Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications

An NbN coating was produced on AISI 316L steel using reactive DC magnetron sputtering. The effects of oxidation of the NbN coating in air on the microstructure, mechanical properties, corrosion resistance, contact angle and bioactivity were investigated. Phase composition was determined using X-ray...
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Gespeichert in:

Autor*in:	Tomasz Borowski [verfasserIn] Justyna Rospondek [verfasserIn] Marek Betiuk [verfasserIn] Bogusława Adamczyk-Cieślak [verfasserIn] Maciej Spychalski [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2023

Schlagwörter:	NbN Nb magnetron sputtering oxidising SBF microstructure

Übergeordnetes Werk:	In: Materials - MDPI AG, 2009, 16(2023), 21, p 6890
Übergeordnetes Werk:	volume:16 ; year:2023 ; number:21, p 6890

Links:	Link aufrufen Link aufrufen Link aufrufen Journal toc

DOI / URN:	10.3390/ma16216890

Katalog-ID:	DOAJ095454365

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allfields	10.3390/ma16216890 doi (DE-627)DOAJ095454365 (DE-599)DOAJ2a90a4dd46664c98b79a542f9eb11557 DE-627 ger DE-627 rakwb eng TK1-9971 TA1-2040 QH201-278.5 QC120-168.85 Tomasz Borowski verfasserin aut Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier An NbN coating was produced on AISI 316L steel using reactive DC magnetron sputtering. The effects of oxidation of the NbN coating in air on the microstructure, mechanical properties, corrosion resistance, contact angle and bioactivity were investigated. Phase composition was determined using X-ray diffraction (XRD), the coatings’ cross-sectional microstructure and thickness including surface morphology using a scanning electron microscope (SEM), microhardness via the Vickers method, corrosion by means of a potentiodynamic polarisation test in Ringer’s solution and bioactivity by observation in an SBF solution, while the contact angle was studied using a goniometer. The NbN coating and the oxidised coating were shown to demonstrate a Ca/P ratio close to that of hydroxyapatite, as well as increased microhardness and corrosion resistance. The best combination of mechanical, corrosion, bioactivity and hydrophilic properties was demonstrated by the air oxidised NbN coating, which featured an orthorhombic Nb<sub<2</sub<O<sub<5</sub< structure in the top, surface layer. NbN Nb<sub<2</sub<O<sub<5</sub< magnetron sputtering oxidising SBF microstructure Technology T Electrical engineering. Electronics. Nuclear engineering Engineering (General). Civil engineering (General) Microscopy Descriptive and experimental mechanics Justyna Rospondek verfasserin aut Marek Betiuk verfasserin aut Bogusława Adamczyk-Cieślak verfasserin aut Maciej Spychalski verfasserin aut In Materials MDPI AG, 2009 16(2023), 21, p 6890 (DE-627)595712649 (DE-600)2487261-1 19961944 nnns volume:16 year:2023 number:21, p 6890 https://doi.org/10.3390/ma16216890 kostenfrei https://doaj.org/article/2a90a4dd46664c98b79a542f9eb11557 kostenfrei https://www.mdpi.com/1996-1944/16/21/6890 kostenfrei https://doaj.org/toc/1996-1944 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 16 2023 21, p 6890
spelling	10.3390/ma16216890 doi (DE-627)DOAJ095454365 (DE-599)DOAJ2a90a4dd46664c98b79a542f9eb11557 DE-627 ger DE-627 rakwb eng TK1-9971 TA1-2040 QH201-278.5 QC120-168.85 Tomasz Borowski verfasserin aut Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier An NbN coating was produced on AISI 316L steel using reactive DC magnetron sputtering. The effects of oxidation of the NbN coating in air on the microstructure, mechanical properties, corrosion resistance, contact angle and bioactivity were investigated. Phase composition was determined using X-ray diffraction (XRD), the coatings’ cross-sectional microstructure and thickness including surface morphology using a scanning electron microscope (SEM), microhardness via the Vickers method, corrosion by means of a potentiodynamic polarisation test in Ringer’s solution and bioactivity by observation in an SBF solution, while the contact angle was studied using a goniometer. The NbN coating and the oxidised coating were shown to demonstrate a Ca/P ratio close to that of hydroxyapatite, as well as increased microhardness and corrosion resistance. The best combination of mechanical, corrosion, bioactivity and hydrophilic properties was demonstrated by the air oxidised NbN coating, which featured an orthorhombic Nb<sub<2</sub<O<sub<5</sub< structure in the top, surface layer. NbN Nb<sub<2</sub<O<sub<5</sub< magnetron sputtering oxidising SBF microstructure Technology T Electrical engineering. Electronics. Nuclear engineering Engineering (General). Civil engineering (General) Microscopy Descriptive and experimental mechanics Justyna Rospondek verfasserin aut Marek Betiuk verfasserin aut Bogusława Adamczyk-Cieślak verfasserin aut Maciej Spychalski verfasserin aut In Materials MDPI AG, 2009 16(2023), 21, p 6890 (DE-627)595712649 (DE-600)2487261-1 19961944 nnns volume:16 year:2023 number:21, p 6890 https://doi.org/10.3390/ma16216890 kostenfrei https://doaj.org/article/2a90a4dd46664c98b79a542f9eb11557 kostenfrei https://www.mdpi.com/1996-1944/16/21/6890 kostenfrei https://doaj.org/toc/1996-1944 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 16 2023 21, p 6890
