Mg, Ca and Ba glutaratouranylates – Synthesis and structure

Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt...
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Autor*in:	Novikov, S.A. [verfasserIn] Serezhkina, L.B. [verfasserIn] Grigoriev, M.S. [verfasserIn] Serezhkin, V.N. [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2017

Schlagwörter:	Uranium Coordination polymers Glutarate Structures

Übergeordnetes Werk:	Enthalten in: Polyhedron - Amsterdam [u.a.] : Elsevier Science, 1982, 141, Seite 147-152
Übergeordnetes Werk:	volume:141 ; pages:147-152

DOI / URN:	10.1016/j.poly.2017.11.031

Katalog-ID:	ELV00155090X

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245	1	0	\|a Mg, Ca and Ba glutaratouranylates – Synthesis and structure
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520			\|a Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt = C5H7O4 − (hydroglutarate) anions. The structures of compounds 1–3 contain 1D [UO2(glt)(Hglt)]− units that belong to the AQ02B01 (A = UO2 2+, Q02 = glt, B01 = Hglt) crystallochemical group. The different roles of alkaline earth R2+ cations in the structures and the flexibility of the glutarate anions account for the structural distinctions of 1–3. The diverse ways for the connection between the R2+ ions and the [UO2(glt)(Hglt)]− chains, the water content and the geometry of the uranyl-glutarate units present the main structural features of the new complexes. A comparative analysis based on Pauling's second rule of 1–3 and alkali glutaratouranylates has allowed an explanation of their structural dissimilarity.
650		4	\|a Uranium
650		4	\|a Coordination polymers
650		4	\|a Glutarate
650		4	\|a Structures
700	1		\|a Serezhkina, L.B. \|e verfasserin \|4 aut
700	1		\|a Grigoriev, M.S. \|e verfasserin \|4 aut
700	1		\|a Serezhkin, V.N. \|e verfasserin \|4 aut
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912			\|a GBV_ILN_2044
912			\|a GBV_ILN_2048
912			\|a GBV_ILN_2049
912			\|a GBV_ILN_2050
912			\|a GBV_ILN_2055
912			\|a GBV_ILN_2056
912			\|a GBV_ILN_2059
912			\|a GBV_ILN_2061
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912			\|a GBV_ILN_2507
912			\|a GBV_ILN_2522
912			\|a GBV_ILN_4035
912			\|a GBV_ILN_4037
912			\|a GBV_ILN_4112
912			\|a GBV_ILN_4125
912			\|a GBV_ILN_4126
912			\|a GBV_ILN_4242
912			\|a GBV_ILN_4251
912			\|a GBV_ILN_4305
912			\|a GBV_ILN_4313
912			\|a GBV_ILN_4323
912			\|a GBV_ILN_4324
912			\|a GBV_ILN_4325
912			\|a GBV_ILN_4326
912			\|a GBV_ILN_4333
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936	b	k	\|a 35.00 \|j Chemie: Allgemeines
951			\|a AR
952			\|d 141 \|h 147-152

