Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol

In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with...
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Autor*in:	Thu Huong Nguyen Thi [verfasserIn] Jiřina Koutecká [verfasserIn] Pavel Kaule [verfasserIn] Luboš Vrtoch [verfasserIn] Václav Šícha [verfasserIn] Jan Čermák [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2023

Schlagwörter:	ionic liquids esterification catalysis sulfonic acid fatty acids bioethanol

Übergeordnetes Werk:	In: Molecules - MDPI AG, 2003, 28(2023), 13, p 5231
Übergeordnetes Werk:	volume:28 ; year:2023 ; number:13, p 5231

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/molecules28135231

Katalog-ID:	DOAJ093991959

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520			\|a In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with ethanol; heating in a microwave reactor was also used. The experimental results indicated that SAIL, with the lipophilic alkyl chain, performed the best due to its increased solubility in the reaction mixture. Microwave heating was found to be more effective than conventional heating. Recycling experiments show that these novel SAILs can be reused without significant loss of the catalytic activity.
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allfields	10.3390/molecules28135231 doi (DE-627)DOAJ093991959 (DE-599)DOAJea0833472aab4e67840b91de1beb0327 DE-627 ger DE-627 rakwb eng QD241-441 Thu Huong Nguyen Thi verfasserin aut Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with ethanol; heating in a microwave reactor was also used. The experimental results indicated that SAIL, with the lipophilic alkyl chain, performed the best due to its increased solubility in the reaction mixture. Microwave heating was found to be more effective than conventional heating. Recycling experiments show that these novel SAILs can be reused without significant loss of the catalytic activity. ionic liquids esterification catalysis sulfonic acid fatty acids bioethanol Organic chemistry Jiřina Koutecká verfasserin aut Pavel Kaule verfasserin aut Luboš Vrtoch verfasserin aut Václav Šícha verfasserin aut Jan Čermák verfasserin aut In Molecules MDPI AG, 2003 28(2023), 13, p 5231 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:28 year:2023 number:13, p 5231 https://doi.org/10.3390/molecules28135231 kostenfrei https://doaj.org/article/ea0833472aab4e67840b91de1beb0327 kostenfrei https://www.mdpi.com/1420-3049/28/13/5231 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 28 2023 13, p 5231
spelling	10.3390/molecules28135231 doi (DE-627)DOAJ093991959 (DE-599)DOAJea0833472aab4e67840b91de1beb0327 DE-627 ger DE-627 rakwb eng QD241-441 Thu Huong Nguyen Thi verfasserin aut Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with ethanol; heating in a microwave reactor was also used. The experimental results indicated that SAIL, with the lipophilic alkyl chain, performed the best due to its increased solubility in the reaction mixture. Microwave heating was found to be more effective than conventional heating. Recycling experiments show that these novel SAILs can be reused without significant loss of the catalytic activity. ionic liquids esterification catalysis sulfonic acid fatty acids bioethanol Organic chemistry Jiřina Koutecká verfasserin aut Pavel Kaule verfasserin aut Luboš Vrtoch verfasserin aut Václav Šícha verfasserin aut Jan Čermák verfasserin aut In Molecules MDPI AG, 2003 28(2023), 13, p 5231 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:28 year:2023 number:13, p 5231 https://doi.org/10.3390/molecules28135231 kostenfrei https://doaj.org/article/ea0833472aab4e67840b91de1beb0327 kostenfrei https://www.mdpi.com/1420-3049/28/13/5231 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 28 2023 13, p 5231
allfields_unstemmed	10.3390/molecules28135231 doi (DE-627)DOAJ093991959 (DE-599)DOAJea0833472aab4e67840b91de1beb0327 DE-627 ger DE-627 rakwb eng QD241-441 Thu Huong Nguyen Thi verfasserin aut Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with ethanol; heating in a microwave reactor was also used. The experimental results indicated that SAIL, with the lipophilic alkyl chain, performed the best due to its increased solubility in the reaction mixture. Microwave heating was found to be more effective than conventional heating. Recycling experiments show that these novel SAILs can be reused without significant loss of the catalytic activity. ionic liquids esterification catalysis sulfonic acid fatty acids bioethanol Organic chemistry Jiřina Koutecká verfasserin aut Pavel Kaule verfasserin aut Luboš Vrtoch verfasserin aut Václav Šícha verfasserin aut Jan Čermák verfasserin aut In Molecules MDPI AG, 2003 28(2023), 13, p 5231 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:28 year:2023 number:13, p 5231 https://doi.org/10.3390/molecules28135231 kostenfrei https://doaj.org/article/ea0833472aab4e67840b91de1beb0327 kostenfrei https://www.mdpi.com/1420-3049/28/13/5231 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 28 2023 13, p 5231
allfieldsGer	10.3390/molecules28135231 doi (DE-627)DOAJ093991959 (DE-599)DOAJea0833472aab4e67840b91de1beb0327 DE-627 ger DE-627 rakwb eng QD241-441 Thu Huong Nguyen Thi verfasserin aut Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with ethanol; heating in a microwave reactor was also used. The experimental results indicated that SAIL, with the lipophilic alkyl chain, performed the best due to its increased solubility in the reaction mixture. Microwave heating was found to be more effective than conventional heating. Recycling experiments show that these novel SAILs can be reused without significant loss of the catalytic activity. ionic liquids esterification catalysis sulfonic acid fatty acids bioethanol Organic chemistry Jiřina Koutecká verfasserin aut Pavel Kaule verfasserin aut Luboš Vrtoch verfasserin aut Václav Šícha verfasserin aut Jan Čermák verfasserin aut In Molecules MDPI AG, 2003 28(2023), 13, p 5231 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:28 year:2023 number:13, p 5231 https://doi.org/10.3390/molecules28135231 kostenfrei https://doaj.org/article/ea0833472aab4e67840b91de1beb0327 kostenfrei https://www.mdpi.com/1420-3049/28/13/5231 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 28 2023 13, p 5231