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allfieldsSound	10.3390/ma16216890 doi (DE-627)DOAJ095454365 (DE-599)DOAJ2a90a4dd46664c98b79a542f9eb11557 DE-627 ger DE-627 rakwb eng TK1-9971 TA1-2040 QH201-278.5 QC120-168.85 Tomasz Borowski verfasserin aut Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier An NbN coating was produced on AISI 316L steel using reactive DC magnetron sputtering. The effects of oxidation of the NbN coating in air on the microstructure, mechanical properties, corrosion resistance, contact angle and bioactivity were investigated. Phase composition was determined using X-ray diffraction (XRD), the coatings’ cross-sectional microstructure and thickness including surface morphology using a scanning electron microscope (SEM), microhardness via the Vickers method, corrosion by means of a potentiodynamic polarisation test in Ringer’s solution and bioactivity by observation in an SBF solution, while the contact angle was studied using a goniometer. The NbN coating and the oxidised coating were shown to demonstrate a Ca/P ratio close to that of hydroxyapatite, as well as increased microhardness and corrosion resistance. The best combination of mechanical, corrosion, bioactivity and hydrophilic properties was demonstrated by the air oxidised NbN coating, which featured an orthorhombic Nb<sub<2</sub<O<sub<5</sub< structure in the top, surface layer. NbN Nb<sub<2</sub<O<sub<5</sub< magnetron sputtering oxidising SBF microstructure Technology T Electrical engineering. Electronics. Nuclear engineering Engineering (General). Civil engineering (General) Microscopy Descriptive and experimental mechanics Justyna Rospondek verfasserin aut Marek Betiuk verfasserin aut Bogusława Adamczyk-Cieślak verfasserin aut Maciej Spychalski verfasserin aut In Materials MDPI AG, 2009 16(2023), 21, p 6890 (DE-627)595712649 (DE-600)2487261-1 19961944 nnns volume:16 year:2023 number:21, p 6890 https://doi.org/10.3390/ma16216890 kostenfrei https://doaj.org/article/2a90a4dd46664c98b79a542f9eb11557 kostenfrei https://www.mdpi.com/1996-1944/16/21/6890 kostenfrei https://doaj.org/toc/1996-1944 Journal toc kostenfrei GBV_USEFLAG_A SYSFLAG_A GBV_DOAJ GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_206 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 16 2023 21, p 6890
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callnumber-first	T - Technology
author	Tomasz Borowski
spellingShingle	Tomasz Borowski misc TK1-9971 misc TA1-2040 misc QH201-278.5 misc QC120-168.85 misc NbN misc Nb<sub<2</sub<O<sub<5</sub< misc magnetron sputtering misc oxidising misc SBF misc microstructure misc Technology misc T misc Electrical engineering. Electronics. Nuclear engineering misc Engineering (General). Civil engineering (General) misc Microscopy misc Descriptive and experimental mechanics Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications
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topic_title	TK1-9971 TA1-2040 QH201-278.5 QC120-168.85 Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications NbN Nb<sub<2</sub<O<sub<5</sub< magnetron sputtering oxidising SBF microstructure
topic	misc TK1-9971 misc TA1-2040 misc QH201-278.5 misc QC120-168.85 misc NbN misc Nb<sub<2</sub<O<sub<5</sub< misc magnetron sputtering misc oxidising misc SBF misc microstructure misc Technology misc T misc Electrical engineering. Electronics. Nuclear engineering misc Engineering (General). Civil engineering (General) misc Microscopy misc Descriptive and experimental mechanics
topic_unstemmed	misc TK1-9971 misc TA1-2040 misc QH201-278.5 misc QC120-168.85 misc NbN misc Nb<sub<2</sub<O<sub<5</sub< misc magnetron sputtering misc oxidising misc SBF misc microstructure misc Technology misc T misc Electrical engineering. Electronics. Nuclear engineering misc Engineering (General). Civil engineering (General) misc Microscopy misc Descriptive and experimental mechanics
topic_browse	misc TK1-9971 misc TA1-2040 misc QH201-278.5 misc QC120-168.85 misc NbN misc Nb<sub<2</sub<O<sub<5</sub< misc magnetron sputtering misc oxidising misc SBF misc microstructure misc Technology misc T misc Electrical engineering. Electronics. Nuclear engineering misc Engineering (General). Civil engineering (General) misc Microscopy misc Descriptive and experimental mechanics
