that the material has an amorphous state with small crystalline regions in the sample, which shows the presence of xylans (small and narrow sharp peaks).
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container_issue	21, p 3374
title_short	Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran
url	https://doi.org/10.3390/foods11213374 https://doaj.org/article/dc6cf8bd8eaa436e9fa8b2a8a2f7031d https://www.mdpi.com/2304-8158/11/21/3374 https://doaj.org/toc/2304-8158
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Biochemical and Structural Characterization of Ferulated Arabinoxylans Extracted from Nixtamalized and Non-Nixtamalized Maize Bran

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