A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements

Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering te...
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Autor*in:	Kagaya, Shigehiro [verfasserIn] Katoh, Toshifumi [verfasserIn] Saito, Mitsuru [verfasserIn] Ohki, Mayu [verfasserIn] Shirota, Riko [verfasserIn] Saeki, Yumi [verfasserIn] Kajiwara, Takehiro [verfasserIn] Nakada, Saori [verfasserIn] Miyazaki, Hiroyuki [verfasserIn] Gemmei-Ide, Makoto [verfasserIn] Inoue, Yoshinori [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2018

Schlagwörter:	Sintered material Presep PolyChelate Particulate polyethylene Solid-phase extraction Trace elements

Übergeordnetes Werk:	Enthalten in: Talanta - Amsterdam [u.a.] : Elsevier Science, 1958, 188, Seite 665-670
Übergeordnetes Werk:	volume:188 ; pages:665-670

DOI / URN:	10.1016/j.talanta.2018.06.024

Katalog-ID:	ELV000047384

Internformat


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100	1		\|a Kagaya, Shigehiro \|e verfasserin \|4 aut
245	1	0	\|a A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements
264		1	\|c 2018
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520			\|a Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering technique. The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. The method was applicable to analyses of certified reference materials (EnviroMAT ES-L-1 ground water and EU-L-3 waste water) and a commercially available table salt.
650		4	\|a Sintered material
650		4	\|a Presep PolyChelate
650		4	\|a Particulate polyethylene
650		4	\|a Solid-phase extraction
650		4	\|a Trace elements
700	1		\|a Katoh, Toshifumi \|e verfasserin \|4 aut
700	1		\|a Saito, Mitsuru \|e verfasserin \|4 aut
700	1		\|a Ohki, Mayu \|e verfasserin \|4 aut
700	1		\|a Shirota, Riko \|e verfasserin \|4 aut
700	1		\|a Saeki, Yumi \|e verfasserin \|4 aut
700	1		\|a Kajiwara, Takehiro \|e verfasserin \|4 aut
700	1		\|a Nakada, Saori \|e verfasserin \|4 aut
700	1		\|a Miyazaki, Hiroyuki \|e verfasserin \|4 aut
700	1		\|a Gemmei-Ide, Makoto \|e verfasserin \|4 aut
700	1		\|a Inoue, Yoshinori \|e verfasserin \|4 aut
773	0	8	\|i Enthalten in \|t Talanta \|d Amsterdam [u.a.] : Elsevier Science, 1958 \|g 188, Seite 665-670 \|h Online-Ressource \|w (DE-627)306712571 \|w (DE-600)1500969-5 \|w (DE-576)251938158 \|x 1873-3573 \|7 nnns
773	1	8	\|g volume:188 \|g pages:665-670
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912			\|a GBV_ILN_4338
912			\|a GBV_ILN_4393
936	b	k	\|a 35.00 \|j Chemie: Allgemeines
951			\|a AR
952			\|d 188 \|h 665-670

