Bis[μ-1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene-κ2N3:N3′]silver(I) dinitrate dihydrate

The reaction of 1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) with silver(I) nitrate in a 1:1 molar ratio generates the metallacyclic title complex, [Ag2(C12H14N4)2](NO3)2·2H2O, in which the bib ligand displays a cis configuration. Each bib ligand acts as a bidentate bridging ligand connecting...
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Gespeichert in:

Autor*in:	Yu-Qiang Ding [verfasserIn] Zhi-Qiang Liu [verfasserIn] Bin Shen [verfasserIn] Chun-Xia Ren [verfasserIn] Hua Sun [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2008

Übergeordnetes Werk:	In: Acta Crystallographica Section E - International Union of Crystallography, 2005, 64(2008), 2, Seite m427-m428
Übergeordnetes Werk:	volume:64 ; year:2008 ; number:2 ; pages:m427-m428

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.1107/S1600536808001633

Katalog-ID:	DOAJ087078457

Internformat


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520			\|a The reaction of 1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) with silver(I) nitrate in a 1:1 molar ratio generates the metallacyclic title complex, [Ag2(C12H14N4)2](NO3)2·2H2O, in which the bib ligand displays a cis configuration. Each bib ligand acts as a bidentate bridging ligand connecting a pair of AgI ions to form a [2 + 2] metallamacrocycle in which the Ag...Ag distance is 6.77 (2) Å. Each AgI ion has weak contacts (2.91 Å) with the nitrate anion. The uncoordinated water molecules make hydrogen bonds with nitrate O atoms, forming chains. The H atoms attached to the uncoordinated nitrogen interact with these chains through N—H...O hydrogen bonds, forming layers parallel to the (overline{1}11) plane.
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allfieldsSound	10.1107/S1600536808001633 doi (DE-627)DOAJ087078457 (DE-599)DOAJb1faa5b5e23f4ee98ff164b0c6f9b743 DE-627 ger DE-627 rakwb eng QD901-999 Yu-Qiang Ding verfasserin aut Bis[μ-1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene-κ2N3:N3′]silver(I) dinitrate dihydrate 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The reaction of 1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) with silver(I) nitrate in a 1:1 molar ratio generates the metallacyclic title complex, [Ag2(C12H14N4)2](NO3)2·2H2O, in which the bib ligand displays a cis configuration. Each bib ligand acts as a bidentate bridging ligand connecting a pair of AgI ions to form a [2 + 2] metallamacrocycle in which the Ag...Ag distance is 6.77 (2) Å. Each AgI ion has weak contacts (2.91 Å) with the nitrate anion. The uncoordinated water molecules make hydrogen bonds with nitrate O atoms, forming chains. The H atoms attached to the uncoordinated nitrogen interact with these chains through N—H...O hydrogen bonds, forming layers parallel to the (overline{1}11) plane. Crystallography Zhi-Qiang Liu verfasserin aut Bin Shen verfasserin aut Chun-Xia Ren verfasserin aut Hua Sun verfasserin aut In Acta Crystallographica Section E International Union of Crystallography, 2005 64(2008), 2, Seite m427-m428 (DE-627)326977392 (DE-600)2041947-8 16005368 nnns volume:64 year:2008 number:2 pages:m427-m428 https://doi.org/10.1107/S1600536808001633 kostenfrei https://doaj.org/article/b1faa5b5e23f4ee98ff164b0c6f9b743 kostenfrei http://scripts.iucr.org/cgi-bin/paper?S1600536808001633 kostenfrei https://doaj.org/toc/1600-5368 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_381 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 64 2008 2 m427-m428
language	English
source	In Acta Crystallographica Section E 64(2008), 2, Seite m427-m428 volume:64 year:2008 number:2 pages:m427-m428
sourceStr	In Acta Crystallographica Section E 64(2008), 2, Seite m427-m428 volume:64 year:2008 number:2 pages:m427-m428
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authorswithroles_txt_mv	Yu-Qiang Ding @@aut@@ Zhi-Qiang Liu @@aut@@ Bin Shen @@aut@@ Chun-Xia Ren @@aut@@ Hua Sun @@aut@@
