High purity Al2O3 ceramic:Metallizing strategy, microstructure and sealing properties
ABSTRACTA high purity Al2O3 ceramic (HPAOC) metallizing strategy was developed via gradient coating process of metallizing pastes with different ratios of Mo to manganese glass (MnG) contents, to improve the wettability and reactivity of metallized layer (ML) to the ceramic substrate and the seconda...
Ausführliche Beschreibung
Autor*in: |
Dongcai Li [verfasserIn] Cangbao He [verfasserIn] Yong Sheng Wang [verfasserIn] Wei Su [verfasserIn] Fengjun Zhang [verfasserIn] Haiyan Xu [verfasserIn] |
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E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2023 |
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Übergeordnetes Werk: |
In: Journal of Asian Ceramic Societies - Taylor & Francis Group, 2015, (2023), Seite 10 |
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Übergeordnetes Werk: |
year:2023 ; pages:10 |
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DOI / URN: |
10.1080/21870764.2023.2195288 |
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Katalog-ID: |
DOAJ088846164 |
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520 | |a ABSTRACTA high purity Al2O3 ceramic (HPAOC) metallizing strategy was developed via gradient coating process of metallizing pastes with different ratios of Mo to manganese glass (MnG) contents, to improve the wettability and reactivity of metallized layer (ML) to the ceramic substrate and the secondary metallizing layer or sealed metals. Self-made HPAOC samples firstly coated by a layer of metallizing paste with a lower proportion of Mo:MnG and superposed a layer of metallizing paste with a higher proportion of Mo:MnG were fired at 1450°C in hydrogen atmosphere. The crystal phase structure, microstructure and element distribution of the metallized samples wer characterized by XRD, SEM and EDS. The results of sealing properties show that the tensile sealing strength of as high as 121MPa and the He leakage rate of as low as 4.2 × 10−11 Pa.m3/s can be obtained of the sealed joints of the as-metallized HPAOC and Kovar. | ||
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10.1080/21870764.2023.2195288 doi (DE-627)DOAJ088846164 (DE-599)DOAJd1817365977342d599e0b1e66bff1ef5 DE-627 ger DE-627 rakwb eng TP785-869 Dongcai Li verfasserin aut High purity Al2O3 ceramic:Metallizing strategy, microstructure and sealing properties 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier ABSTRACTA high purity Al2O3 ceramic (HPAOC) metallizing strategy was developed via gradient coating process of metallizing pastes with different ratios of Mo to manganese glass (MnG) contents, to improve the wettability and reactivity of metallized layer (ML) to the ceramic substrate and the secondary metallizing layer or sealed metals. Self-made HPAOC samples firstly coated by a layer of metallizing paste with a lower proportion of Mo:MnG and superposed a layer of metallizing paste with a higher proportion of Mo:MnG were fired at 1450°C in hydrogen atmosphere. The crystal phase structure, microstructure and element distribution of the metallized samples wer characterized by XRD, SEM and EDS. The results of sealing properties show that the tensile sealing strength of as high as 121MPa and the He leakage rate of as low as 4.2 × 10−11 Pa.m3/s can be obtained of the sealed joints of the as-metallized HPAOC and Kovar. High purity Al2O3 ceramic Manganese glass gradient coating process Metallizing,sealing Clay industries. Ceramics. Glass Cangbao He verfasserin aut Yong Sheng Wang verfasserin aut Wei Su verfasserin aut Fengjun Zhang verfasserin aut Haiyan Xu verfasserin aut In Journal of Asian Ceramic Societies Taylor & Francis Group, 2015 (2023), Seite 10 (DE-627)77685545X (DE-600)2751145-5 21870764 nnns year:2023 pages:10 https://doi.org/10.1080/21870764.2023.2195288 kostenfrei https://doaj.org/article/d1817365977342d599e0b1e66bff1ef5 kostenfrei https://www.tandfonline.com/doi/10.1080/21870764.2023.2195288 kostenfrei https://doaj.org/toc/2187-0764 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 2023 10 |
