Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes
13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of th...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Forman, Evan M. [verfasserIn] Baniani, Amineh [verfasserIn] Fan, Lei [verfasserIn] Ziegler, Kirk J. [verfasserIn] Zhou, Erkang [verfasserIn] Zhang, Fengyi [verfasserIn] Lively, Ryan P. [verfasserIn] Vasenkov, Sergey [verfasserIn] |
|---|
| Format: |
E-Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
2018 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Microporous and mesoporous materials - Amsterdam [u.a.] : Elsevier, 1998, 274, Seite 163-170 |
|---|---|
| Übergeordnetes Werk: |
volume:274 ; pages:163-170 |
| DOI / URN: |
10.1016/j.micromeso.2018.07.044 |
|---|
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ELV000998893 |
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| 245 | 1 | 0 | |a Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes |
| 264 | 1 | |c 2018 | |
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| 520 | |a 13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of the following three polymers: Torlon, Matrimid, and 6FDA-DAM. PFG NMR data allowed obtaining ethylene diffusivities inside ZIF-11 crystals in the crystal beds and MMMs under the same or similar conditions. It was observed that the intra-ZIF diffusivities in ZIF-11/Torlon MMM are smaller than the corresponding diffusivities in the ZIF-11 bed. The observed diffusivity reduction becomes less significant with increasing ethylene loading. At the same time, within uncertainty, no difference in the intra-ZIF diffusivities between ZIF-11 bed and MMMs were observed for ZIF-11/Matrimid and ZIF-11/6FDA-DAM MMMs. The intra-ZIF diffusivity reduction observed for ZIF-11/Torlon MMM is tentatively attributed to the reduced framework flexibility of ZIF-11 crystals once embedded in the Torlon to form the MMM. The absence of such diffusivity reduction in the other two studied MMMs is tentatively explained by the higher bulk modulus of Torlon compared to Matrimid and 6FDA-DAM. | ||
| 650 | 4 | |a Diffusion | |
| 650 | 4 | |a PFG NMR | |
| 650 | 4 | |a MOF | |
| 650 | 4 | |a Mixed-matrix membrane | |
| 700 | 1 | |a Baniani, Amineh |e verfasserin |4 aut | |
| 700 | 1 | |a Fan, Lei |e verfasserin |4 aut | |
| 700 | 1 | |a Ziegler, Kirk J. |e verfasserin |4 aut | |
| 700 | 1 | |a Zhou, Erkang |e verfasserin |4 aut | |
| 700 | 1 | |a Zhang, Fengyi |e verfasserin |4 aut | |
| 700 | 1 | |a Lively, Ryan P. |e verfasserin |0 (orcid)0000-0002-8039-4008 |4 aut | |
| 700 | 1 | |a Vasenkov, Sergey |e verfasserin |0 (orcid)0000-0002-8619-0612 |4 aut | |
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10.1016/j.micromeso.2018.07.044 doi (DE-627)ELV000998893 (ELSEVIER)S1387-1811(18)30419-0 DE-627 ger DE-627 rda eng 530 DE-600 38.30 bkl 35.68 bkl 33.61 bkl 35.90 bkl 51.45 bkl Forman, Evan M. verfasserin aut Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier 13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of the following three polymers: Torlon, Matrimid, and 6FDA-DAM. PFG NMR data allowed obtaining ethylene diffusivities inside ZIF-11 crystals in the crystal beds and MMMs under the same or similar conditions. It was observed that the intra-ZIF diffusivities in ZIF-11/Torlon MMM are smaller than the corresponding diffusivities in the ZIF-11 bed. The observed diffusivity reduction becomes less significant with increasing ethylene loading. At the same time, within uncertainty, no difference in the intra-ZIF diffusivities between ZIF-11 bed and MMMs were observed for ZIF-11/Matrimid and ZIF-11/6FDA-DAM MMMs. The intra-ZIF diffusivity reduction observed for ZIF-11/Torlon MMM is tentatively attributed to the reduced framework flexibility of ZIF-11 crystals once embedded in the Torlon to form the MMM. The absence of such diffusivity reduction