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title	Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications
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title_full	Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications
author_sort	Tomasz Borowski
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author_browse	Tomasz Borowski Justyna Rospondek Marek Betiuk Bogusława Adamczyk-Cieślak Maciej Spychalski
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title_sort	influence of magnetron sputtering-deposited niobium nitride coating and its thermal oxidation on the properties of aisi 316l steel in terms of its medical applications
callnumber	TK1-9971
title_auth	Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications
abstract	An NbN coating was produced on AISI 316L steel using reactive DC magnetron sputtering. The effects of oxidation of the NbN coating in air on the microstructure, mechanical properties, corrosion resistance, contact angle and bioactivity were investigated. Phase composition was determined using X-ray diffraction (XRD), the coatings’ cross-sectional microstructure and thickness including surface morphology using a scanning electron microscope (SEM), microhardness via the Vickers method, corrosion by means of a potentiodynamic polarisation test in Ringer’s solution and bioactivity by observation in an SBF solution, while the contact angle was studied using a goniometer. The NbN coating and the oxidised coating were shown to demonstrate a Ca/P ratio close to that of hydroxyapatite, as well as increased microhardness and corrosion resistance. The best combination of mechanical, corrosion, bioactivity and hydrophilic properties was demonstrated by the air oxidised NbN coating, which featured an orthorhombic Nb<sub<2</sub<O<sub<5</sub< structure in the top, surface layer.
abstractGer	An NbN coating was produced on AISI 316L steel using reactive DC magnetron sputtering. The effects of oxidation of the NbN coating in air on the microstructure, mechanical properties, corrosion resistance, contact angle and bioactivity were investigated. Phase composition was determined using X-ray diffraction (XRD), the coatings’ cross-sectional microstructure and thickness including surface morphology using a scanning electron microscope (SEM), microhardness via the Vickers method, corrosion by means of a potentiodynamic polarisation test in Ringer’s solution and bioactivity by observation in an SBF solution, while the contact angle was studied using a goniometer. The NbN coating and the oxidised coating were shown to demonstrate a Ca/P ratio close to that of hydroxyapatite, as well as increased microhardness and corrosion resistance. The best combination of mechanical, corrosion, bioactivity and hydrophilic properties was demonstrated by the air oxidised NbN coating, which featured an orthorhombic Nb<sub<2</sub<O<sub<5</sub< structure in the top, surface layer.
abstract_unstemmed	An NbN coating was produced on AISI 316L steel using reactive DC magnetron sputtering. The effects of oxidation of the NbN coating in air on the microstructure, mechanical properties, corrosion resistance, contact angle and bioactivity were investigated. Phase composition was determined using X-ray diffraction (XRD), the coatings’ cross-sectional microstructure and thickness including surface morphology using a scanning electron microscope (SEM), microhardness via the Vickers method, corrosion by means of a potentiodynamic polarisation test in Ringer’s solution and bioactivity by observation in an SBF solution, while the contact angle was studied using a goniometer. The NbN coating and the oxidised coating were shown to demonstrate a Ca/P ratio close to that of hydroxyapatite, as well as increased microhardness and corrosion resistance. The best combination of mechanical, corrosion, bioactivity and hydrophilic properties was demonstrated by the air oxidised NbN coating, which featured an orthorhombic Nb<sub<2</sub<O<sub<5</sub< structure in the top, surface layer.
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title_short	Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications
url	https://doi.org/10.3390/ma16216890 https://doaj.org/article/2a90a4dd46664c98b79a542f9eb11557 https://www.mdpi.com/1996-1944/16/21/6890 https://doaj.org/toc/1996-1944
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up_date	2024-07-03T14:45:29.844Z
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Influence of Magnetron Sputtering-Deposited Niobium Nitride Coating and Its Thermal Oxidation on the Properties of AISI 316L Steel in Terms of Its Medical Applications

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