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10.1080/21870764.2023.2195288 doi (DE-627)DOAJ088846164 (DE-599)DOAJd1817365977342d599e0b1e66bff1ef5 DE-627 ger DE-627 rakwb eng TP785-869 Dongcai Li verfasserin aut High purity Al2O3 ceramic:Metallizing strategy, microstructure and sealing properties 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier ABSTRACTA high purity Al2O3 ceramic (HPAOC) metallizing strategy was developed via gradient coating process of metallizing pastes with different ratios of Mo to manganese glass (MnG) contents, to improve the wettability and reactivity of metallized layer (ML) to the ceramic substrate and the secondary metallizing layer or sealed metals. Self-made HPAOC samples firstly coated by a layer of metallizing paste with a lower proportion of Mo:MnG and superposed a layer of metallizing paste with a higher proportion of Mo:MnG were fired at 1450°C in hydrogen atmosphere. The crystal phase structure, microstructure and element distribution of the metallized samples wer characterized by XRD, SEM and EDS. The results of sealing properties show that the tensile sealing strength of as high as 121MPa and the He leakage rate of as low as 4.2 × 10−11 Pa.m3/s can be obtained of the sealed joints of the as-metallized HPAOC and Kovar. High purity Al2O3 ceramic Manganese glass gradient coating process Metallizing,sealing Clay industries. Ceramics. Glass Cangbao He verfasserin aut Yong Sheng Wang verfasserin aut Wei Su verfasserin aut Fengjun Zhang verfasserin aut Haiyan Xu verfasserin aut In Journal of Asian Ceramic Societies Taylor & Francis Group, 2015 (2023), Seite 10 (DE-627)77685545X (DE-600)2751145-5 21870764 nnns year:2023 pages:10 https://doi.org/10.1080/21870764.2023.2195288 kostenfrei https://doaj.org/article/d1817365977342d599e0b1e66bff1ef5 kostenfrei https://www.tandfonline.com/doi/10.1080/21870764.2023.2195288 kostenfrei https://doaj.org/toc/2187-0764 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 2023 10 |
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10.1080/21870764.2023.2195288 doi (DE-627)DOAJ088846164 (DE-599)DOAJd1817365977342d599e0b1e66bff1ef5 DE-627 ger DE-627 rakwb eng TP785-869 Dongcai Li verfasserin aut High purity Al2O3 ceramic:Metallizing strategy, microstructure and sealing properties 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier ABSTRACTA high purity Al2O3 ceramic (HPAOC) metallizing strategy was developed via gradient coating process of metallizing pastes with different ratios of Mo to manganese glass (MnG) contents, to improve the wettability and reactivity of metallized layer (ML) to the ceramic substrate and the secondary metallizing layer or sealed metals. Self-made HPAOC samples firstly coated by a layer of metallizing paste with a lower proportion of Mo:MnG and superposed a layer of metallizing paste with a higher proportion of Mo:MnG were fired at 1450°C in hydrogen atmosphere. The crystal phase structure, microstructure and element distribution of the metallized samples wer characterized by XRD, SEM and EDS. The results of sealing properties show that the tensile sealing strength of as high as 121MPa and the He leakage rate of as low as 4.2 × 10−11 Pa.m3/s can be obtained of the sealed joints of the as-metallized HPAOC and Kovar. High purity Al2O3 ceramic Manganese glass gradient coating process Metallizing,sealing Clay industries. Ceramics. Glass Cangbao He verfasserin aut Yong Sheng Wang verfasserin aut Wei Su verfasserin aut Fengjun Zhang verfasserin aut Haiyan Xu verfasserin aut In Journal of Asian Ceramic Societies Taylor & Francis Group, 2015 (2023), Seite 10 (DE-627)77685545X (DE-600)2751145-5 21870764 nnns year:2023 pages:10 https://doi.org/10.1080/21870764.2023.2195288 kostenfrei https://doaj.org/article/d1817365977342d599e0b1e66bff1ef5 kostenfrei https://www.tandfonline.com/doi/10.1080/21870764.2023.2195288 kostenfrei https://doaj.org/toc/2187-0764 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 2023 10 |
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10.1080/21870764.2023.2195288 doi (DE-627)DOAJ088846164 (DE-599)DOAJd1817365977342d599e0b1e66bff1ef5 DE-627 ger DE-627 rakwb eng TP785-869 Dongcai Li verfasserin aut High purity Al2O3 ceramic:Metallizing strategy, microstructure and sealing properties 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier ABSTRACTA high purity Al2O3 ceramic (HPAOC) metallizing strategy was developed via gradient coating process of metallizing pastes with different ratios of Mo to manganese glass (MnG) contents, to improve the wettability and reactivity of metallized layer (ML) to the ceramic substrate and the secondary metallizing layer or sealed metals. Self-made HPAOC samples firstly coated by a layer of metallizing