allfieldsSound	10.3390/molecules28135231 doi (DE-627)DOAJ093991959 (DE-599)DOAJea0833472aab4e67840b91de1beb0327 DE-627 ger DE-627 rakwb eng QD241-441 Thu Huong Nguyen Thi verfasserin aut Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with ethanol; heating in a microwave reactor was also used. The experimental results indicated that SAIL, with the lipophilic alkyl chain, performed the best due to its increased solubility in the reaction mixture. Microwave heating was found to be more effective than conventional heating. Recycling experiments show that these novel SAILs can be reused without significant loss of the catalytic activity. ionic liquids esterification catalysis sulfonic acid fatty acids bioethanol Organic chemistry Jiřina Koutecká verfasserin aut Pavel Kaule verfasserin aut Luboš Vrtoch verfasserin aut Václav Šícha verfasserin aut Jan Čermák verfasserin aut In Molecules MDPI AG, 2003 28(2023), 13, p 5231 (DE-627)311313132 (DE-600)2008644-1 14203049 nnns volume:28 year:2023 number:13, p 5231 https://doi.org/10.3390/molecules28135231 kostenfrei https://doaj.org/article/ea0833472aab4e67840b91de1beb0327 kostenfrei https://www.mdpi.com/1420-3049/28/13/5231 kostenfrei https://doaj.org/toc/1420-3049 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2111 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 28 2023 13, p 5231
language	English
source	In Molecules 28(2023), 13, p 5231 volume:28 year:2023 number:13, p 5231
sourceStr	In Molecules 28(2023), 13, p 5231 volume:28 year:2023 number:13, p 5231
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	ionic liquids esterification catalysis sulfonic acid fatty acids bioethanol Organic chemistry
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container_title	Molecules
authorswithroles_txt_mv	Thu Huong Nguyen Thi @@aut@@ Jiřina Koutecká @@aut@@ Pavel Kaule @@aut@@ Luboš Vrtoch @@aut@@ Václav Šícha @@aut@@ Jan Čermák @@aut@@
publishDateDaySort_date	2023-01-01T00:00:00Z
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callnumber-first	Q - Science
author	Thu Huong Nguyen Thi
spellingShingle	Thu Huong Nguyen Thi misc QD241-441 misc ionic liquids misc esterification catalysis misc sulfonic acid misc fatty acids misc bioethanol misc Organic chemistry Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol
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topic_title	QD241-441 Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol ionic liquids esterification catalysis sulfonic acid fatty acids bioethanol
topic	misc QD241-441 misc ionic liquids misc esterification catalysis misc sulfonic acid misc fatty acids misc bioethanol misc Organic chemistry
topic_unstemmed	misc QD241-441 misc ionic liquids misc esterification catalysis misc sulfonic acid misc fatty acids misc bioethanol misc Organic chemistry
topic_browse	misc QD241-441 misc ionic liquids misc esterification catalysis misc sulfonic acid misc fatty acids misc bioethanol misc Organic chemistry
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title	Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol
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title_full	Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol
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title_sort	design and synthesis of new sulfonic acid functionalized ionic liquids as catalysts for esterification of fatty acids with bioethanol
callnumber	QD241-441
title_auth	Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol
abstract	In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with ethanol; heating in a microwave reactor was also used. The experimental results indicated that SAIL, with the lipophilic alkyl chain, performed the best due to its increased solubility in the reaction mixture. Microwave heating was found to be more effective than conventional heating. Recycling experiments show that these novel SAILs can be reused without significant loss of the catalytic activity.
abstractGer	In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with ethanol; heating in a microwave reactor was also used. The experimental results indicated that SAIL, with the lipophilic alkyl chain, performed the best due to its increased solubility in the reaction mixture. Microwave heating was found to be more effective than conventional heating. Recycling experiments show that these novel SAILs can be reused without significant loss of the catalytic activity.
abstract_unstemmed	In this study, three types of sulfonic acid group functionalized ionic liquids (SAILs) with a different number of catalytic groups and lipophilicity were synthesized and characterized by FT-IR, NMR, and MS analyses. Their catalytic activities were studied in a model esterification of oleic acid with ethanol; heating in a microwave reactor was also used. The experimental results indicated that SAIL, with the lipophilic alkyl chain, performed the best due to its increased solubility in the reaction mixture. Microwave heating was found to be more effective than conventional heating. Recycling experiments show that these novel SAILs can be reused without significant loss of the catalytic activity.
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title_short	Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol
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Design and Synthesis of New Sulfonic Acid Functionalized Ionic Liquids as Catalysts for Esterification of Fatty Acids with Bioethanol

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