in the other two studied MMMs is tentatively explained by the higher bulk modulus of Torlon compared to Matrimid and 6FDA-DAM. Diffusion PFG NMR MOF Mixed-matrix membrane Baniani, Amineh verfasserin aut Fan, Lei verfasserin aut Ziegler, Kirk J. verfasserin aut Zhou, Erkang verfasserin aut Zhang, Fengyi verfasserin aut Lively, Ryan P. verfasserin (orcid)0000-0002-8039-4008 aut Vasenkov, Sergey verfasserin (orcid)0000-0002-8619-0612 aut Enthalten in Microporous and mesoporous materials Amsterdam [u.a.] : Elsevier, 1998 274, Seite 163-170 Online-Ressource (DE-627)318368277 (DE-600)2012505-7 (DE-576)09529998X 1387-1811 nnns volume:274 pages:163-170 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 38.30 Mineralogie 35.68 Organische Verbindungen: Sonstiges 33.61 Festkörperphysik 35.90 Festkörperchemie 51.45 Werkstoffe mit besonderen Eigenschaften AR 274 163-170 |
| spelling |
10.1016/j.micromeso.2018.07.044 doi (DE-627)ELV000998893 (ELSEVIER)S1387-1811(18)30419-0 DE-627 ger DE-627 rda eng 530 DE-600 38.30 bkl 35.68 bkl 33.61 bkl 35.90 bkl 51.45 bkl Forman, Evan M. verfasserin aut Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier 13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of the following three polymers: Torlon, Matrimid, and 6FDA-DAM. PFG NMR data allowed obtaining ethylene diffusivities inside ZIF-11 crystals in the crystal beds and MMMs under the same or similar conditions. It was observed that the intra-ZIF diffusivities in ZIF-11/Torlon MMM are smaller than the corresponding diffusivities in the ZIF-11 bed. The observed diffusivity reduction becomes less significant with increasing ethylene loading. At the same time, within uncertainty, no difference in the intra-ZIF diffusivities between ZIF-11 bed and MMMs were observed for ZIF-11/Matrimid and ZIF-11/6FDA-DAM MMMs. The intra-ZIF diffusivity reduction observed for ZIF-11/Torlon MMM is tentatively attributed to the reduced framework flexibility of ZIF-11 crystals once embedded in the Torlon to form the MMM. The absence of such diffusivity reduction in the other two studied MMMs is tentatively explained by the higher bulk modulus of Torlon compared to Matrimid and 6FDA-DAM. Diffusion PFG NMR MOF Mixed-matrix membrane Baniani, Amineh verfasserin aut Fan, Lei verfasserin aut Ziegler, Kirk J. verfasserin aut Zhou, Erkang verfasserin aut Zhang, Fengyi verfasserin aut Lively, Ryan P. verfasserin (orcid)0000-0002-8039-4008 aut Vasenkov, Sergey verfasserin (orcid)0000-0002-8619-0612 aut Enthalten in Microporous and mesoporous materials Amsterdam [u.a.] : Elsevier, 1998 274, Seite 163-170 Online-Ressource (DE-627)318368277 (DE-600)2012505-7 (DE-576)09529998X 1387-1811 nnns volume:274 pages:163-170 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 38.30 Mineralogie 35.68 Organische Verbindungen: Sonstiges 33.61 Festkörperphysik 35.90 Festkörperchemie 51.45 Werkstoffe mit besonderen Eigenschaften AR 274 163-170 |
| allfields_unstemmed |
10.1016/j.micromeso.2018.07.044 doi (DE-627)ELV000998893 (ELSEVIER)S1387-1811(18)30419-0 DE-627 ger DE-627 rda eng 530 DE-600 38.30 bkl 35.68 bkl 33.61 bkl 35.90 bkl 51.45 bkl Forman, Evan M. verfasserin aut Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier 13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of the following three polymers: Torlon, Matrimid, and 6FDA-DAM. PFG NMR data allowed obtaining ethylene diffusivities inside ZIF-11 crystals in the crystal beds and MMMs under the same or similar conditions. It was observed that the intra-ZIF diffusivities in ZIF-11/Torlon MMM are smaller than the corresponding diffusivities in the ZIF-11 bed. The observed diffusivity reduction becomes less significant with increasing ethylene loading. At the same time, within uncertainty, no difference in the intra-ZIF diffusivities between ZIF-11 bed and MMMs were observed for