Indexfelder

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allfields	10.1016/j.talanta.2018.06.024 doi (DE-627)ELV000047384 (ELSEVIER)S0039-9140(18)30629-5 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Kagaya, Shigehiro verfasserin aut A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering technique. The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. The method was applicable to analyses of certified reference materials (EnviroMAT ES-L-1 ground water and EU-L-3 waste water) and a commercially available table salt. Sintered material Presep PolyChelate Particulate polyethylene Solid-phase extraction Trace elements Katoh, Toshifumi verfasserin aut Saito, Mitsuru verfasserin aut Ohki, Mayu verfasserin aut Shirota, Riko verfasserin aut Saeki, Yumi verfasserin aut Kajiwara, Takehiro verfasserin aut Nakada, Saori verfasserin aut Miyazaki, Hiroyuki verfasserin aut Gemmei-Ide, Makoto verfasserin aut Inoue, Yoshinori verfasserin aut Enthalten in Talanta Amsterdam [u.a.] : Elsevier Science, 1958 188, Seite 665-670 Online-Ressource (DE-627)306712571 (DE-600)1500969-5 (DE-576)251938158 1873-3573 nnns volume:188 pages:665-670 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 188 665-670
spelling	10.1016/j.talanta.2018.06.024 doi (DE-627)ELV000047384 (ELSEVIER)S0039-9140(18)30629-5 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Kagaya, Shigehiro verfasserin aut A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering technique. The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. The method was applicable to analyses of certified reference materials (EnviroMAT ES-L-1 ground water and EU-L-3 waste water) and a commercially available table salt. Sintered material Presep PolyChelate Particulate polyethylene Solid-phase extraction Trace elements Katoh, Toshifumi verfasserin aut Saito, Mitsuru verfasserin aut Ohki, Mayu verfasserin aut Shirota, Riko verfasserin aut Saeki, Yumi verfasserin aut Kajiwara, Takehiro verfasserin aut Nakada, Saori verfasserin aut Miyazaki, Hiroyuki verfasserin aut Gemmei-Ide, Makoto verfasserin aut Inoue, Yoshinori verfasserin aut Enthalten in Talanta Amsterdam [u.a.] : Elsevier Science, 1958 188, Seite 665-670 Online-Ressource (DE-627)306712571 (DE-600)1500969-5 (DE-576)251938158 1873-3573 nnns volume:188 pages:665-670 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 188 665-670
allfields_unstemmed	10.1016/j.talanta.2018.06.024 doi (DE-627)ELV000047384 (ELSEVIER)S0039-9140(18)30629-5 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Kagaya, Shigehiro verfasserin aut A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering technique. The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. The method was applicable to analyses of certified reference materials (EnviroMAT ES-L-1 ground water and EU-L-3 waste water) and a commercially available table salt. Sintered material Presep PolyChelate Particulate polyethylene Solid-phase extraction Trace elements Katoh, Toshifumi verfasserin aut Saito, Mitsuru verfasserin aut Ohki, Mayu verfasserin aut Shirota, Riko verfasserin aut Saeki, Yumi verfasserin aut Kajiwara, Takehiro verfasserin aut Nakada, Saori verfasserin aut Miyazaki, Hiroyuki verfasserin aut Gemmei-Ide, Makoto verfasserin aut Inoue, Yoshinori verfasserin aut Enthalten in Talanta Amsterdam [u.a.] : Elsevier Science, 1958 188, Seite 665-670 Online-Ressource (DE-627)306712571 (DE-600)1500969-5 (DE-576)251938158 1873-3573 nnns volume:188 pages:665-670 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 188 665-670
allfieldsGer	10.1016/j.talanta.2018.06.024 doi (DE-627)ELV000047384 (ELSEVIER)S0039-9140(18)30629-5 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Kagaya, Shigehiro verfasserin aut A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering technique. The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. The method was applicable to analyses of certified reference materials (EnviroMAT ES-L-1 ground water and EU-L-3 waste water) and a commercially available table salt. Sintered material Presep PolyChelate Particulate polyethylene Solid-phase extraction Trace elements Katoh, Toshifumi verfasserin aut Saito, Mitsuru verfasserin aut Ohki, Mayu verfasserin aut Shirota, Riko verfasserin aut Saeki, Yumi verfasserin aut Kajiwara, Takehiro verfasserin aut Nakada, Saori verfasserin aut Miyazaki, Hiroyuki verfasserin aut Gemmei-Ide, Makoto verfasserin aut Inoue, Yoshinori verfasserin aut Enthalten in Talanta Amsterdam [u.a.] : Elsevier Science, 1958 188, Seite 665-670 Online-Ressource (DE-627)306712571 (DE-600)1500969-5 (DE-576)251938158 1873-3573 nnns volume:188 pages:665-670 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 188 665-670
allfieldsSound	10.1016/j.talanta.2018.06.024 doi (DE-627)ELV000047384 (ELSEVIER)S0039-9140(18)30629-5 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Kagaya, Shigehiro verfasserin aut A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering technique. The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. The method was applicable to analyses of certified reference materials (EnviroMAT ES-L-1 ground water and EU-L-3 waste water) and a commercially available table salt. Sintered material Presep PolyChelate Particulate polyethylene Solid-phase extraction Trace elements Katoh, Toshifumi verfasserin aut Saito, Mitsuru verfasserin aut Ohki, Mayu verfasserin aut Shirota, Riko verfasserin aut Saeki, Yumi verfasserin aut Kajiwara, Takehiro verfasserin aut Nakada, Saori verfasserin aut Miyazaki, Hiroyuki verfasserin aut Gemmei-Ide, Makoto verfasserin aut Inoue, Yoshinori verfasserin aut Enthalten in Talanta Amsterdam [u.a.] : Elsevier Science, 1958 188, Seite 665-670 Online-Ressource (DE-627)306712571 (DE-600)1500969-5 (DE-576)251938158 1873-3573 nnns volume:188 pages:665-670 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 188 665-670
