Analyses of Experimental Dental Adhesives Based on Zirconia/Silver Phosphate Nanoparticles
This study aimed to evaluate the incorporation of zirconia/silver phosphate nanoparticles to develop experimental dental adhesives and to measure their physical and mechanical properties. The nanoparticles were synthesized by the sonication method, and the phase purity, morphological pattern, and an...
Ausführliche Beschreibung
Autor*in: |
Abdul Samad Khan [verfasserIn] Yasmin Alhamdan [verfasserIn] Hala Alibrahim [verfasserIn] Khalid S. Almulhim [verfasserIn] Muhammad Nawaz [verfasserIn] Syed Zubairuddin Ahmed [verfasserIn] Khalid Aljuaid [verfasserIn] Ijlal Shahrukh Ateeq [verfasserIn] Sultan Akhtar [verfasserIn] Mohammad Azam Ansari [verfasserIn] Intisar Ahmad Siddiqui [verfasserIn] |
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E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2023 |
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Übergeordnetes Werk: |
In: Polymers - MDPI AG, 2011, 15(2023), 12, p 2614 |
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Übergeordnetes Werk: |
volume:15 ; year:2023 ; number:12, p 2614 |
Links: |
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DOI / URN: |
10.3390/polym15122614 |
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Katalog-ID: |
DOAJ094075212 |
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10.3390/polym15122614 doi (DE-627)DOAJ094075212 (DE-599)DOAJee3a7760e22548a2b7da8ee6c4f99e6a DE-627 ger DE-627 rakwb eng QD241-441 Abdul Samad Khan verfasserin aut Analyses of Experimental Dental Adhesives Based on Zirconia/Silver Phosphate Nanoparticles 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier This study aimed to evaluate the incorporation of zirconia/silver phosphate nanoparticles to develop experimental dental adhesives and to measure their physical and mechanical properties. The nanoparticles were synthesized by the sonication method, and the phase purity, morphological pattern, and antibacterial properties with <i<Staphylococcus aureus</i< and <i<Pseudomonas aeruginosa</i< were assessed. The silanized nanoparticles were incorporated (0, 0.15, 0.25, and 0.5 wt.%) into the photoactivated dimethacrylate resins. The degree of conversion (DC) was assessed, followed by the micro-hardness and flexural strength/modulus test. Long-term color stability was investigated. The bond strength with the dentin surface was conducted on days 1 and 30. The transmission electron microscopy and X-ray diffractogram confirmed the nano-structure and phase purity of the particles. The nanoparticles showed antibacterial activities against both strains and inhibited biofilm formation. The DC range of the experimental groups was 55–66%. The micro-hardness and flexural strength increased with the concentration of nanoparticles in the resin. The 0.5 wt.% group showed significantly high micro-hardness values, whereas a non-significant difference was observed between the experimental groups for flexural strength. The bond strength was higher on day 1 than on day 30, and a significant difference was observed between the two periods. At day 30, the 0.5 wt.% showed significantly higher values compared to other groups. Long-term color stability was observed for all the samples. The experimental adhesives showed promising results and potential to be used for clinical applications. However, further investigations such as antibacterial, penetration depth, and cytocompatibility are required. dental adhesives adhesion zirconia silver phosphate nanoparticles Organic chemistry Yasmin Alhamdan verfasserin aut Hala Alibrahim verfasserin aut Khalid S. Almulhim verfasserin aut Muhammad Nawaz verfasserin aut Syed Zubairuddin Ahmed verfasserin aut Khalid Aljuaid verfasserin aut Ijlal Shahrukh Ateeq verfasserin aut Sultan Akhtar verfasserin aut Mohammad Azam Ansari verfasserin aut Intisar Ahmad Siddiqui verfasserin aut In Polymers MDPI AG, 2011 15(2023), 12, p 2614 (DE-627)61409612X (DE-600)2527146-5 20734360 nnns volume:15 year:2023 number:12, p 2614 https://doi.org/10.3390/polym15122614 kostenfrei https://doaj.org/article/ee3a7760e22548a2b7da8ee6c4f99e6a kostenfrei https://www.mdpi.com/2073-4360/15/12/2614 kostenfrei https://doaj.org/toc/2073-4360 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2023 12, p 2614 |