ZIF-11/Matrimid and ZIF-11/6FDA-DAM MMMs. The intra-ZIF diffusivity reduction observed for ZIF-11/Torlon MMM is tentatively attributed to the reduced framework flexibility of ZIF-11 crystals once embedded in the Torlon to form the MMM. The absence of such diffusivity reduction in the other two studied MMMs is tentatively explained by the higher bulk modulus of Torlon compared to Matrimid and 6FDA-DAM. Diffusion PFG NMR MOF Mixed-matrix membrane Baniani, Amineh verfasserin aut Fan, Lei verfasserin aut Ziegler, Kirk J. verfasserin aut Zhou, Erkang verfasserin aut Zhang, Fengyi verfasserin aut Lively, Ryan P. verfasserin (orcid)0000-0002-8039-4008 aut Vasenkov, Sergey verfasserin (orcid)0000-0002-8619-0612 aut Enthalten in Microporous and mesoporous materials Amsterdam [u.a.] : Elsevier, 1998 274, Seite 163-170 Online-Ressource (DE-627)318368277 (DE-600)2012505-7 (DE-576)09529998X 1387-1811 nnns volume:274 pages:163-170 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 38.30 Mineralogie 35.68 Organische Verbindungen: Sonstiges 33.61 Festkörperphysik 35.90 Festkörperchemie 51.45 Werkstoffe mit besonderen Eigenschaften AR 274 163-170 |
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10.1016/j.micromeso.2018.07.044 doi (DE-627)ELV000998893 (ELSEVIER)S1387-1811(18)30419-0 DE-627 ger DE-627 rda eng 530 DE-600 38.30 bkl 35.68 bkl 33.61 bkl 35.90 bkl 51.45 bkl Forman, Evan M. verfasserin aut Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier 13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of the following three polymers: Torlon, Matrimid, and 6FDA-DAM. PFG NMR data allowed obtaining ethylene diffusivities inside ZIF-11 crystals in the crystal beds and MMMs under the same or similar conditions. It was observed that the intra-ZIF diffusivities in ZIF-11/Torlon MMM are smaller than the corresponding diffusivities in the ZIF-11 bed. The observed diffusivity reduction becomes less significant with increasing ethylene loading. At the same time, within uncertainty, no difference in the intra-ZIF diffusivities between ZIF-11 bed and MMMs were observed for ZIF-11/Matrimid and ZIF-11/6FDA-DAM MMMs. The intra-ZIF diffusivity reduction observed for ZIF-11/Torlon MMM is tentatively attributed to the reduced framework flexibility of ZIF-11 crystals once embedded in the Torlon to form the MMM. The absence of such diffusivity reduction in the other two studied MMMs is tentatively explained by the higher bulk modulus of Torlon compared to Matrimid and 6FDA-DAM. Diffusion PFG NMR MOF Mixed-matrix membrane Baniani, Amineh verfasserin aut Fan, Lei verfasserin aut Ziegler, Kirk J. verfasserin aut Zhou, Erkang verfasserin aut Zhang, Fengyi verfasserin aut Lively, Ryan P. verfasserin (orcid)0000-0002-8039-4008 aut Vasenkov, Sergey verfasserin (orcid)0000-0002-8619-0612 aut Enthalten in Microporous and mesoporous materials Amsterdam [u.a.] : Elsevier, 1998 274, Seite 163-170 Online-Ressource (DE-627)318368277 (DE-600)2012505-7 (DE-576)09529998X 1387-1811 nnns volume:274 pages:163-170 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 38.30 Mineralogie 35.68 Organische Verbindungen: Sonstiges 33.61 Festkörperphysik 35.90 Festkörperchemie 51.45 Werkstoffe mit besonderen Eigenschaften AR 274 163-170 |
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10.1016/j.micromeso.2018.07.044 doi (DE-627)ELV000998893 (ELSEVIER)S1387-1811(18)30419-0 DE-627 ger DE-627 rda eng 530 DE-600 38.30 bkl 35.68 bkl 33.61 bkl 35.90 bkl 51.45 bkl Forman, Evan M. verfasserin aut Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier 13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of the following three polymers: Torlon, Matrimid, and 6FDA-DAM. PFG NMR data allowed obtaining ethylene diffusivities inside ZIF-11 crystals in the crystal beds and MMMs under the same or similar conditions. It was observed that the intra-ZIF