Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber
In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal p...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Gong, Xueyong [verfasserIn] Dang, Guangyao [verfasserIn] Guo, Jing [verfasserIn] Liu, Yuanfa [verfasserIn] Gong, Yumei [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2019 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: International journal of biological macromolecules - New York, NY [u.a.] : Elsevier, 1979, 131, Seite 192-200 |
|---|---|
| Übergeordnetes Werk: |
volume:131 ; pages:192-200 |
| DOI / URN: |
10.1016/j.ijbiomac.2019.02.168 |
|---|
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| 520 | |a In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal property was characterized by DSC, and the morphology features was analyzed by SEM and EDS. The NMR result demonstrates there are chemical shifts at δ = 155.6 ppm indicating CC has been successfully introduced via acylation，and at δ = 70.06 ppm indicating that allyloxy polyethylene glycol (APEG) has been grafted onto feather keratin (FK). The DSC results show an decline in the endothermic peak related to melting of the APEG from 54.87 °C to 40.1 °C (phase change fiber), indicating the strong interaction between sodium alginate (SA) and feather keratin-g-allyloxy polyethylene glycol (FK-g-APEG). The mechanical properties test shows that the optimal spinning temperature is 40 °C, and the optimal Centrifugal speed is 500 r/min. | ||
| 650 | 4 | |a Phase change materials | |
| 650 | 4 | |a Composite fiber | |
| 650 | 4 | |a Centrifugal spinning | |
| 650 | 4 | |a Feather keratin | |
| 700 | 1 | |a Dang, Guangyao |e verfasserin |4 aut | |
| 700 | 1 | |a Guo, Jing |e verfasserin |4 aut | |
| 700 | 1 | |a Liu, Yuanfa |e verfasserin |4 aut | |
| 700 | 1 | |a Gong, Yumei |e verfasserin |4 aut | |
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10.1016/j.ijbiomac.2019.02.168 doi (DE-627)ELV00217572X (ELSEVIER)S0141-8130(18)37225-8 DE-627 ger DE-627 rda eng 540 570 DE-600 BIODIV DE-30 fid 35.80 bkl 58.30 bkl Gong, Xueyong verfasserin (orcid)0000-0001-6675-2262 aut Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal property was characterized by DSC, and the morphology features was analyzed by SEM and EDS. The NMR result demonstrates there are chemical shifts at δ = 155.6 ppm indicating CC has been successfully introduced via acylation，and at δ = 70.06 ppm indicating that allyloxy polyethylene glycol (APEG) has been grafted onto feather keratin (FK). The DSC results show an decline in the endothermic peak related to melting of the APEG from 54.87 °C to 40.1 °C (phase change fiber), indicating the strong interaction between sodium alginate (SA) and feather keratin-g-allyloxy polyethylene glycol (FK-g-APEG). The mechanical properties test shows that the optimal spinning temperature is 40 °C, and the optimal Centrifugal speed is 500 r/min. Phase change materials Composite fiber Centrifugal spinning Feather keratin Dang, Guangyao verfasserin aut Guo, Jing verfasserin aut Liu, Yuanfa verfasserin aut Gong, Yumei verfasserin aut Enthalten in International journal of biological macromolecules New York, NY [u.a.] : Elsevier, 1979 131, Seite 192-200 Online-Ressource (DE-627)30089502X (DE-600)1483284-7 (DE-576)259270814 1879-0003 nnns volume:131 pages:192-200 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-BIODIV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.80 Makromolekulare Chemie 58.30 Biotechnologie AR 131 192-200 |
| spelling |
10.1016/j.ijbiomac.2019.02.168 doi (DE-627)ELV00217572X (ELSEVIER)S0141-8130(18)37225-8 DE-627 ger DE-627 rda eng 540 570 DE-600 BIODIV DE-30 fid 35.80 bkl 58.30 bkl Gong, Xueyong verfasserin (orcid)0000-0001-6675-2262 aut Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal property was characterized by DSC, and the morphology features was analyzed by SEM and EDS. The NMR result demonstrates there are chemical shifts at δ = 155.6 ppm indicating CC has been successfully introduced via acylation，and at δ = 70.06 ppm indicating that allyloxy polyethylene glycol (APEG) has been grafted onto feather keratin (FK). The DSC results show an decline in the endothermic peak related to melting of the APEG from 54.87 °C to 40.1 °C (phase change fiber), indicating the strong interaction between sodium alginate (SA) and feather keratin-g-allyloxy polyethylene glycol (FK-g-APEG). The mechanical properties test shows that the optimal spinning temperature is 40 °C, and the optimal Centrifugal speed is 500 r/min. Phase change materials Composite fiber Centrifugal spinning Feather keratin Dang, Guangyao verfasserin aut Guo, Jing verfasserin aut Liu, Yuanfa verfasserin aut Gong, Yumei verfasserin aut Enthalten in International journal of biological macromolecules New York, NY [u.a.] : Elsevier, 1979 131, Seite 192-200 Online-Ressource (DE-627)30089502X (DE-600)1483284-7 (DE-576)259270814 1879-0003 nnns volume:131 pages:192-200 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-BIODIV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.80 Makromolekulare Chemie 58.30 Biotechnologie AR 131 192-200 |