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10.3390/polym15122614 doi (DE-627)DOAJ094075212 (DE-599)DOAJee3a7760e22548a2b7da8ee6c4f99e6a DE-627 ger DE-627 rakwb eng QD241-441 Abdul Samad Khan verfasserin aut Analyses of Experimental Dental Adhesives Based on Zirconia/Silver Phosphate Nanoparticles 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier This study aimed to evaluate the incorporation of zirconia/silver phosphate nanoparticles to develop experimental dental adhesives and to measure their physical and mechanical properties. The nanoparticles were synthesized by the sonication method, and the phase purity, morphological pattern, and antibacterial properties with <i<Staphylococcus aureus</i< and <i<Pseudomonas aeruginosa</i< were assessed. The silanized nanoparticles were incorporated (0, 0.15, 0.25, and 0.5 wt.%) into the photoactivated dimethacrylate resins. The degree of conversion (DC) was assessed, followed by the micro-hardness and flexural strength/modulus test. Long-term color stability was investigated. The bond strength with the dentin surface was conducted on days 1 and 30. The transmission electron microscopy and X-ray diffractogram confirmed the nano-structure and phase purity of the particles. The nanoparticles showed antibacterial activities against both strains and inhibited biofilm formation. The DC range of the experimental groups was 55–66%. The micro-hardness and flexural strength increased with the concentration of nanoparticles in the resin. The 0.5 wt.% group showed significantly high micro-hardness values, whereas a non-significant difference was observed between the experimental groups for flexural strength. The bond strength was higher on day 1 than on day 30, and a significant difference was observed between the two periods. At day 30, the 0.5 wt.% showed significantly higher values compared to other groups. Long-term color stability was observed for all the samples. The experimental adhesives showed promising results and potential to be used for clinical applications. However, further investigations such as antibacterial, penetration depth, and cytocompatibility are required. dental adhesives adhesion zirconia silver phosphate nanoparticles Organic chemistry Yasmin Alhamdan verfasserin aut Hala Alibrahim verfasserin aut Khalid S. Almulhim verfasserin aut Muhammad Nawaz verfasserin aut Syed Zubairuddin Ahmed verfasserin aut Khalid Aljuaid verfasserin aut Ijlal Shahrukh Ateeq verfasserin aut Sultan Akhtar verfasserin aut Mohammad Azam Ansari verfasserin aut Intisar Ahmad Siddiqui verfasserin aut In Polymers MDPI AG, 2011 15(2023), 12, p 2614 (DE-627)61409612X (DE-600)2527146-5 20734360 nnns volume:15 year:2023 number:12, p 2614 https://doi.org/10.3390/polym15122614 kostenfrei https://doaj.org/article/ee3a7760e22548a2b7da8ee6c4f99e6a kostenfrei https://www.mdpi.com/2073-4360/15/12/2614 kostenfrei https://doaj.org/toc/2073-4360 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2023 12, p 2614 |
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10.3390/polym15122614 doi (DE-627)DOAJ094075212 (DE-599)DOAJee3a7760e22548a2b7da8ee6c4f99e6a DE-627 ger DE-627 rakwb eng QD241-441 Abdul Samad Khan verfasserin aut Analyses of Experimental Dental Adhesives Based on Zirconia/Silver Phosphate Nanoparticles 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier This study aimed to evaluate the incorporation of zirconia/silver phosphate nanoparticles to develop experimental dental adhesives and to measure their physical and mechanical properties. The nanoparticles were synthesized by the sonication method, and the phase purity, morphological pattern, and antibacterial properties with <i<Staphylococcus aureus</i< and <i<Pseudomonas aeruginosa</i< were assessed. The silanized nanoparticles were incorporated (0, 0.15, 0.25, and 0.5 wt.%) into the photoactivated dimethacrylate resins. The degree of conversion (DC) was assessed, followed by the micro-hardness and flexural strength/modulus test. Long-term color stability was investigated. The bond strength with the dentin surface was conducted on days 1 and 30. The transmission electron microscopy and X-ray diffractogram confirmed the nano-structure and phase purity of the particles. The nanoparticles showed antibacterial activities against both strains and inhibited biofilm formation. The DC range of the experimental groups was 55–66%. The micro-hardness and flexural strength increased with the concentration of nanoparticles in the resin. The 0.5 wt.% group showed significantly high micro-hardness values, whereas a non-significant difference was observed between the experimental groups for flexural strength. The bond strength was higher on day 1 than on day 30, and a significant difference was observed between the two periods. At day 30, the 0.5 wt.