Determination of thermal expansion of KCaI
KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Lindsey, Adam C. [verfasserIn] Loyd, Matthew [verfasserIn] Patel, Maulik K. [verfasserIn] Rawl, Ryan [verfasserIn] Zhou, Haidong [verfasserIn] Koschan, Merry [verfasserIn] Melcher, Charles L. [verfasserIn] Zhuravleva, Mariya [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2018 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Materials chemistry and physics - New York, NY [u.a.] : Elsevier, 1983, 212, Seite 161-166 |
|---|---|
| Übergeordnetes Werk: |
volume:212 ; pages:161-166 |
| DOI / URN: |
10.1016/j.matchemphys.2018.03.016 |
|---|
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ELV00153484X |
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| 245 | 1 | 0 | |a Determination of thermal expansion of KCaI |
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| 520 | |a KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-situ high temperature X-ray diffraction on powdered samples. Samples from single crystals of both pure and Eu-doped KCaI3 grown by the Bridgman method were used for comparison. Expansion with temperature along the b-axis is greatest with an average linear coefficient of thermal expansion of ≈ (41–46) x 10−6 K−1 resulting from the weaker bonding between alternating layers of K and Ca parallel to the b-axis. Thermal expansion in each of the KCaI3 samples has the highest degree of anisotropy with respect to the b and c axis with ratio ᾱb/ᾱc of 1.4–1.5. Additionally, we identify the predominant cleavage plane in KCaI3 as (0 -3 -1) based upon Laue reflection imaging. | ||
| 650 | 4 | |a X-ray diffraction | |
| 650 | 4 | |a Bridgman technique | |
| 650 | 4 | |a Halides | |
| 650 | 4 | |a Scintillator materials | |
| 700 | 1 | |a Loyd, Matthew |e verfasserin |4 aut | |
| 700 | 1 | |a Patel, Maulik K. |e verfasserin |4 aut | |
| 700 | 1 | |a Rawl, Ryan |e verfasserin |4 aut | |
| 700 | 1 | |a Zhou, Haidong |e verfasserin |4 aut | |
| 700 | 1 | |a Koschan, Merry |e verfasserin |4 aut | |
| 700 | 1 | |a Melcher, Charles L. |e verfasserin |4 aut | |
| 700 | 1 | |a Zhuravleva, Mariya |e verfasserin |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Materials chemistry and physics |d New York, NY [u.a.] : Elsevier, 1983 |g 212, Seite 161-166 |h Online-Ressource |w (DE-627)302719350 |w (DE-600)1491959-X |w (DE-576)096806435 |7 nnns |
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10.1016/j.matchemphys.2018.03.016 doi (DE-627)ELV00153484X (ELSEVIER)S0254-0584(18)30179-2 DE-627 ger DE-627 rda eng 540 530 DE-600 ASIEN DE-1a fid 6,25 ssgn 35.90 bkl 33.61 bkl 51.00 bkl Lindsey, Adam C. verfasserin aut Determination of thermal expansion of KCaI 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-situ high temperature X-ray diffraction on powdered samples. Samples from single crystals of both pure and Eu-doped KCaI3 grown by the Bridgman method were used for comparison. Expansion with temperature along the b-axis is greatest with an average linear coefficient of thermal expansion of ≈ (41–46) x 10−6 K−1 resulting from the weaker bonding between alternating layers of K and Ca parallel to the b-axis. Thermal expansion in each of the KCaI3 samples has the highest degree of anisotropy with respect to the b and c axis with ratio ᾱb/ᾱc of 1.4–1.5. Additionally, we identify the predominant cleavage plane in KCaI3 as (0 -3 -1) based upon Laue reflection imaging. X-ray diffraction Bridgman technique Halides Scintillator materials Loyd, Matthew verfasserin aut Patel, Maulik K. verfasserin aut Rawl, Ryan verfasserin aut Zhou, Haidong verfasserin aut Koschan, Merry verfasserin aut Melcher, Charles L. verfasserin aut Zhuravleva, Mariya verfasserin aut Enthalten in Materials chemistry and physics New York, NY [u.a.] : Elsevier, 1983 212, Seite 161-166 Online-Ressource (DE-627)302719350 (DE-600)1491959-X (DE-576)096806435 nnns volume:212 pages:161-166 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-ASIEN SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.90 Festkörperchemie 33.61 Festkörperphysik 51.00 Werkstoffkunde: Allgemeines AR 212 161-166 |
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10.1016/j.matchemphys.2018.03.016 doi (DE-627)ELV00153484X (ELSEVIER)S0254-0584(18)30179-2 DE-627 ger DE-627 rda eng 540 530 DE-600 ASIEN DE-1a fid 6,25 ssgn 35.90 bkl 33.61 bkl 51.00 bkl Lindsey, Adam C. verfasserin aut Determination of thermal expansion of KCaI 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-situ high temperature X-ray diffraction on powdered samples. Samples from single crystals of both pure and Eu-doped KCaI3 grown by the Bridgman method were used for comparison. Expansion with temperature along the b-axis is greatest with an average linear coefficient of thermal expansion of ≈ (41–46) x 10−6 K−1 resulting from the weaker bonding between alternating layers of