Indexfelder

author_variant	s n sn l s ls m g mg v s vs
matchkey_str	novikovsaserezhkinalbgrigorievmsserezhki:2017----:ganbguaaornltsytei
hierarchy_sort_str	2017
bklnumber	35.00
publishDate	2017
allfields	10.1016/j.poly.2017.11.031 doi (DE-627)ELV00155090X (ELSEVIER)S0277-5387(17)30759-3 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Novikov, S.A. verfasserin aut Mg, Ca and Ba glutaratouranylates – Synthesis and structure 2017 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt = C5H7O4 − (hydroglutarate) anions. The structures of compounds 1–3 contain 1D [UO2(glt)(Hglt)]− units that belong to the AQ02B01 (A = UO2 2+, Q02 = glt, B01 = Hglt) crystallochemical group. The different roles of alkaline earth R2+ cations in the structures and the flexibility of the glutarate anions account for the structural distinctions of 1–3. The diverse ways for the connection between the R2+ ions and the [UO2(glt)(Hglt)]− chains, the water content and the geometry of the uranyl-glutarate units present the main structural features of the new complexes. A comparative analysis based on Pauling's second rule of 1–3 and alkali glutaratouranylates has allowed an explanation of their structural dissimilarity. Uranium Coordination polymers Glutarate Structures Serezhkina, L.B. verfasserin aut Grigoriev, M.S. verfasserin aut Serezhkin, V.N. verfasserin aut Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 141, Seite 147-152 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:141 pages:147-152 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 141 147-152
spelling	10.1016/j.poly.2017.11.031 doi (DE-627)ELV00155090X (ELSEVIER)S0277-5387(17)30759-3 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Novikov, S.A. verfasserin aut Mg, Ca and Ba glutaratouranylates – Synthesis and structure 2017 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt = C5H7O4 − (hydroglutarate) anions. The structures of compounds 1–3 contain 1D [UO2(glt)(Hglt)]− units that belong to the AQ02B01 (A = UO2 2+, Q02 = glt, B01 = Hglt) crystallochemical group. The different roles of alkaline earth R2+ cations in the structures and the flexibility of the glutarate anions account for the structural distinctions of 1–3. The diverse ways for the connection between the R2+ ions and the [UO2(glt)(Hglt)]− chains, the water content and the geometry of the uranyl-glutarate units present the main structural features of the new complexes. A comparative analysis based on Pauling's second rule of 1–3 and alkali glutaratouranylates has allowed an explanation of their structural dissimilarity. Uranium Coordination polymers Glutarate Structures Serezhkina, L.B. verfasserin aut Grigoriev, M.S. verfasserin aut Serezhkin, V.N. verfasserin aut Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 141, Seite 147-152 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:141 pages:147-152 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 141 147-152
allfields_unstemmed	10.1016/j.poly.2017.11.031 doi (DE-627)ELV00155090X (ELSEVIER)S0277-5387(17)30759-3 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Novikov, S.A. verfasserin aut Mg, Ca and Ba glutaratouranylates – Synthesis and structure 2017 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt = C5H7O4 − (hydroglutarate) anions. The structures of compounds 1–3 contain 1D [UO2(glt)(Hglt)]− units that belong to the AQ02B01 (A = UO2 2+, Q02 = glt, B01 = Hglt) crystallochemical group. The different roles of alkaline earth R2+ cations in the structures and the flexibility of the glutarate anions account for the structural distinctions of 1–3. The diverse ways for the connection between the R2+ ions and the [UO2(glt)(Hglt)]− chains, the water content and the geometry of the uranyl-glutarate units present the main structural features of the new complexes. A comparative analysis based on Pauling's second rule of 1–3 and alkali glutaratouranylates has allowed an explanation of their structural dissimilarity. Uranium Coordination polymers Glutarate Structures Serezhkina, L.B. verfasserin aut Grigoriev, M.S. verfasserin aut Serezhkin, V.N. verfasserin aut Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 141, Seite 147-152 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:141 pages:147-152 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 141 147-152
allfieldsGer	10.1016/j.poly.2017.11.031 doi (DE-627)ELV00155090X (ELSEVIER)S0277-5387(17)30759-3 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Novikov, S.A. verfasserin aut Mg, Ca and Ba glutaratouranylates – Synthesis and structure 2017 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt = C5H7O4 − (hydroglutarate) anions. The structures of compounds 1–3 contain 1D [UO2(glt)(Hglt)]− units that belong to the AQ02B01 (A = UO2 2+, Q02 = glt, B01 = Hglt) crystallochemical group. The different roles of alkaline earth R2+ cations in the structures and the flexibility of the glutarate anions account for the structural distinctions of 1–3. The diverse ways for the connection between the R2+ ions and the [UO2(glt)(Hglt)]− chains, the water content and the geometry of the uranyl-glutarate units present the main structural features of the new complexes. A comparative analysis based on Pauling's second rule of 1–3 and alkali glutaratouranylates has allowed an explanation of their structural dissimilarity. Uranium Coordination polymers Glutarate Structures Serezhkina, L.B. verfasserin aut Grigoriev, M.S. verfasserin aut Serezhkin, V.N. verfasserin aut Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 141, Seite 147-152 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:141 pages:147-152 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 141 147-152