diffusivities in ZIF-11/Torlon MMM are smaller than the corresponding diffusivities in the ZIF-11 bed. The observed diffusivity reduction becomes less significant with increasing ethylene loading. At the same time, within uncertainty, no difference in the intra-ZIF diffusivities between ZIF-11 bed and MMMs were observed for ZIF-11/Matrimid and ZIF-11/6FDA-DAM MMMs. The intra-ZIF diffusivity reduction observed for ZIF-11/Torlon MMM is tentatively attributed to the reduced framework flexibility of ZIF-11 crystals once embedded in the Torlon to form the MMM. The absence of such diffusivity reduction in the other two studied MMMs is tentatively explained by the higher bulk modulus of Torlon compared to Matrimid and 6FDA-DAM. Diffusion PFG NMR MOF Mixed-matrix membrane Baniani, Amineh verfasserin aut Fan, Lei verfasserin aut Ziegler, Kirk J. verfasserin aut Zhou, Erkang verfasserin aut Zhang, Fengyi verfasserin aut Lively, Ryan P. verfasserin (orcid)0000-0002-8039-4008 aut Vasenkov, Sergey verfasserin (orcid)0000-0002-8619-0612 aut Enthalten in Microporous and mesoporous materials Amsterdam [u.a.] : Elsevier, 1998 274, Seite 163-170 Online-Ressource (DE-627)318368277 (DE-600)2012505-7 (DE-576)09529998X 1387-1811 nnns volume:274 pages:163-170 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 38.30 Mineralogie 35.68 Organische Verbindungen: Sonstiges 33.61 Festkörperphysik 35.90 Festkörperchemie 51.45 Werkstoffe mit besonderen Eigenschaften AR 274 163-170 |
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Enthalten in Microporous and mesoporous materials 274, Seite 163-170 volume:274 pages:163-170 |
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Enthalten in Microporous and mesoporous materials 274, Seite 163-170 volume:274 pages:163-170 |
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Mineralogie Organische Verbindungen: Sonstiges Festkörperphysik Festkörperchemie Werkstoffe mit besonderen Eigenschaften |
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Diffusion PFG NMR MOF Mixed-matrix membrane |
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Forman, Evan M. @@aut@@ Baniani, Amineh @@aut@@ Fan, Lei @@aut@@ Ziegler, Kirk J. @@aut@@ Zhou, Erkang @@aut@@ Zhang, Fengyi @@aut@@ Lively, Ryan P. @@aut@@ Vasenkov, Sergey @@aut@@ |
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2018-01-01T00:00:00Z |
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Forman, Evan M. |
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Forman, Evan M. ddc 530 bkl 38.30 bkl 35.68 bkl 33.61 bkl 35.90 bkl 51.45 misc Diffusion misc PFG NMR misc MOF misc Mixed-matrix membrane Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes |
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530 DE-600 38.30 bkl 35.68 bkl 33.61 bkl 35.90 bkl 51.45 bkl Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes Diffusion PFG NMR MOF Mixed-matrix membrane |
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ddc 530 bkl 38.30 bkl 35.68 bkl 33.61 bkl 35.90 bkl 51.45 misc Diffusion misc PFG NMR misc MOF misc Mixed-matrix membrane |
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ddc 530 bkl 38.30 bkl 35.68 bkl 33.61 bkl 35.90 bkl 51.45 misc Diffusion misc PFG NMR misc MOF misc Mixed-matrix membrane |
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Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes |
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Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes |
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Forman, Evan M. |
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Microporous and mesoporous materials |
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Forman, Evan M. Baniani, Amineh Fan, Lei Ziegler, Kirk J. Zhou, Erkang Zhang, Fengyi Lively, Ryan P. Vasenkov, Sergey |
