Diammonium hydrogenphosphate for the consolidation of building materials. Investigation of newly-formed calcium phosphates
Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controvers...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Possenti, Elena [verfasserIn] Colombo, Chiara [verfasserIn] Conti, Claudia [verfasserIn] Gigli, Lara [verfasserIn] Merlini, Marco [verfasserIn] Plaisier, Jasper Rikkert [verfasserIn] Realini, Marco [verfasserIn] Sali, Diego [verfasserIn] Gatta, G. Diego [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2018 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Construction and building materials - Amsterdam [u.a.] : Elsevier Science, 1987, 195, Seite 557-563 |
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| Übergeordnetes Werk: |
volume:195 ; pages:557-563 |
| DOI / URN: |
10.1016/j.conbuildmat.2018.11.077 |
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| 245 | 1 | 0 | |a Diammonium hydrogenphosphate for the consolidation of building materials. Investigation of newly-formed calcium phosphates |
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| 520 | |a Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controversial. This study investigated how the DAP molarity, the treatment method and the microstructure of the stone influence the formation of specific phases. Thermal treatments and cutting-edge techniques (XRD with synchrotron radiation in transmitting geometry and high resolution FTIR microspectroscopy) were used to overcome the analytical limits of the more conventional methods, shading light to an in depth evaluation of DAP consolidating processes and treatment conditions. | ||
| 650 | 4 | |a Carrara marble | |
| 650 | 4 | |a Calcium phosphates | |
| 650 | 4 | |a Consolidation | |
| 650 | 4 | |a Diammonium hydrogenphosphate | |
| 650 | 4 | |a Synchrotron X-ray powder diffraction | |
| 650 | 4 | |a High resolution FTIR microspectroscopy | |
| 700 | 1 | |a Colombo, Chiara |e verfasserin |4 aut | |
| 700 | 1 | |a Conti, Claudia |e verfasserin |4 aut | |
| 700 | 1 | |a Gigli, Lara |e verfasserin |4 aut | |
| 700 | 1 | |a Merlini, Marco |e verfasserin |4 aut | |
| 700 | 1 | |a Plaisier, Jasper Rikkert |e verfasserin |4 aut | |
| 700 | 1 | |a Realini, Marco |e verfasserin |4 aut | |
| 700 | 1 | |a Sali, Diego |e verfasserin |4 aut | |
| 700 | 1 | |a Gatta, G. Diego |e verfasserin |4 aut | |
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10.1016/j.conbuildmat.2018.11.077 doi (DE-627)ELV00128553X (ELSEVIER)S0950-0618(18)32741-7 DE-627 ger DE-627 rda eng 690 DE-600 56.45 bkl Possenti, Elena verfasserin (orcid)0000-0002-9041-7971 aut Diammonium hydrogenphosphate for the consolidation of building materials. Investigation of newly-formed calcium phosphates 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controversial. This study investigated how the DAP molarity, the treatment method and the microstructure of the stone influence the formation of specific phases. Thermal treatments and cutting-edge techniques (XRD with synchrotron radiation in transmitting geometry and high resolution FTIR microspectroscopy) were used to overcome the analytical limits of the more conventional methods, shading light to an in depth evaluation of DAP consolidating processes and treatment conditions. Carrara marble Calcium phosphates Consolidation Diammonium hydrogenphosphate Synchrotron X-ray powder diffraction High resolution FTIR microspectroscopy Colombo, Chiara verfasserin aut Conti, Claudia verfasserin aut Gigli, Lara verfasserin aut Merlini, Marco verfasserin aut Plaisier, Jasper Rikkert verfasserin aut Realini, Marco verfasserin aut Sali, Diego verfasserin aut Gatta, G. Diego verfasserin aut Enthalten in Construction and building materials Amsterdam [u.a.] : Elsevier Science, 1987 195, Seite 557-563 Online-Ressource (DE-627)320423115 (DE-600)2002804-0 (DE-576)259271187 nnns volume:195 pages:557-563 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 56.45 Baustoffkunde AR 195 557-563 |