K and Ca parallel to the b-axis. Thermal expansion in each of the KCaI3 samples has the highest degree of anisotropy with respect to the b and c axis with ratio ᾱb/ᾱc of 1.4–1.5. Additionally, we identify the predominant cleavage plane in KCaI3 as (0 -3 -1) based upon Laue reflection imaging. X-ray diffraction Bridgman technique Halides Scintillator materials Loyd, Matthew verfasserin aut Patel, Maulik K. verfasserin aut Rawl, Ryan verfasserin aut Zhou, Haidong verfasserin aut Koschan, Merry verfasserin aut Melcher, Charles L. verfasserin aut Zhuravleva, Mariya verfasserin aut Enthalten in Materials chemistry and physics New York, NY [u.a.] : Elsevier, 1983 212, Seite 161-166 Online-Ressource (DE-627)302719350 (DE-600)1491959-X (DE-576)096806435 nnns volume:212 pages:161-166 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-ASIEN SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.90 Festkörperchemie 33.61 Festkörperphysik 51.00 Werkstoffkunde: Allgemeines AR 212 161-166 |
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10.1016/j.matchemphys.2018.03.016 doi (DE-627)ELV00153484X (ELSEVIER)S0254-0584(18)30179-2 DE-627 ger DE-627 rda eng 540 530 DE-600 ASIEN DE-1a fid 6,25 ssgn 35.90 bkl 33.61 bkl 51.00 bkl Lindsey, Adam C. verfasserin aut Determination of thermal expansion of KCaI 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-situ high temperature X-ray diffraction on powdered samples. Samples from single crystals of both pure and Eu-doped KCaI3 grown by the Bridgman method were used for comparison. Expansion with temperature along the b-axis is greatest with an average linear coefficient of thermal expansion of ≈ (41–46) x 10−6 K−1 resulting from the weaker bonding between alternating layers of K and Ca parallel to the b-axis. Thermal expansion in each of the KCaI3 samples has the highest degree of anisotropy with respect to the b and c axis with ratio ᾱb/ᾱc of 1.4–1.5. Additionally, we identify the predominant cleavage plane in KCaI3 as (0 -3 -1) based upon Laue reflection imaging. X-ray diffraction Bridgman technique Halides Scintillator materials Loyd, Matthew verfasserin aut Patel, Maulik K. verfasserin aut Rawl, Ryan verfasserin aut Zhou, Haidong verfasserin aut Koschan, Merry verfasserin aut Melcher, Charles L. verfasserin aut Zhuravleva, Mariya verfasserin aut Enthalten in Materials chemistry and physics New York, NY [u.a.] : Elsevier, 1983 212, Seite 161-166 Online-Ressource (DE-627)302719350 (DE-600)1491959-X (DE-576)096806435 nnns volume:212 pages:161-166 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-ASIEN SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.90 Festkörperchemie 33.61 Festkörperphysik 51.00 Werkstoffkunde: Allgemeines AR 212 161-166 |
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10.1016/j.matchemphys.2018.03.016 doi (DE-627)ELV00153484X (ELSEVIER)S0254-0584(18)30179-2 DE-627 ger DE-627 rda eng 540 530 DE-600 ASIEN DE-1a fid 6,25 ssgn 35.90 bkl 33.61 bkl 51.00 bkl Lindsey, Adam C. verfasserin aut Determination of thermal expansion of KCaI 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-situ high temperature X-ray diffraction on powdered samples. Samples from single crystals of both pure and Eu-doped KCaI3 grown by the Bridgman method were used for comparison. Expansion with temperature along the b-axis is greatest with an average linear coefficient of thermal expansion of ≈ (41–46) x 10−6 K−1 resulting from the weaker bonding between alternating layers of K and Ca parallel to the b-axis. Thermal expansion in each of the KCaI3 samples has the highest degree of anisotropy with respect to the b and c axis with ratio ᾱb/ᾱc of 1.4–1.5. Additionally, we identify the predominant cleavage plane in KCaI3 as (0 -3 -1) based upon Laue reflection imaging. X-ray diffraction Bridgman technique Halides Scintillator materials Loyd, Matthew verfasserin aut Patel, Maulik K. verfasserin aut Rawl, Ryan verfasserin aut Zhou, Haidong verfasserin aut Koschan, Merry verfasserin aut Melcher, Charles L. verfasserin aut Zhuravleva, Mariya verfasserin aut Enthalten in Materials chemistry and physics New York, NY [u.a.] : Elsevier, 1983 212, Seite 161-166 Online-Ressource (DE-627)302719350 (DE-600)1491959-X (DE-576)096806435 nnns volume:212 pages:161-166 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-ASIEN SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.90 Festkörperchemie 33.61 Festkörperphysik 51.00 Werkstoffkunde: Allgemeines AR 212 161-166 |
