The microstructure and texture of Gilsocarbon graphite
The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes i...
Ausführliche Beschreibung
Autor*in: |
Shen, Ke [verfasserIn] Yu, Suyuan [verfasserIn] Kang, Feiyu [verfasserIn] |
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Format: |
E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2019 |
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Übergeordnetes Werk: |
Enthalten in: Carbon - Amsterdam [u.a.] : Elsevier Science, 1963, 153, Seite 428-437 |
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Übergeordnetes Werk: |
volume:153 ; pages:428-437 |
DOI / URN: |
10.1016/j.carbon.2019.06.108 |
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Katalog-ID: |
ELV002827980 |
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520 | |a The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes in nuclear graphite. The texture of nuclear graphite involves the preferred orientation of graphite crystallites and the domain structure. This study developed a technique based on combined micro-Raman spectroscopy mapping and atomic force microscope, and demonstrate the application of this technique to texture characterization of GCMB Gilsocarbon graphite. A crystallite orientation analysis approach was proposed to describe the local arrangement of graphite crystallites. For comparison, the texture characterization results are present for Gilsonite coke filler, and different parts of binder phase, respectively. The domain orientation within Gilsonite coke filler is irregular, but statistically follows the spherical particles. The major binder phase shows less ordered texture, however, certain parts of the binder phase shows very ordered planar crystallite orientation, and even larger lateral crystal size than that of filler particle. The clear description of texture provides the bases for future simulations and investigation of the properties and irradiation performance of Gilsocarbon graphite. | ||
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2019 |
allfields |
10.1016/j.carbon.2019.06.108 doi (DE-627)ELV002827980 (ELSEVIER)S0008-6223(19)30684-0 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Shen, Ke verfasserin aut The microstructure and texture of Gilsocarbon graphite 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes in nuclear graphite. The texture of nuclear graphite involves the preferred orientation of graphite crystallites and the domain structure. This study developed a technique based on combined micro-Raman spectroscopy mapping and atomic force microscope, and demonstrate the application of this technique to texture characterization of GCMB Gilsocarbon graphite. A crystallite orientation analysis approach was proposed to describe the local arrangement of graphite crystallites. For comparison, the texture characterization results are present for Gilsonite coke filler, and different parts of binder phase, respectively. The domain orientation within Gilsonite coke filler is irregular, but statistically follows the spherical particles. The major binder phase shows less ordered texture, however, certain parts of the binder phase shows very ordered planar crystallite orientation, and even larger lateral crystal size than that of filler particle. The clear description of texture provides the bases for future simulations and investigation of the properties and irradiation performance of Gilsocarbon graphite. Yu, Suyuan verfasserin aut Kang, Feiyu verfasserin aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 153, Seite 428-437 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:153 pages:428-437 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 153 428-437 |
spelling |
10.1016/j.carbon.2019.06.108 doi (DE-627)ELV002827980 (ELSEVIER)S0008-6223(19)30684-0 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Shen, Ke verfasserin aut The microstructure and texture of Gilsocarbon graphite 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes in nuclear graphite. The texture of nuclear graphite involves the preferred orientation of graphite crystallites and the domain structure. This study developed a technique based on combined micro-Raman spectroscopy mapping and atomic force microscope, and demonstrate the application of this technique to texture characterization of GCMB Gilsocarbon graphite. A crystallite orientation analysis approach was proposed to describe the local arrangement of graphite crystallites. For comparison, the texture characterization results are present for Gilsonite coke filler, and different parts of binder phase, respectively. The domain orientation within Gilsonite coke filler is irregular, but statistically follows the spherical particles. The major binder phase shows less ordered texture, however, certain parts of the binder phase shows very ordered planar crystallite orientation, and even larger lateral crystal size than that of filler particle. The clear description of texture provides the bases for future simulations and investigation of the properties and irradiation performance of Gilsocarbon graphite. Yu, Suyuan verfasserin aut Kang, Feiyu verfasserin aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 153, Seite 428-437 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:153 pages:428-437 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 153 428-437 |
allfields_unstemmed |
10.1016/j.carbon.2019.06.108 doi (DE-627)ELV002827980 (ELSEVIER)S0008-6223(19)30684-0 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Shen, Ke verfasserin aut The microstructure and texture of Gilsocarbon graphite 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes in nuclear graphite. The texture of nuclear graphite involves the preferred orientation of graphite crystallites and the domain structure. This study developed a technique based on combined micro-Raman spectroscopy mapping and atomic force microscope, and demonstrate the application of this technique to texture characterization of GCMB Gilsocarbon graphite. A crystallite orientation analysis approach was proposed to describe the local arrangement of graphite crystallites. For comparison, the texture characterization results are present for Gilsonite coke filler, and different parts of binder phase, respectively. The domain orientation within Gilsonite coke filler is irregular, but statistically follows the spherical particles. The major binder phase shows less ordered texture, however, certain parts of the binder phase shows very ordered planar crystallite orientation, and even larger lateral crystal size than that of filler particle. The clear description of texture provides the bases for future simulations and investigation of the properties and irradiation performance of Gilsocarbon graphite. Yu, Suyuan verfasserin aut Kang, Feiyu verfasserin aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 153, Seite 428-437 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:153 pages:428-437 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 153 428-437 |
allfieldsGer |