% showed significantly higher values compared to other groups. Long-term color stability was observed for all the samples. The experimental adhesives showed promising results and potential to be used for clinical applications. However, further investigations such as antibacterial, penetration depth, and cytocompatibility are required. dental adhesives adhesion zirconia silver phosphate nanoparticles Organic chemistry Yasmin Alhamdan verfasserin aut Hala Alibrahim verfasserin aut Khalid S. Almulhim verfasserin aut Muhammad Nawaz verfasserin aut Syed Zubairuddin Ahmed verfasserin aut Khalid Aljuaid verfasserin aut Ijlal Shahrukh Ateeq verfasserin aut Sultan Akhtar verfasserin aut Mohammad Azam Ansari verfasserin aut Intisar Ahmad Siddiqui verfasserin aut In Polymers MDPI AG, 2011 15(2023), 12, p 2614 (DE-627)61409612X (DE-600)2527146-5 20734360 nnns volume:15 year:2023 number:12, p 2614 https://doi.org/10.3390/polym15122614 kostenfrei https://doaj.org/article/ee3a7760e22548a2b7da8ee6c4f99e6a kostenfrei https://www.mdpi.com/2073-4360/15/12/2614 kostenfrei https://doaj.org/toc/2073-4360 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2023 12, p 2614 |
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10.3390/polym15122614 doi (DE-627)DOAJ094075212 (DE-599)DOAJee3a7760e22548a2b7da8ee6c4f99e6a DE-627 ger DE-627 rakwb eng QD241-441 Abdul Samad Khan verfasserin aut Analyses of Experimental Dental Adhesives Based on Zirconia/Silver Phosphate Nanoparticles 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier This study aimed to evaluate the incorporation of zirconia/silver phosphate nanoparticles to develop experimental dental adhesives and to measure their physical and mechanical properties. The nanoparticles were synthesized by the sonication method, and the phase purity, morphological pattern, and antibacterial properties with <i<Staphylococcus aureus</i< and <i<Pseudomonas aeruginosa</i< were assessed. The silanized nanoparticles were incorporated (0, 0.15, 0.25, and 0.5 wt.%) into the photoactivated dimethacrylate resins. The degree of conversion (DC) was assessed, followed by the micro-hardness and flexural strength/modulus test. Long-term color stability was investigated. The bond strength with the dentin surface was conducted on days 1 and 30. The transmission electron microscopy and X-ray diffractogram confirmed the nano-structure and phase purity of the particles. The nanoparticles showed antibacterial activities against both strains and inhibited biofilm formation. The DC range of the experimental groups was 55–66%. The micro-hardness and flexural strength increased with the concentration of nanoparticles in the resin. The 0.5 wt.% group showed significantly high micro-hardness values, whereas a non-significant difference was observed between the experimental groups for flexural strength. The bond strength was higher on day 1 than on day 30, and a significant difference was observed between the two periods. At day 30, the 0.5 wt.% showed significantly higher values compared to other groups. Long-term color stability was observed for all the samples. The experimental adhesives showed promising results and potential to be used for clinical applications. However, further investigations such as antibacterial, penetration depth, and cytocompatibility are required. dental adhesives adhesion zirconia silver phosphate nanoparticles Organic chemistry Yasmin Alhamdan verfasserin aut Hala Alibrahim verfasserin aut Khalid S. Almulhim verfasserin aut Muhammad Nawaz verfasserin aut Syed Zubairuddin Ahmed verfasserin aut Khalid Aljuaid verfasserin aut Ijlal Shahrukh Ateeq verfasserin aut Sultan Akhtar verfasserin aut Mohammad Azam Ansari verfasserin aut Intisar Ahmad Siddiqui verfasserin aut In Polymers MDPI AG, 2011 15(2023), 12, p 2614 (DE-627)61409612X (DE-600)2527146-5 20734360 nnns volume:15 year:2023 number:12, p 2614 https://doi.org/10.3390/polym15122614 kostenfrei https://doaj.org/article/ee3a7760e22548a2b7da8ee6c4f99e6a kostenfrei https://www.mdpi.com/2073-4360/15/12/2614 kostenfrei https://doaj.org/toc/2073-4360 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2023 12, p 2614 |
