Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate

The reversible electrochemical lithiation of potassium iron hexacyanocobaltate (FeCo) was studied by operando X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) assisted by chemometric techniques. In this way, it was possible to follow the system dynamics and retrieve structural and...
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Autor*in:	Angelo Mullaliu [verfasserIn] Paolo Conti [verfasserIn] Giuliana Aquilanti [verfasserIn] Jasper Rikkert Plaisier [verfasserIn] Lorenzo Stievano [verfasserIn] Marco Giorgetti [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2018

Schlagwörter:	battery XRD XAFS EXAFS MCR-ALS operando

Übergeordnetes Werk:	In: Condensed Matter - MDPI AG, 2017, 3(2018), 4, p 36
Übergeordnetes Werk:	volume:3 ; year:2018 ; number:4, p 36

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/condmat3040036

Katalog-ID:	DOAJ08658958X

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520			\|a The reversible electrochemical lithiation of potassium iron hexacyanocobaltate (FeCo) was studied by operando X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) assisted by chemometric techniques. In this way, it was possible to follow the system dynamics and retrieve structural and electronic transformations along cycling at both Fe and Co sites. These analyses confirmed that FeCo features iron as the main electroactive site. Even though the release of potassium ions causes a local disorder around the iron site, the material exhibits an excellent structural stability during the alkali ion deinsertion/insertion processes. An independent but interrelated analysis approach offers a good strategy for data treatment and provides a time-resolved picture of the studied system.
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spelling	10.3390/condmat3040036 doi (DE-627)DOAJ08658958X (DE-599)DOAJ404f0971fdc94161b80be6d0800dcb51 DE-627 ger DE-627 rakwb eng QC1-999 Angelo Mullaliu verfasserin aut Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reversible electrochemical lithiation of potassium iron hexacyanocobaltate (FeCo) was studied by operando X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) assisted by chemometric techniques. In this way, it was possible to follow the system dynamics and retrieve structural and electronic transformations along cycling at both Fe and Co sites. These analyses confirmed that FeCo features iron as the main electroactive site. Even though the release of potassium ions causes a local disorder around the iron site, the material exhibits an excellent structural stability during the alkali ion deinsertion/insertion processes. An independent but interrelated analysis approach offers a good strategy for data treatment and provides a time-resolved picture of the studied system. battery XRD XAFS EXAFS MCR-ALS operando Physics Paolo Conti verfasserin aut Giuliana Aquilanti verfasserin aut Jasper Rikkert Plaisier verfasserin aut Lorenzo Stievano verfasserin aut Marco Giorgetti verfasserin aut In Condensed Matter MDPI AG, 2017 3(2018), 4, p 36 (DE-627)873952502 (DE-600)2877004-3 24103896 nnns volume:3 year:2018 number:4, p 36 https://doi.org/10.3390/condmat3040036 kostenfrei https://doaj.org/article/404f0971fdc94161b80be6d0800dcb51 kostenfrei https://www.mdpi.com/2410-3896/3/4/36 kostenfrei https://doaj.org/toc/2410-3896 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 3 2018 4, p 36
allfields_unstemmed	10.3390/condmat3040036 doi (DE-627)DOAJ08658958X (DE-599)DOAJ404f0971fdc94161b80be6d0800dcb51 DE-627 ger DE-627 rakwb eng QC1-999 Angelo Mullaliu verfasserin aut Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reversible electrochemical lithiation of potassium iron hexacyanocobaltate (FeCo) was studied by operando X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) assisted by chemometric techniques. In this way, it was possible to follow the system dynamics and retrieve structural and electronic transformations along cycling at both Fe and Co sites. These analyses confirmed that FeCo features iron as the main electroactive site. Even though the release of potassium ions causes a local disorder around the iron site, the material exhibits an excellent structural stability during the alkali ion deinsertion/insertion processes. An independent but interrelated analysis approach offers a good strategy for data treatment and provides a time-resolved picture of the studied system. battery XRD XAFS EXAFS MCR-ALS operando Physics Paolo Conti verfasserin aut Giuliana Aquilanti verfasserin aut Jasper Rikkert Plaisier verfasserin aut Lorenzo Stievano verfasserin aut Marco Giorgetti verfasserin aut In Condensed Matter MDPI AG, 2017 3(2018), 4, p 36 (DE-627)873952502 (DE-600)2877004-3 24103896 nnns volume:3 year:2018 number:4, p 36 https://doi.org/10.3390/condmat3040036 kostenfrei https://doaj.org/article/404f0971fdc94161b80be6d0800dcb51 kostenfrei https://www.mdpi.com/2410-3896/3/4/36 kostenfrei https://doaj.org/toc/2410-3896 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 3 2018 4, p 36
allfieldsGer	10.3390/condmat3040036 doi (DE-627)DOAJ08658958X (DE-599)DOAJ404f0971fdc94161b80be6d0800dcb51 DE-627 ger DE-627 rakwb eng QC1-999 Angelo Mullaliu verfasserin aut Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reversible electrochemical lithiation of potassium iron hexacyanocobaltate (FeCo) was studied by operando X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) assisted by chemometric techniques. In this way, it was possible to follow the system dynamics and retrieve structural and electronic transformations along cycling at both Fe and Co sites. These analyses confirmed that FeCo features iron as the main electroactive site. Even though the release of potassium ions causes a local disorder around the iron site, the material exhibits an excellent structural stability during the alkali ion deinsertion/insertion processes. An independent but interrelated analysis approach offers a good strategy for data treatment and provides a time-resolved picture of the studied system. battery XRD XAFS EXAFS MCR-ALS operando Physics Paolo Conti verfasserin aut Giuliana Aquilanti verfasserin aut Jasper Rikkert Plaisier verfasserin aut Lorenzo Stievano verfasserin aut Marco Giorgetti verfasserin aut In Condensed Matter MDPI AG, 2017 3(2018), 4, p 36 (DE-627)873952502 (DE-600)2877004-3 24103896 nnns volume:3 year:2018 number:4, p 36 https://doi.org/10.3390/condmat3040036 kostenfrei https://doaj.org/article/404f0971fdc94161b80be6d0800dcb51 kostenfrei https://www.mdpi.com/2410-3896/3/4/36 kostenfrei https://doaj.org/toc/2410-3896 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 3 2018 4, p 36