paste with a lower proportion of Mo:MnG and superposed a layer of metallizing paste with a higher proportion of Mo:MnG were fired at 1450°C in hydrogen atmosphere. The crystal phase structure, microstructure and element distribution of the metallized samples wer characterized by XRD, SEM and EDS. The results of sealing properties show that the tensile sealing strength of as high as 121MPa and the He leakage rate of as low as 4.2 × 10−11 Pa.m3/s can be obtained of the sealed joints of the as-metallized HPAOC and Kovar. High purity Al2O3 ceramic Manganese glass gradient coating process Metallizing,sealing Clay industries. Ceramics. Glass Cangbao He verfasserin aut Yong Sheng Wang verfasserin aut Wei Su verfasserin aut Fengjun Zhang verfasserin aut Haiyan Xu verfasserin aut In Journal of Asian Ceramic Societies Taylor & Francis Group, 2015 (2023), Seite 10 (DE-627)77685545X (DE-600)2751145-5 21870764 nnns year:2023 pages:10 https://doi.org/10.1080/21870764.2023.2195288 kostenfrei https://doaj.org/article/d1817365977342d599e0b1e66bff1ef5 kostenfrei https://www.tandfonline.com/doi/10.1080/21870764.2023.2195288 kostenfrei https://doaj.org/toc/2187-0764 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 2023 10 |
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High purity Al2O3 ceramic:Metallizing strategy, microstructure and sealing properties |
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ABSTRACTA high purity Al2O3 ceramic (HPAOC) metallizing strategy was developed via gradient coating process of metallizing pastes with different ratios of Mo to manganese glass (MnG) contents, to improve the wettability and reactivity of metallized layer (ML) to the ceramic substrate and the secondary metallizing layer or sealed metals. Self-made HPAOC samples firstly coated by a layer of metallizing paste with a lower proportion of Mo:MnG and superposed a layer of metallizing paste with a higher proportion of Mo:MnG were fired at 1450°C in hydrogen atmosphere. The crystal phase structure, microstructure and element distribution of the metallized samples wer characterized by XRD, SEM and EDS. The results of sealing properties show that the tensile sealing strength of as high as 121MPa and the He leakage rate of as low as 4.2 × 10−11 Pa.m3/s can be obtained of the sealed joints of the as-metallized HPAOC and Kovar. |
abstractGer |
ABSTRACTA high purity Al2O3 ceramic (HPAOC) metallizing strategy was developed via gradient coating process of metallizing pastes with different ratios of Mo to manganese glass (MnG) contents, to improve the wettability and reactivity of metallized layer (ML) to the ceramic substrate and the secondary metallizing layer or sealed metals. Self-made HPAOC samples firstly coated by a layer of metallizing paste with a lower proportion of Mo:MnG and superposed a layer of metallizing paste with a higher proportion of Mo:MnG were fired at 1450°C in hydrogen atmosphere. The crystal phase structure, microstructure and element distribution of the metallized samples wer characterized by XRD, SEM and EDS. The results of sealing properties show that the tensile sealing strength of as high as 121MPa and the He leakage rate of as low as 4.2 × 10−11 Pa.m3/s can be obtained of the sealed joints of the as-metallized HPAOC and Kovar. |
abstract_unstemmed |
ABSTRACTA high purity Al2O3 ceramic (HPAOC) metallizing strategy was developed via gradient coating process of metallizing pastes with different ratios of Mo to manganese glass (MnG) contents, to improve the wettability and reactivity of metallized layer (ML) to the ceramic substrate and the secondary metallizing layer or sealed metals. Self-made HPAOC samples firstly coated by a layer of metallizing paste with a lower proportion of Mo:MnG and superposed a layer of metallizing paste with a higher proportion of Mo:MnG were fired at 1450°C in hydrogen atmosphere. The crystal phase structure, microstructure and element distribution of the metallized samples wer characterized by XRD, SEM and EDS. The results of sealing properties show that the tensile sealing strength of as high as 121MPa and the He leakage rate of as low as 4.2 × 10−11 Pa.m3/s can be obtained of the sealed joints of the as-metallized HPAOC and Kovar. |
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High purity Al2O3 ceramic:Metallizing strategy, microstructure and sealing properties |
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