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10.3390/polym15122614 doi (DE-627)DOAJ094075212 (DE-599)DOAJee3a7760e22548a2b7da8ee6c4f99e6a DE-627 ger DE-627 rakwb eng QD241-441 Abdul Samad Khan verfasserin aut Analyses of Experimental Dental Adhesives Based on Zirconia/Silver Phosphate Nanoparticles 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier This study aimed to evaluate the incorporation of zirconia/silver phosphate nanoparticles to develop experimental dental adhesives and to measure their physical and mechanical properties. The nanoparticles were synthesized by the sonication method, and the phase purity, morphological pattern, and antibacterial properties with <i<Staphylococcus aureus</i< and <i<Pseudomonas aeruginosa</i< were assessed. The silanized nanoparticles were incorporated (0, 0.15, 0.25, and 0.5 wt.%) into the photoactivated dimethacrylate resins. The degree of conversion (DC) was assessed, followed by the micro-hardness and flexural strength/modulus test. Long-term color stability was investigated. The bond strength with the dentin surface was conducted on days 1 and 30. The transmission electron microscopy and X-ray diffractogram confirmed the nano-structure and phase purity of the particles. The nanoparticles showed antibacterial activities against both strains and inhibited biofilm formation. The DC range of the experimental groups was 55–66%. The micro-hardness and flexural strength increased with the concentration of nanoparticles in the resin. The 0.5 wt.% group showed significantly high micro-hardness values, whereas a non-significant difference was observed between the experimental groups for flexural strength. The bond strength was higher on day 1 than on day 30, and a significant difference was observed between the two periods. At day 30, the 0.5 wt.% showed significantly higher values compared to other groups. Long-term color stability was observed for all the samples. The experimental adhesives showed promising results and potential to be used for clinical applications. However, further investigations such as antibacterial, penetration depth, and cytocompatibility are required. dental adhesives adhesion zirconia silver phosphate nanoparticles Organic chemistry Yasmin Alhamdan verfasserin aut Hala Alibrahim verfasserin aut Khalid S. Almulhim verfasserin aut Muhammad Nawaz verfasserin aut Syed Zubairuddin Ahmed verfasserin aut Khalid Aljuaid verfasserin aut Ijlal Shahrukh Ateeq verfasserin aut Sultan Akhtar verfasserin aut Mohammad Azam Ansari verfasserin aut Intisar Ahmad Siddiqui verfasserin aut In Polymers MDPI AG, 2011 15(2023), 12, p 2614 (DE-627)61409612X (DE-600)2527146-5 20734360 nnns volume:15 year:2023 number:12, p 2614 https://doi.org/10.3390/polym15122614 kostenfrei https://doaj.org/article/ee3a7760e22548a2b7da8ee6c4f99e6a kostenfrei https://www.mdpi.com/2073-4360/15/12/2614 kostenfrei https://doaj.org/toc/2073-4360 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 15 2023 12, p 2614 |
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Analyses of Experimental Dental Adhesives Based on Zirconia/Silver Phosphate Nanoparticles |
abstract |
This study aimed to evaluate the incorporation of zirconia/silver phosphate nanoparticles to develop experimental dental adhesives and to measure their physical and mechanical properties. The nanoparticles were synthesized by the sonication method, and the phase purity, morphological pattern, and antibacterial properties with <i<Staphylococcus aureus</i< and <i<Pseudomonas aeruginosa</i< were assessed. The silanized nanoparticles were incorporated (0, 0.15, 0.25, and 0.5 wt.%) into the photoactivated dimethacrylate resins. The degree of conversion (DC) was assessed, followed by the micro-hardness and flexural strength/modulus test. Long-term color stability was investigated. The bond strength with the dentin surface was conducted on days 1 and 30. The transmission electron microscopy and X-ray diffractogram confirmed the nano-structure and phase purity of the particles. The nanoparticles showed antibacterial activities against both strains and inhibited biofilm formation. The DC range of the experimental groups was 55–66%. The micro-hardness and flexural strength increased with the concentration of nanoparticles in the resin. The 0.5 wt.% group showed significantly high micro-hardness values, whereas a non-significant difference was observed between the experimental groups for flexural strength. The bond strength was higher on day 1 than on day 30, and a significant difference was observed between the two periods. At day 30, the 0.5 wt.% showed significantly higher values compared to other groups. Long-term color stability was observed for all the samples. The experimental adhesives showed promising results and potential to be used for clinical applications. However, further investigations such as antibacterial, penetration depth, and cytocompatibility are required. |
abstractGer |