10.1016/j.carbon.2019.06.108 doi (DE-627)ELV002827980 (ELSEVIER)S0008-6223(19)30684-0 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Shen, Ke verfasserin aut The microstructure and texture of Gilsocarbon graphite 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes in nuclear graphite. The texture of nuclear graphite involves the preferred orientation of graphite crystallites and the domain structure. This study developed a technique based on combined micro-Raman spectroscopy mapping and atomic force microscope, and demonstrate the application of this technique to texture characterization of GCMB Gilsocarbon graphite. A crystallite orientation analysis approach was proposed to describe the local arrangement of graphite crystallites. For comparison, the texture characterization results are present for Gilsonite coke filler, and different parts of binder phase, respectively. The domain orientation within Gilsonite coke filler is irregular, but statistically follows the spherical particles. The major binder phase shows less ordered texture, however, certain parts of the binder phase shows very ordered planar crystallite orientation, and even larger lateral crystal size than that of filler particle. The clear description of texture provides the bases for future simulations and investigation of the properties and irradiation performance of Gilsocarbon graphite. Yu, Suyuan verfasserin aut Kang, Feiyu verfasserin aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 153, Seite 428-437 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:153 pages:428-437 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 153 428-437 |
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10.1016/j.carbon.2019.06.108 doi (DE-627)ELV002827980 (ELSEVIER)S0008-6223(19)30684-0 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Shen, Ke verfasserin aut The microstructure and texture of Gilsocarbon graphite 2019 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes in nuclear graphite. The texture of nuclear graphite involves the preferred orientation of graphite crystallites and the domain structure. This study developed a technique based on combined micro-Raman spectroscopy mapping and atomic force microscope, and demonstrate the application of this technique to texture characterization of GCMB Gilsocarbon graphite. A crystallite orientation analysis approach was proposed to describe the local arrangement of graphite crystallites. For comparison, the texture characterization results are present for Gilsonite coke filler, and different parts of binder phase, respectively. The domain orientation within Gilsonite coke filler is irregular, but statistically follows the spherical particles. The major binder phase shows less ordered texture, however, certain parts of the binder phase shows very ordered planar crystallite orientation, and even larger lateral crystal size than that of filler particle. The clear description of texture provides the bases for future simulations and investigation of the properties and irradiation performance of Gilsocarbon graphite. Yu, Suyuan verfasserin aut Kang, Feiyu verfasserin aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 153, Seite 428-437 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:153 pages:428-437 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 153 428-437 |
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Shen, Ke |
doi_str_mv |
10.1016/j.carbon.2019.06.108 |
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verfasserin |
title_sort |
the microstructure and texture of gilsocarbon graphite |
title_auth |
The microstructure and texture of Gilsocarbon graphite |
abstract |
The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes in nuclear graphite. The texture of nuclear graphite involves the preferred orientation of graphite crystallites and the domain structure. This study developed a technique based on combined micro-Raman spectroscopy mapping and atomic force microscope, and demonstrate the application of this technique to texture characterization of GCMB Gilsocarbon graphite. A crystallite orientation analysis approach was proposed to describe the local arrangement of graphite crystallites. For comparison, the texture characterization results are present for Gilsonite coke filler, and different parts of binder phase, respectively. The domain orientation within Gilsonite coke filler is irregular, but statistically follows the spherical particles. The major binder phase shows less ordered texture, however, certain parts of the binder phase shows very ordered planar crystallite orientation, and even larger lateral crystal size than that of filler particle. The clear description of texture provides the bases for future simulations and investigation of the properties and irradiation performance of Gilsocarbon graphite. |
abstractGer |
The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes in nuclear graphite. The texture of nuclear graphite involves the preferred orientation of graphite crystallites and the domain structure. This study developed a technique based on combined micro-Raman spectroscopy mapping and atomic force microscope, and demonstrate the application of this technique to texture characterization of GCMB Gilsocarbon graphite. A crystallite orientation analysis approach was proposed to describe the local arrangement of graphite crystallites. For comparison, the texture characterization results are present for Gilsonite coke filler, and different parts of binder phase, respectively. The domain orientation within Gilsonite coke filler is irregular, but statistically follows the spherical particles. The major binder phase shows less ordered texture, however, certain parts of the binder phase shows very ordered planar crystallite orientation, and even larger lateral crystal size than that of filler particle. The clear description of texture provides the bases for future simulations and investigation of the properties and irradiation performance of Gilsocarbon graphite. |
abstract_unstemmed |
The material properties of nuclear graphite are defined by the as-manufactured graphite texture and their evolution due to irradiation and oxidation in reactors. Thus an understanding of the graphite microstructure and texture is essential in simulating and the predicting material property changes in nuclear graphite. The texture of nuclear graphite involves the preferred orientation of graphite crystallites and the domain structure. This study developed a technique based on combined micro-Raman spectroscopy mapping and atomic force microscope, and demonstrate the application of this technique to texture characterization of GCMB Gilsocarbon graphite. A crystallite orientation analysis approach was proposed to describe the local arrangement of graphite crystallites. For comparison, the texture characterization results are present for Gilsonite coke filler, and different parts of binder phase, respectively. The domain orientation within Gilsonite coke filler is irregular, but statistically follows the spherical particles. The major binder phase shows less ordered texture, however, certain parts of the binder phase shows very ordered planar crystallite orientation, and even larger lateral crystal size than that of filler particle. The clear description of texture provides the bases for future simulations and investigation of the properties and irradiation performance of Gilsocarbon graphite. |
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title_short |
The microstructure and texture of Gilsocarbon graphite |
remote_bool |
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author2 |
Yu, Suyuan Kang, Feiyu |
author2Str |
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doi_str |
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up_date |
2024-07-06T17:35:23.056Z |
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