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10.1016/j.conbuildmat.2018.11.077 doi (DE-627)ELV00128553X (ELSEVIER)S0950-0618(18)32741-7 DE-627 ger DE-627 rda eng 690 DE-600 56.45 bkl Possenti, Elena verfasserin (orcid)0000-0002-9041-7971 aut Diammonium hydrogenphosphate for the consolidation of building materials. Investigation of newly-formed calcium phosphates 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controversial. This study investigated how the DAP molarity, the treatment method and the microstructure of the stone influence the formation of specific phases. Thermal treatments and cutting-edge techniques (XRD with synchrotron radiation in transmitting geometry and high resolution FTIR microspectroscopy) were used to overcome the analytical limits of the more conventional methods, shading light to an in depth evaluation of DAP consolidating processes and treatment conditions. Carrara marble Calcium phosphates Consolidation Diammonium hydrogenphosphate Synchrotron X-ray powder diffraction High resolution FTIR microspectroscopy Colombo, Chiara verfasserin aut Conti, Claudia verfasserin aut Gigli, Lara verfasserin aut Merlini, Marco verfasserin aut Plaisier, Jasper Rikkert verfasserin aut Realini, Marco verfasserin aut Sali, Diego verfasserin aut Gatta, G. Diego verfasserin aut Enthalten in Construction and building materials Amsterdam [u.a.] : Elsevier Science, 1987 195, Seite 557-563 Online-Ressource (DE-627)320423115 (DE-600)2002804-0 (DE-576)259271187 nnns volume:195 pages:557-563 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 56.45 Baustoffkunde AR 195 557-563 |
| allfields_unstemmed |
10.1016/j.conbuildmat.2018.11.077 doi (DE-627)ELV00128553X (ELSEVIER)S0950-0618(18)32741-7 DE-627 ger DE-627 rda eng 690 DE-600 56.45 bkl Possenti, Elena verfasserin (orcid)0000-0002-9041-7971 aut Diammonium hydrogenphosphate for the consolidation of building materials. Investigation of newly-formed calcium phosphates 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controversial. This study investigated how the DAP molarity, the treatment method and the microstructure of the stone influence the formation of specific phases. Thermal treatments and cutting-edge techniques (XRD with synchrotron radiation in transmitting geometry and high resolution FTIR microspectroscopy) were used to overcome the analytical limits of the more conventional methods, shading light to an in depth evaluation of DAP consolidating processes and treatment conditions. Carrara marble Calcium phosphates Consolidation Diammonium hydrogenphosphate Synchrotron X-ray powder diffraction High resolution FTIR microspectroscopy Colombo, Chiara verfasserin aut Conti, Claudia verfasserin aut Gigli, Lara verfasserin aut Merlini, Marco verfasserin aut Plaisier, Jasper Rikkert verfasserin aut Realini, Marco verfasserin aut Sali, Diego verfasserin aut Gatta, G. Diego verfasserin aut Enthalten in Construction and building materials Amsterdam [u.a.] : Elsevier Science, 1987 195, Seite 557-563 Online-Ressource (DE-627)320423115 (DE-600)2002804-0 (DE-576)259271187 nnns volume:195 pages:557-563 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 56.45 Baustoffkunde AR 195 557-563 |
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10.1016/j.conbuildmat.2018.11.077 doi (DE-627)ELV00128553X (ELSEVIER)S0950-0618(18)32741-7 DE-627 ger DE-627 rda eng 690 DE-600 56.45 bkl Possenti, Elena verfasserin (orcid)0000-0002-9041-7971 aut Diammonium hydrogenphosphate for the consolidation of building materials. Investigation of newly-formed calcium phosphates 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controversial. This study investigated how the DAP molarity, the treatment method and the microstructure of the stone influence the formation of specific phases. Thermal treatments and cutting-edge techniques (XRD with synchrotron radiation in transmitting geometry and high resolution FTIR microspectroscopy) were used to overcome the analytical limits of the more conventional methods, shading light to an in depth evaluation of DAP consolidating processes and treatment conditions. Carrara marble Calcium phosphates Consolidation Diammonium hydrogenphosphate Synchrotron X-ray powder diffraction High resolution FTIR microspectroscopy Colombo, Chiara verfasserin aut Conti, Claudia verfasserin aut Gigli, Lara verfasserin aut Merlini, Marco verfasserin aut Plaisier, Jasper Rikkert verfasserin aut Realini, Marco verfasserin aut Sali, Diego verfasserin aut Gatta, G. Diego verfasserin aut Enthalten in Construction and building materials Amsterdam [u.a.] : Elsevier Science, 1987 195, Seite 557-563 Online-Ressource (DE-627)320423115 (DE-600)2002804-0 (DE-576)259271187 nnns volume:195 pages:557-563 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 56.45 Baustoffkunde AR 195 557-563 |