This study aimed to evaluate the incorporation of zirconia/silver phosphate nanoparticles to develop experimental dental adhesives and to measure their physical and mechanical properties. The nanoparticles were synthesized by the sonication method, and the phase purity, morphological pattern, and antibacterial properties with <i<Staphylococcus aureus</i< and <i<Pseudomonas aeruginosa</i< were assessed. The silanized nanoparticles were incorporated (0, 0.15, 0.25, and 0.5 wt.%) into the photoactivated dimethacrylate resins. The degree of conversion (DC) was assessed, followed by the micro-hardness and flexural strength/modulus test. Long-term color stability was investigated. The bond strength with the dentin surface was conducted on days 1 and 30. The transmission electron microscopy and X-ray diffractogram confirmed the nano-structure and phase purity of the particles. The nanoparticles showed antibacterial activities against both strains and inhibited biofilm formation. The DC range of the experimental groups was 55–66%. The micro-hardness and flexural strength increased with the concentration of nanoparticles in the resin. The 0.5 wt.% group showed significantly high micro-hardness values, whereas a non-significant difference was observed between the experimental groups for flexural strength. The bond strength was higher on day 1 than on day 30, and a significant difference was observed between the two periods. At day 30, the 0.5 wt.% showed significantly higher values compared to other groups. Long-term color stability was observed for all the samples. The experimental adhesives showed promising results and potential to be used for clinical applications. However, further investigations such as antibacterial, penetration depth, and cytocompatibility are required. |
abstract_unstemmed |
This study aimed to evaluate the incorporation of zirconia/silver phosphate nanoparticles to develop experimental dental adhesives and to measure their physical and mechanical properties. The nanoparticles were synthesized by the sonication method, and the phase purity, morphological pattern, and antibacterial properties with <i<Staphylococcus aureus</i< and <i<Pseudomonas aeruginosa</i< were assessed. The silanized nanoparticles were incorporated (0, 0.15, 0.25, and 0.5 wt.%) into the photoactivated dimethacrylate resins. The degree of conversion (DC) was assessed, followed by the micro-hardness and flexural strength/modulus test. Long-term color stability was investigated. The bond strength with the dentin surface was conducted on days 1 and 30. The transmission electron microscopy and X-ray diffractogram confirmed the nano-structure and phase purity of the particles. The nanoparticles showed antibacterial activities against both strains and inhibited biofilm formation. The DC range of the experimental groups was 55–66%. The micro-hardness and flexural strength increased with the concentration of nanoparticles in the resin. The 0.5 wt.% group showed significantly high micro-hardness values, whereas a non-significant difference was observed between the experimental groups for flexural strength. The bond strength was higher on day 1 than on day 30, and a significant difference was observed between the two periods. At day 30, the 0.5 wt.% showed significantly higher values compared to other groups. Long-term color stability was observed for all the samples. The experimental adhesives showed promising results and potential to be used for clinical applications. However, further investigations such as antibacterial, penetration depth, and cytocompatibility are required. |
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container_issue |
12, p 2614 |
title_short |
Analyses of Experimental Dental Adhesives Based on Zirconia/Silver Phosphate Nanoparticles |
url |
https://doi.org/10.3390/polym15122614 https://doaj.org/article/ee3a7760e22548a2b7da8ee6c4f99e6a https://www.mdpi.com/2073-4360/15/12/2614 https://doaj.org/toc/2073-4360 |
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author2 |
Yasmin Alhamdan Hala Alibrahim Khalid S. Almulhim Muhammad Nawaz Syed Zubairuddin Ahmed Khalid Aljuaid Ijlal Shahrukh Ateeq Sultan Akhtar Mohammad Azam Ansari Intisar Ahmad Siddiqui |
author2Str |
Yasmin Alhamdan Hala Alibrahim Khalid S. Almulhim Muhammad Nawaz Syed Zubairuddin Ahmed Khalid Aljuaid Ijlal Shahrukh Ateeq Sultan Akhtar Mohammad Azam Ansari Intisar Ahmad Siddiqui |
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doi_str |
10.3390/polym15122614 |
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up_date |
2024-07-03T21:06:30.365Z |
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