| allfields_unstemmed |
10.1016/j.ijbiomac.2019.02.168 doi (DE-627)ELV00217572X (ELSEVIER)S0141-8130(18)37225-8 DE-627 ger DE-627 rda eng 540 570 DE-600 BIODIV DE-30 fid 35.80 bkl 58.30 bkl Gong, Xueyong verfasserin (orcid)0000-0001-6675-2262 aut Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal property was characterized by DSC, and the morphology features was analyzed by SEM and EDS. The NMR result demonstrates there are chemical shifts at δ = 155.6 ppm indicating CC has been successfully introduced via acylation，and at δ = 70.06 ppm indicating that allyloxy polyethylene glycol (APEG) has been grafted onto feather keratin (FK). The DSC results show an decline in the endothermic peak related to melting of the APEG from 54.87 °C to 40.1 °C (phase change fiber), indicating the strong interaction between sodium alginate (SA) and feather keratin-g-allyloxy polyethylene glycol (FK-g-APEG). The mechanical properties test shows that the optimal spinning temperature is 40 °C, and the optimal Centrifugal speed is 500 r/min. Phase change materials Composite fiber Centrifugal spinning Feather keratin Dang, Guangyao verfasserin aut Guo, Jing verfasserin aut Liu, Yuanfa verfasserin aut Gong, Yumei verfasserin aut Enthalten in International journal of biological macromolecules New York, NY [u.a.] : Elsevier, 1979 131, Seite 192-200 Online-Ressource (DE-627)30089502X (DE-600)1483284-7 (DE-576)259270814 1879-0003 nnns volume:131 pages:192-200 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-BIODIV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.80 Makromolekulare Chemie 58.30 Biotechnologie AR 131 192-200 |
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10.1016/j.ijbiomac.2019.02.168 doi (DE-627)ELV00217572X (ELSEVIER)S0141-8130(18)37225-8 DE-627 ger DE-627 rda eng 540 570 DE-600 BIODIV DE-30 fid 35.80 bkl 58.30 bkl Gong, Xueyong verfasserin (orcid)0000-0001-6675-2262 aut Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal property was characterized by DSC, and the morphology features was analyzed by SEM and EDS. The NMR result demonstrates there are chemical shifts at δ = 155.6 ppm indicating CC has been successfully introduced via acylation，and at δ = 70.06 ppm indicating that allyloxy polyethylene glycol (APEG) has been grafted onto feather keratin (FK). The DSC results show an decline in the endothermic peak related to melting of the APEG from 54.87 °C to 40.1 °C (phase change fiber), indicating the strong interaction between sodium alginate (SA) and feather keratin-g-allyloxy polyethylene glycol (FK-g-APEG). The mechanical properties test shows that the optimal spinning temperature is 40 °C, and the optimal Centrifugal speed is 500 r/min. Phase change materials Composite fiber Centrifugal spinning Feather keratin Dang, Guangyao verfasserin aut Guo, Jing verfasserin aut Liu, Yuanfa verfasserin aut Gong, Yumei verfasserin aut Enthalten in International journal of biological macromolecules New York, NY [u.a.] : Elsevier, 1979 131, Seite 192-200 Online-Ressource (DE-627)30089502X (DE-600)1483284-7 (DE-576)259270814 1879-0003 nnns volume:131 pages:192-200 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-BIODIV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.80 Makromolekulare Chemie 58.30 Biotechnologie AR 131 192-200 |
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10.1016/j.ijbiomac.2019.02.168 doi (DE-627)ELV00217572X (ELSEVIER)S0141-8130(18)37225-8 DE-627 ger DE-627 rda eng 540 570 DE-600 BIODIV DE-30 fid 35.80 bkl 58.30 bkl Gong, Xueyong verfasserin (orcid)0000-0001-6675-2262 aut Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal property was characterized by DSC, and the morphology features was analyzed by SEM and EDS. The NMR result demonstrates there are chemical shifts at δ = 155.6 ppm indicating CC has been successfully introduced via acylation，and at δ = 70.06 ppm indicating that allyloxy polyethylene glycol (APEG) has been grafted onto feather keratin (FK). The DSC results show an decline in the endothermic peak related to melting of the APEG from 54.87 °C to 40.1 °C (phase change fiber), indicating the strong interaction between sodium alginate (SA) and feather keratin-g-allyloxy polyethylene glycol (FK-g-APEG). The mechanical properties test shows that the optimal spinning temperature is 40 °C, and the optimal Centrifugal speed is 500 r/min. Phase change materials Composite fiber Centrifugal spinning Feather keratin Dang, Guangyao verfasserin aut Guo, Jing verfasserin aut Liu, Yuanfa verfasserin aut Gong, Yumei verfasserin aut Enthalten in International journal of biological macromolecules New York, NY [u.a.] : Elsevier, 1979 131, Seite 192-200 Online-Ressource (DE-627)30089502X (DE-600)1483284-7 (DE-576)259270814 1879-0003 nnns volume:131 pages:192-200 GBV_USEFLAG_U SYSFLAG_U GBV_ELV FID-BIODIV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.80 Makromolekulare Chemie 58.30 Biotechnologie AR 131 192-200 |
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Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber |
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Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber |
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Gong, Xueyong |
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International journal of biological macromolecules |
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Gong, Xueyong Dang, Guangyao Guo, Jing Liu, Yuanfa Gong, Yumei |
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Gong, Xueyong |
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10.1016/j.ijbiomac.2019.02.168 |
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sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber |
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Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber |
| abstract |
In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal property was characterized by DSC, and the morphology features was analyzed by SEM and EDS. The NMR result demonstrates there are chemical shifts at δ = 155.6 ppm indicating CC has been successfully introduced via acylation，and at δ = 70.06 ppm indicating that allyloxy polyethylene glycol (APEG) has been grafted onto feather keratin (FK). The DSC results show an decline in the endothermic peak related to melting of the APEG from 54.87 °C to 40.1 °C (phase change fiber), indicating the strong interaction between sodium alginate (SA) and feather keratin-g-allyloxy polyethylene glycol (FK-g-APEG). The mechanical properties test shows that the optimal spinning temperature is 40 °C, and the optimal Centrifugal speed is 500 r/min. |
| abstractGer |
In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal property was characterized by DSC, and the morphology features was analyzed by SEM and EDS. The NMR result demonstrates there are chemical shifts at δ = 155.6 ppm indicating CC has been successfully introduced via acylation，and at δ = 70.06 ppm indicating that allyloxy polyethylene glycol (APEG) has been grafted onto feather keratin (FK). The DSC results show an decline in the endothermic peak related to melting of the APEG from 54.87 °C to 40.1 °C (phase change fiber), indicating the strong interaction between sodium alginate (SA) and feather keratin-g-allyloxy polyethylene glycol (FK-g-APEG). The mechanical properties test shows that the optimal spinning temperature is 40 °C, and the optimal Centrifugal speed is 500 r/min. |
| abstract_unstemmed |
In this study, the novel sodium alginate/feather keratin-g-allyloxy polyethylene glycol (SA/FK-g-APEG) composite phase change fiber was designed and fabricated via centrifugal spinning for the first time. The chemical structure of the composite fiber was characterized by FT-IF and NMR, the thermal property was characterized by DSC, and the morphology features was analyzed by SEM and EDS. The NMR result demonstrates there are chemical shifts at δ = 155.6 ppm indicating CC has been successfully introduced via acylation，and at δ = 70.06 ppm indicating that allyloxy polyethylene glycol (APEG) has been grafted onto feather keratin (FK). The DSC results show an decline in the endothermic peak related to melting of the APEG from 54.87 °C to 40.1 °C (phase change fiber), indicating the strong interaction between sodium alginate (SA) and feather keratin-g-allyloxy polyethylene glycol (FK-g-APEG). The mechanical properties test shows that the optimal spinning temperature is 40 °C, and the optimal Centrifugal speed is 500 r/min. |
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Sodium alginate/feather keratin-g-allyloxy polyethylene glycol composite phase change fiber |
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Dang, Guangyao Guo, Jing Liu, Yuanfa Gong, Yumei |
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