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10.1016/j.conbuildmat.2018.11.077 doi (DE-627)ELV00128553X (ELSEVIER)S0950-0618(18)32741-7 DE-627 ger DE-627 rda eng 690 DE-600 56.45 bkl Possenti, Elena verfasserin (orcid)0000-0002-9041-7971 aut Diammonium hydrogenphosphate for the consolidation of building materials. Investigation of newly-formed calcium phosphates 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controversial. This study investigated how the DAP molarity, the treatment method and the microstructure of the stone influence the formation of specific phases. Thermal treatments and cutting-edge techniques (XRD with synchrotron radiation in transmitting geometry and high resolution FTIR microspectroscopy) were used to overcome the analytical limits of the more conventional methods, shading light to an in depth evaluation of DAP consolidating processes and treatment conditions. Carrara marble Calcium phosphates Consolidation Diammonium hydrogenphosphate Synchrotron X-ray powder diffraction High resolution FTIR microspectroscopy Colombo, Chiara verfasserin aut Conti, Claudia verfasserin aut Gigli, Lara verfasserin aut Merlini, Marco verfasserin aut Plaisier, Jasper Rikkert verfasserin aut Realini, Marco verfasserin aut Sali, Diego verfasserin aut Gatta, G. Diego verfasserin aut Enthalten in Construction and building materials Amsterdam [u.a.] : Elsevier Science, 1987 195, Seite 557-563 Online-Ressource (DE-627)320423115 (DE-600)2002804-0 (DE-576)259271187 nnns volume:195 pages:557-563 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 56.45 Baustoffkunde AR 195 557-563 |
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Possenti, Elena |
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Possenti, Elena ddc 690 bkl 56.45 misc Carrara marble misc Calcium phosphates misc Consolidation misc Diammonium hydrogenphosphate misc Synchrotron X-ray powder diffraction misc High resolution FTIR microspectroscopy Diammonium hydrogenphosphate for the consolidation of building materials. Investigation of newly-formed calcium phosphates |
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diammonium hydrogenphosphate for the consolidation of building materials. investigation of newly-formed calcium phosphates |
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Diammonium hydrogenphosphate for the consolidation of building materials. Investigation of newly-formed calcium phosphates |
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Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controversial. This study investigated how the DAP molarity, the treatment method and the microstructure of the stone influence the formation of specific phases. Thermal treatments and cutting-edge techniques (XRD with synchrotron radiation in transmitting geometry and high resolution FTIR microspectroscopy) were used to overcome the analytical limits of the more conventional methods, shading light to an in depth evaluation of DAP consolidating processes and treatment conditions. |
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Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controversial. This study investigated how the DAP molarity, the treatment method and the microstructure of the stone influence the formation of specific phases. Thermal treatments and cutting-edge techniques (XRD with synchrotron radiation in transmitting geometry and high resolution FTIR microspectroscopy) were used to overcome the analytical limits of the more conventional methods, shading light to an in depth evaluation of DAP consolidating processes and treatment conditions. |
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Diammonium hydrogenphosphate (DAP) is a water soluble consolidant for decayed carbonatic materials of historical buildings. The reaction of DAP solutions with polycrystalline calcite of marbles is non-stoichiometric and forms a calcium phosphates mixture whose identification is tricky and controversial. This study investigated how the DAP molarity, the treatment method and the microstructure of the stone influence the formation of specific phases. Thermal treatments and cutting-edge techniques (XRD with synchrotron radiation in transmitting geometry and high resolution FTIR microspectroscopy) were used to overcome the analytical limits of the more conventional methods, shading light to an in depth evaluation of DAP consolidating processes and treatment conditions. |
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