allfieldsSound	10.1016/j.poly.2017.11.031 doi (DE-627)ELV00155090X (ELSEVIER)S0277-5387(17)30759-3 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Novikov, S.A. verfasserin aut Mg, Ca and Ba glutaratouranylates – Synthesis and structure 2017 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt = C5H7O4 − (hydroglutarate) anions. The structures of compounds 1–3 contain 1D [UO2(glt)(Hglt)]− units that belong to the AQ02B01 (A = UO2 2+, Q02 = glt, B01 = Hglt) crystallochemical group. The different roles of alkaline earth R2+ cations in the structures and the flexibility of the glutarate anions account for the structural distinctions of 1–3. The diverse ways for the connection between the R2+ ions and the [UO2(glt)(Hglt)]− chains, the water content and the geometry of the uranyl-glutarate units present the main structural features of the new complexes. A comparative analysis based on Pauling's second rule of 1–3 and alkali glutaratouranylates has allowed an explanation of their structural dissimilarity. Uranium Coordination polymers Glutarate Structures Serezhkina, L.B. verfasserin aut Grigoriev, M.S. verfasserin aut Serezhkin, V.N. verfasserin aut Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 141, Seite 147-152 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:141 pages:147-152 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 141 147-152
language	English
source	Enthalten in Polyhedron 141, Seite 147-152 volume:141 pages:147-152
sourceStr	Enthalten in Polyhedron 141, Seite 147-152 volume:141 pages:147-152
format_phy_str_mv	Article
bklname	Chemie: Allgemeines
institution	findex.gbv.de
topic_facet	Uranium Coordination polymers Glutarate Structures
dewey-raw	540
isfreeaccess_bool	false
container_title	Polyhedron
authorswithroles_txt_mv	Novikov, S.A. @@aut@@ Serezhkina, L.B. @@aut@@ Grigoriev, M.S. @@aut@@ Serezhkin, V.N. @@aut@@
publishDateDaySort_date	2017-01-01T00:00:00Z
hierarchy_top_id	320402967
dewey-sort	3540
id	ELV00155090X
language_de	englisch
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author	Novikov, S.A.
spellingShingle	Novikov, S.A. ddc 540 bkl 35.00 misc Uranium misc Coordination polymers misc Glutarate misc Structures Mg, Ca and Ba glutaratouranylates – Synthesis and structure
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topic_title	540 DE-600 35.00 bkl Mg, Ca and Ba glutaratouranylates – Synthesis and structure Uranium Coordination polymers Glutarate Structures
topic	ddc 540 bkl 35.00 misc Uranium misc Coordination polymers misc Glutarate misc Structures
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title	Mg, Ca and Ba glutaratouranylates – Synthesis and structure
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title_full	Mg, Ca and Ba glutaratouranylates – Synthesis and structure
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author_browse	Novikov, S.A. Serezhkina, L.B. Grigoriev, M.S. Serezhkin, V.N.
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title_sort	mg, ca and ba glutaratouranylates – synthesis and structure
title_auth	Mg, Ca and Ba glutaratouranylates – Synthesis and structure
abstract	Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt = C5H7O4 − (hydroglutarate) anions. The structures of compounds 1–3 contain 1D [UO2(glt)(Hglt)]− units that belong to the AQ02B01 (A = UO2 2+, Q02 = glt, B01 = Hglt) crystallochemical group. The different roles of alkaline earth R2+ cations in the structures and the flexibility of the glutarate anions account for the structural distinctions of 1–3. The diverse ways for the connection between the R2+ ions and the [UO2(glt)(Hglt)]− chains, the water content and the geometry of the uranyl-glutarate units present the main structural features of the new complexes. A comparative analysis based on Pauling's second rule of 1–3 and alkali glutaratouranylates has allowed an explanation of their structural dissimilarity.
abstractGer	Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt = C5H7O4 − (hydroglutarate) anions. The structures of compounds 1–3 contain 1D [UO2(glt)(Hglt)]− units that belong to the AQ02B01 (A = UO2 2+, Q02 = glt, B01 = Hglt) crystallochemical group. The different roles of alkaline earth R2+ cations in the structures and the flexibility of the glutarate anions account for the structural distinctions of 1–3. The diverse ways for the connection between the R2+ ions and the [UO2(glt)(Hglt)]− chains, the water content and the geometry of the uranyl-glutarate units present the main structural features of the new complexes. A comparative analysis based on Pauling's second rule of 1–3 and alkali glutaratouranylates has allowed an explanation of their structural dissimilarity.
abstract_unstemmed	Three novel uranyl coordination polymers were synthesized and structurally characterized by single crystal X-ray diffraction – [Mg(H2O)6][UO2(glt)(Hglt)]2·6H2O (1), [Ca(H2O)4][UO2(glt)(Hglt)]2·4H2O (2) and [Ba(H2O)5][UO2(glt)(Hglt)]2·2H2O (3), where glt = C5H6O4 2− (glutarate) and Hglt = C5H7O4 − (hydroglutarate) anions. The structures of compounds 1–3 contain 1D [UO2(glt)(Hglt)]− units that belong to the AQ02B01 (A = UO2 2+, Q02 = glt, B01 = Hglt) crystallochemical group. The different roles of alkaline earth R2+ cations in the structures and the flexibility of the glutarate anions account for the structural distinctions of 1–3. The diverse ways for the connection between the R2+ ions and the [UO2(glt)(Hglt)]− chains, the water content and the geometry of the uranyl-glutarate units present the main structural features of the new complexes. A comparative analysis based on Pauling's second rule of 1–3 and alkali glutaratouranylates has allowed an explanation of their structural dissimilarity.
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title_short	Mg, Ca and Ba glutaratouranylates – Synthesis and structure
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author2	Serezhkina, L.B. Grigoriev, M.S. Serezhkin, V.N.
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doi_str	10.1016/j.poly.2017.11.031
up_date	2024-07-06T21:45:38.132Z
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Mg, Ca and Ba glutaratouranylates – Synthesis and structure

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