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10.1016/j.matchemphys.2018.03.016 doi (DE-627)ELV00153484X (ELSEVIER)S0254-0584(18)30179-2 DE-627 ger DE-627 rda eng 540 530 DE-600 ASIEN DE-1a fid 6,25 ssgn 35.90 bkl 33.61 bkl 51.00 bkl Lindsey, Adam C. verfasserin aut Determination of thermal expansion of KCaI 2018 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-situ high temperature X-ray diffraction on powdered samples. Samples from single crystals of both pure and Eu-doped KCaI3 grown by the Bridgman method were used for comparison. Expansion with temperature along the b-axis is greatest with an average linear coefficient of thermal expansion of ≈ (41–46) x 10−6 K−1 resulting from the weaker bonding between alternating layers of K and Ca parallel to the b-axis. Thermal expansion in each of the KCaI3 samples has the highest degree of anisotropy with respect to the b and c axis with ratio ᾱb/ᾱc of 1.4–1.5. Additionally, we identify the predominant cleavage plane in KCaI3 as (0 -3 -1) based upon Laue reflection imaging. X-ray diffraction Bridgman technique Halides Scintillator materials Loyd, Matthew verfasserin aut Patel, Maulik K. verfasserin aut Rawl, Ryan verfasserin aut Zhou, Haidong verfasserin aut Koschan, Merry verfasserin aut Melcher, Charles L. verfasserin aut Zhuravleva, Mariya verfasserin aut Enthalten in Materials chemistry and physics New York, NY [u.a.] : Elsevier, 1983 212, Seite 161-166 Online-Ressource (DE-627)302719350 (DE-600)1491959-X (DE-576)096806435 nnns volume:212 pages:161-166 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-ASIEN SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.90 Festkörperchemie 33.61 Festkörperphysik 51.00 Werkstoffkunde: Allgemeines AR 212 161-166 |
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Lindsey, Adam C. |
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Lindsey, Adam C. ddc 540 fid ASIEN ssgn 6,25 bkl 35.90 bkl 33.61 bkl 51.00 misc X-ray diffraction misc Bridgman technique misc Halides misc Scintillator materials Determination of thermal expansion of KCaI |
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Determination of thermal expansion of KCaI |
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Determination of thermal expansion of KCaI |
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Lindsey, Adam C. Loyd, Matthew Patel, Maulik K. Rawl, Ryan Zhou, Haidong Koschan, Merry Melcher, Charles L. Zhuravleva, Mariya |
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determination of thermal expansion of kcai |
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Determination of thermal expansion of KCaI |
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KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-situ high temperature X-ray diffraction on powdered samples. Samples from single crystals of both pure and Eu-doped KCaI3 grown by the Bridgman method were used for comparison. Expansion with temperature along the b-axis is greatest with an average linear coefficient of thermal expansion of ≈ (41–46) x 10−6 K−1 resulting from the weaker bonding between alternating layers of K and Ca parallel to the b-axis. Thermal expansion in each of the KCaI3 samples has the highest degree of anisotropy with respect to the b and c axis with ratio ᾱb/ᾱc of 1.4–1.5. Additionally, we identify the predominant cleavage plane in KCaI3 as (0 -3 -1) based upon Laue reflection imaging. |
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KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-situ high temperature X-ray diffraction on powdered samples. Samples from single crystals of both pure and Eu-doped KCaI3 grown by the Bridgman method were used for comparison. Expansion with temperature along the b-axis is greatest with an average linear coefficient of thermal expansion of ≈ (41–46) x 10−6 K−1 resulting from the weaker bonding between alternating layers of K and Ca parallel to the b-axis. Thermal expansion in each of the KCaI3 samples has the highest degree of anisotropy with respect to the b and c axis with ratio ᾱb/ᾱc of 1.4–1.5. Additionally, we identify the predominant cleavage plane in KCaI3 as (0 -3 -1) based upon Laue reflection imaging. |
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KCaI3:Eu single crystals exhibit favorable scintillation properties and have potential for use in domestic security applications requiring radioisotope identification. The anisotropic thermal expansion of the orthorhombic unit cell of this perovskite-type scintillator has been investigated using in-situ high temperature X-ray diffraction on powdered samples. Samples from single crystals of both pure and Eu-doped KCaI3 grown by the Bridgman method were used for comparison. Expansion with temperature along the b-axis is greatest with an average linear coefficient of thermal expansion of ≈ (41–46) x 10−6 K−1 resulting from the weaker bonding between alternating layers of K and Ca parallel to the b-axis. Thermal expansion in each of the KCaI3 samples has the highest degree of anisotropy with respect to the b and c axis with ratio ᾱb/ᾱc of 1.4–1.5. Additionally, we identify the predominant cleavage plane in KCaI3 as (0 -3 -1) based upon Laue reflection imaging. |
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