language	English
source	Enthalten in Talanta 188, Seite 665-670 volume:188 pages:665-670
sourceStr	Enthalten in Talanta 188, Seite 665-670 volume:188 pages:665-670
format_phy_str_mv	Article
bklname	Chemie: Allgemeines
institution	findex.gbv.de
topic_facet	Sintered material Presep PolyChelate Particulate polyethylene Solid-phase extraction Trace elements
dewey-raw	540
isfreeaccess_bool	false
container_title	Talanta
authorswithroles_txt_mv	Kagaya, Shigehiro @@aut@@ Katoh, Toshifumi @@aut@@ Saito, Mitsuru @@aut@@ Ohki, Mayu @@aut@@ Shirota, Riko @@aut@@ Saeki, Yumi @@aut@@ Kajiwara, Takehiro @@aut@@ Nakada, Saori @@aut@@ Miyazaki, Hiroyuki @@aut@@ Gemmei-Ide, Makoto @@aut@@ Inoue, Yoshinori @@aut@@
publishDateDaySort_date	2018-01-01T00:00:00Z
hierarchy_top_id	306712571
dewey-sort	3540
id	ELV000047384
language_de	englisch
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author	Kagaya, Shigehiro
spellingShingle	Kagaya, Shigehiro ddc 540 bkl 35.00 misc Sintered material misc Presep PolyChelate misc Particulate polyethylene misc Solid-phase extraction misc Trace elements A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements
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topic_title	540 DE-600 35.00 bkl A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements Sintered material Presep PolyChelate Particulate polyethylene Solid-phase extraction Trace elements
topic	ddc 540 bkl 35.00 misc Sintered material misc Presep PolyChelate misc Particulate polyethylene misc Solid-phase extraction misc Trace elements
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title	A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements
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title_full	A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements
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author_browse	Kagaya, Shigehiro Katoh, Toshifumi Saito, Mitsuru Ohki, Mayu Shirota, Riko Saeki, Yumi Kajiwara, Takehiro Nakada, Saori Miyazaki, Hiroyuki Gemmei-Ide, Makoto Inoue, Yoshinori
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title_sort	a porous sintered material consisting of presep polychelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements
title_auth	A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements
abstract	Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering technique. The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. The method was applicable to analyses of certified reference materials (EnviroMAT ES-L-1 ground water and EU-L-3 waste water) and a commercially available table salt.
abstractGer	Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering technique. The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. The method was applicable to analyses of certified reference materials (EnviroMAT ES-L-1 ground water and EU-L-3 waste water) and a commercially available table salt.
abstract_unstemmed	Cylinder-type and disk-type sintered materials consisting of Presep PolyChelate, which is a commercially available chelating resin immobilizing carboxymethylated polyethyleneimine as a functional group, and particulate polyethylene as a thermoplastic binder were prepared using a polymer sintering technique. The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. The method was applicable to analyses of certified reference materials (EnviroMAT ES-L-1 ground water and EU-L-3 waste water) and a commercially available table salt.
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title_short	A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements
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author2	Katoh, Toshifumi Saito, Mitsuru Ohki, Mayu Shirota, Riko Saeki, Yumi Kajiwara, Takehiro Nakada, Saori Miyazaki, Hiroyuki Gemmei-Ide, Makoto Inoue, Yoshinori
author2Str	Katoh, Toshifumi Saito, Mitsuru Ohki, Mayu Shirota, Riko Saeki, Yumi Kajiwara, Takehiro Nakada, Saori Miyazaki, Hiroyuki Gemmei-Ide, Makoto Inoue, Yoshinori
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up_date	2024-07-06T16:41:26.483Z
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The sintered materials had a continuously porous structure. The sintering process at 130 °C for 20 min did not affect the ability of the chelating resin in the sintered materials; the selectivity of the sintered material was almost the same as that of the particulate chelating resin which was not sintered. The sintering materials could quantitatively extract 11 kinds of trace elements, namely Cd, Co, Cu, Fe, Mn, Mo, Ni, Pb, Ti, V, and Zn, at pH 5.5. When the disk-type sintered material was used, the recoveries of these elements remained almost constant at a flow rate of at least 50 mL min−1; the extracted elements could be eluted using 10 mL of 3 mol L−1 nitric acid at a flow rate of 5 mL min−1. Solid-phase extraction using the disk-type sintered material was applied to the separation and preconcentration of trace elements prior to their inductively coupled plasma atomic emission spectrometric determination. 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A porous sintered material consisting of Presep PolyChelate as a chelating resin and particulate polyethylene as a thermoplastic binder for solid-phase extraction of trace elements

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