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callnumber-first	Q - Science
author	Yu-Qiang Ding
spellingShingle	Yu-Qiang Ding misc QD901-999 misc Crystallography Bis[μ-1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene-κ2N3:N3′]silver(I) dinitrate dihydrate
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topic_title	QD901-999 Bis[μ-1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene-κ2N3:N3′]silver(I) dinitrate dihydrate
topic	misc QD901-999 misc Crystallography
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title	Bis[μ-1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene-κ2N3:N3′]silver(I) dinitrate dihydrate
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title_full	Bis[μ-1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene-κ2N3:N3′]silver(I) dinitrate dihydrate
author_sort	Yu-Qiang Ding
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title_sort	bis[μ-1,4-bis(4,5-dihydro-1h-imidazol-2-yl)benzene-κ2n3:n3′]silver(i) dinitrate dihydrate
callnumber	QD901-999
title_auth	Bis[μ-1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene-κ2N3:N3′]silver(I) dinitrate dihydrate
abstract	The reaction of 1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) with silver(I) nitrate in a 1:1 molar ratio generates the metallacyclic title complex, [Ag2(C12H14N4)2](NO3)2·2H2O, in which the bib ligand displays a cis configuration. Each bib ligand acts as a bidentate bridging ligand connecting a pair of AgI ions to form a [2 + 2] metallamacrocycle in which the Ag...Ag distance is 6.77 (2) Å. Each AgI ion has weak contacts (2.91 Å) with the nitrate anion. The uncoordinated water molecules make hydrogen bonds with nitrate O atoms, forming chains. The H atoms attached to the uncoordinated nitrogen interact with these chains through N—H...O hydrogen bonds, forming layers parallel to the (overline{1}11) plane.
abstractGer	The reaction of 1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) with silver(I) nitrate in a 1:1 molar ratio generates the metallacyclic title complex, [Ag2(C12H14N4)2](NO3)2·2H2O, in which the bib ligand displays a cis configuration. Each bib ligand acts as a bidentate bridging ligand connecting a pair of AgI ions to form a [2 + 2] metallamacrocycle in which the Ag...Ag distance is 6.77 (2) Å. Each AgI ion has weak contacts (2.91 Å) with the nitrate anion. The uncoordinated water molecules make hydrogen bonds with nitrate O atoms, forming chains. The H atoms attached to the uncoordinated nitrogen interact with these chains through N—H...O hydrogen bonds, forming layers parallel to the (overline{1}11) plane.
abstract_unstemmed	The reaction of 1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) with silver(I) nitrate in a 1:1 molar ratio generates the metallacyclic title complex, [Ag2(C12H14N4)2](NO3)2·2H2O, in which the bib ligand displays a cis configuration. Each bib ligand acts as a bidentate bridging ligand connecting a pair of AgI ions to form a [2 + 2] metallamacrocycle in which the Ag...Ag distance is 6.77 (2) Å. Each AgI ion has weak contacts (2.91 Å) with the nitrate anion. The uncoordinated water molecules make hydrogen bonds with nitrate O atoms, forming chains. The H atoms attached to the uncoordinated nitrogen interact with these chains through N—H...O hydrogen bonds, forming layers parallel to the (overline{1}11) plane.
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title_short	Bis[μ-1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene-κ2N3:N3′]silver(I) dinitrate dihydrate
url	https://doi.org/10.1107/S1600536808001633 https://doaj.org/article/b1faa5b5e23f4ee98ff164b0c6f9b743 http://scripts.iucr.org/cgi-bin/paper?S1600536808001633 https://doaj.org/toc/1600-5368
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up_date	2024-07-04T00:09:32.199Z
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Bis[μ-1,4-bis(4,5-dihydro-1H-imidazol-2-yl)benzene-κ2N3:N3′]silver(I) dinitrate dihydrate

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