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ethylene diffusion in crystals of zeolitic imidazole framework-11 embedded in polymers to form mixed-matrix membranes |
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Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes |
| abstract |
13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of the following three polymers: Torlon, Matrimid, and 6FDA-DAM. PFG NMR data allowed obtaining ethylene diffusivities inside ZIF-11 crystals in the crystal beds and MMMs under the same or similar conditions. It was observed that the intra-ZIF diffusivities in ZIF-11/Torlon MMM are smaller than the corresponding diffusivities in the ZIF-11 bed. The observed diffusivity reduction becomes less significant with increasing ethylene loading. At the same time, within uncertainty, no difference in the intra-ZIF diffusivities between ZIF-11 bed and MMMs were observed for ZIF-11/Matrimid and ZIF-11/6FDA-DAM MMMs. The intra-ZIF diffusivity reduction observed for ZIF-11/Torlon MMM is tentatively attributed to the reduced framework flexibility of ZIF-11 crystals once embedded in the Torlon to form the MMM. The absence of such diffusivity reduction in the other two studied MMMs is tentatively explained by the higher bulk modulus of Torlon compared to Matrimid and 6FDA-DAM. |
| abstractGer |
13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of the following three polymers: Torlon, Matrimid, and 6FDA-DAM. PFG NMR data allowed obtaining ethylene diffusivities inside ZIF-11 crystals in the crystal beds and MMMs under the same or similar conditions. It was observed that the intra-ZIF diffusivities in ZIF-11/Torlon MMM are smaller than the corresponding diffusivities in the ZIF-11 bed. The observed diffusivity reduction becomes less significant with increasing ethylene loading. At the same time, within uncertainty, no difference in the intra-ZIF diffusivities between ZIF-11 bed and MMMs were observed for ZIF-11/Matrimid and ZIF-11/6FDA-DAM MMMs. The intra-ZIF diffusivity reduction observed for ZIF-11/Torlon MMM is tentatively attributed to the reduced framework flexibility of ZIF-11 crystals once embedded in the Torlon to form the MMM. The absence of such diffusivity reduction in the other two studied MMMs is tentatively explained by the higher bulk modulus of Torlon compared to Matrimid and 6FDA-DAM. |
| abstract_unstemmed |
13C Pulsed field gradient (PFG) NMR was used to study the self-diffusion of ethylene in loosely packed beds of ZIF-11 crystals and ZIF-11 based mixed matrix membranes (MMMs) at different sorbate loadings and diffusion times. The ZIF-11 based MMMs were formed by embedding ZIF-11 crystals in one of the following three polymers: Torlon, Matrimid, and 6FDA-DAM. PFG NMR data allowed obtaining ethylene diffusivities inside ZIF-11 crystals in the crystal beds and MMMs under the same or similar conditions. It was observed that the intra-ZIF diffusivities in ZIF-11/Torlon MMM are smaller than the corresponding diffusivities in the ZIF-11 bed. The observed diffusivity reduction becomes less significant with increasing ethylene loading. At the same time, within uncertainty, no difference in the intra-ZIF diffusivities between ZIF-11 bed and MMMs were observed for ZIF-11/Matrimid and ZIF-11/6FDA-DAM MMMs. The intra-ZIF diffusivity reduction observed for ZIF-11/Torlon MMM is tentatively attributed to the reduced framework flexibility of ZIF-11 crystals once embedded in the Torlon to form the MMM. The absence of such diffusivity reduction in the other two studied MMMs is tentatively explained by the higher bulk modulus of Torlon compared to Matrimid and 6FDA-DAM. |
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Ethylene diffusion in crystals of zeolitic imidazole Framework-11 embedded in polymers to form mixed-matrix membranes |
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