allfieldsSound	10.3390/condmat3040036 doi (DE-627)DOAJ08658958X (DE-599)DOAJ404f0971fdc94161b80be6d0800dcb51 DE-627 ger DE-627 rakwb eng QC1-999 Angelo Mullaliu verfasserin aut Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reversible electrochemical lithiation of potassium iron hexacyanocobaltate (FeCo) was studied by operando X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) assisted by chemometric techniques. In this way, it was possible to follow the system dynamics and retrieve structural and electronic transformations along cycling at both Fe and Co sites. These analyses confirmed that FeCo features iron as the main electroactive site. Even though the release of potassium ions causes a local disorder around the iron site, the material exhibits an excellent structural stability during the alkali ion deinsertion/insertion processes. An independent but interrelated analysis approach offers a good strategy for data treatment and provides a time-resolved picture of the studied system. battery XRD XAFS EXAFS MCR-ALS operando Physics Paolo Conti verfasserin aut Giuliana Aquilanti verfasserin aut Jasper Rikkert Plaisier verfasserin aut Lorenzo Stievano verfasserin aut Marco Giorgetti verfasserin aut In Condensed Matter MDPI AG, 2017 3(2018), 4, p 36 (DE-627)873952502 (DE-600)2877004-3 24103896 nnns volume:3 year:2018 number:4, p 36 https://doi.org/10.3390/condmat3040036 kostenfrei https://doaj.org/article/404f0971fdc94161b80be6d0800dcb51 kostenfrei https://www.mdpi.com/2410-3896/3/4/36 kostenfrei https://doaj.org/toc/2410-3896 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 3 2018 4, p 36
language	English
source	In Condensed Matter 3(2018), 4, p 36 volume:3 year:2018 number:4, p 36
sourceStr	In Condensed Matter 3(2018), 4, p 36 volume:3 year:2018 number:4, p 36
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institution	findex.gbv.de
topic_facet	battery XRD XAFS EXAFS MCR-ALS operando Physics
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container_title	Condensed Matter
authorswithroles_txt_mv	Angelo Mullaliu @@aut@@ Paolo Conti @@aut@@ Giuliana Aquilanti @@aut@@ Jasper Rikkert Plaisier @@aut@@ Lorenzo Stievano @@aut@@ Marco Giorgetti @@aut@@
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callnumber-first	Q - Science
author	Angelo Mullaliu
spellingShingle	Angelo Mullaliu misc QC1-999 misc battery misc XRD misc XAFS misc EXAFS misc MCR-ALS misc operando misc Physics Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate
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topic_title	QC1-999 Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate battery XRD XAFS EXAFS MCR-ALS operando
topic	misc QC1-999 misc battery misc XRD misc XAFS misc EXAFS misc MCR-ALS misc operando misc Physics
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title	Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate
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title_full	Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate
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title_sort	operando xafs and xrd study of a prussian blue analogue cathode material: iron hexacyanocobaltate
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title_auth	Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate
abstract	The reversible electrochemical lithiation of potassium iron hexacyanocobaltate (FeCo) was studied by operando X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) assisted by chemometric techniques. In this way, it was possible to follow the system dynamics and retrieve structural and electronic transformations along cycling at both Fe and Co sites. These analyses confirmed that FeCo features iron as the main electroactive site. Even though the release of potassium ions causes a local disorder around the iron site, the material exhibits an excellent structural stability during the alkali ion deinsertion/insertion processes. An independent but interrelated analysis approach offers a good strategy for data treatment and provides a time-resolved picture of the studied system.
abstractGer	The reversible electrochemical lithiation of potassium iron hexacyanocobaltate (FeCo) was studied by operando X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) assisted by chemometric techniques. In this way, it was possible to follow the system dynamics and retrieve structural and electronic transformations along cycling at both Fe and Co sites. These analyses confirmed that FeCo features iron as the main electroactive site. Even though the release of potassium ions causes a local disorder around the iron site, the material exhibits an excellent structural stability during the alkali ion deinsertion/insertion processes. An independent but interrelated analysis approach offers a good strategy for data treatment and provides a time-resolved picture of the studied system.
abstract_unstemmed	The reversible electrochemical lithiation of potassium iron hexacyanocobaltate (FeCo) was studied by operando X-ray diffraction (XRD) and X-ray absorption fine structure (XAFS) assisted by chemometric techniques. In this way, it was possible to follow the system dynamics and retrieve structural and electronic transformations along cycling at both Fe and Co sites. These analyses confirmed that FeCo features iron as the main electroactive site. Even though the release of potassium ions causes a local disorder around the iron site, the material exhibits an excellent structural stability during the alkali ion deinsertion/insertion processes. An independent but interrelated analysis approach offers a good strategy for data treatment and provides a time-resolved picture of the studied system.
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title_short	Operando XAFS and XRD Study of a Prussian Blue Analogue Cathode Material: Iron Hexacyanocobaltate
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