Microstructure and mechanical properties of ZrC coating on zirconium fabricated by interstitial carburization
Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon a...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Zhao, Ziyuan [verfasserIn] Liu, Fuyuan [verfasserIn] Wang, Qin [verfasserIn] Li, Junming [verfasserIn] Zhong, Lisheng [verfasserIn] Xu, Yunhua [verfasserIn] Hui, Pengfei [verfasserIn] Zhu, Jianlei [verfasserIn] Yan, Fuxue [verfasserIn] Zhao, Mingxuan [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2020 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of alloys and compounds - Lausanne : Elsevier, 1991, 834 |
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| Übergeordnetes Werk: |
volume:834 |
| DOI / URN: |
10.1016/j.jallcom.2020.155110 |
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ELV004092627 |
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| 245 | 1 | 0 | |a Microstructure and mechanical properties of ZrC coating on zirconium fabricated by interstitial carburization |
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| 520 | |a Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon atoms diffused into the surface of Zr forming a ZrC coating. The microstructure of the coating was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron backscattered diffraction (EBSD). The obtained coating was completely dense and pure ceramic, consisting of a single ZrC phase with a volume fraction of 100%. The diameter of ZrC grains exhibited a gradient distribution with a range of 180 nm to 5.9 μm. The thickness of the coating was proportional to the square root of the carburizing time, following the classical parabolic law, reaching a coating thickness of 7.2 μm after carburizing for 10 h. The microhardness tested on the coating surface reached 1500 HV and nanohardness measured on the cross-section of the ZrC coating reached 27 GPa, displaying a remarkable improvement compared to the zirconium substrate (192 HV and 3.6 GPa). The average fracture toughness of ZrC coating measured via Vickers indentation was 1.9 MPa·m1⁄2. In response to a scratch where the scratch load increased linearly from 0 to 100 N, the coating demonstrated excellent adhesion with the substrate. As per the obtained results, we expect that the interstitial carburization method can also be applied to various Zr-based alloys. | ||
| 650 | 4 | |a Hard coating | |
| 650 | 4 | |a Ceramic coating | |
| 650 | 4 | |a Diffusion | |
| 650 | 4 | |a Hot pressing | |
| 650 | 4 | |a Refractory material | |
| 650 | 4 | |a Carburizing | |
| 700 | 1 | |a Liu, Fuyuan |e verfasserin |4 aut | |
| 700 | 1 | |a Wang, Qin |e verfasserin |4 aut | |
| 700 | 1 | |a Li, Junming |e verfasserin |4 aut | |
| 700 | 1 | |a Zhong, Lisheng |e verfasserin |4 aut | |
| 700 | 1 | |a Xu, Yunhua |e verfasserin |4 aut | |
| 700 | 1 | |a Hui, Pengfei |e verfasserin |4 aut | |
| 700 | 1 | |a Zhu, Jianlei |e verfasserin |4 aut | |
| 700 | 1 | |a Yan, Fuxue |e verfasserin |4 aut | |
| 700 | 1 | |a Zhao, Mingxuan |e verfasserin |4 aut | |
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10.1016/j.jallcom.2020.155110 doi (DE-627)ELV004092627 (ELSEVIER)S0925-8388(20)31473-0 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Zhao, Ziyuan verfasserin aut Microstructure and mechanical properties of ZrC coating on zirconium fabricated by interstitial carburization 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon atoms diffused into the surface of Zr forming a ZrC coating. The microstructure of the coating was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron backscattered diffraction (EBSD). The obtained coating was completely dense and pure ceramic, consisting of a single ZrC phase with a volume fraction of 100%. The diameter of ZrC grains exhibited a gradient distribution with a range of 180 nm to 5.9 μm. The thickness of the coating was proportional to the square root of the carburizing time, following the classical parabolic law, reaching a coating thickness of 7.2 μm after carburizing for 10 h. The microhardness tested on the coating surface reached 1500 HV and nanohardness measured on the cross-section of the ZrC coating reached 27 GPa, displaying a remarkable improvement compared to the zirconium substrate (192 HV and 3.6 GPa). The average fracture toughness of ZrC coating measured via Vickers indentation was 1.9 MPa·m1⁄2. In response to a scratch where the scratch load increased linearly from 0 to 100 N, the coating demonstrated excellent adhesion with the substrate. As per the obtained results, we expect that the interstitial carburization method can also be applied to various Zr-based alloys. Hard coating Ceramic coating Diffusion Hot pressing Refractory material Carburizing Liu, Fuyuan verfasserin aut Wang, Qin verfasserin aut Li, Junming verfasserin aut Zhong, Lisheng verfasserin aut Xu, Yunhua verfasserin aut Hui, Pengfei verfasserin aut Zhu, Jianlei verfasserin aut Yan, Fuxue verfasserin aut Zhao, Mingxuan verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 834 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:834 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 834 |
| spelling |
10.1016/j.jallcom.2020.155110 doi (DE-627)ELV004092627 (ELSEVIER)S0925-8388(20)31473-0 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Zhao, Ziyuan verfasserin aut Microstructure and mechanical properties of ZrC coating on zirconium fabricated by interstitial carburization 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon atoms diffused into the surface of Zr forming a ZrC coating. The microstructure of the coating was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron backscattered diffraction (EBSD). The obtained coating was completely dense and pure ceramic, consisting of a single ZrC phase with a volume fraction of 100%. The diameter of ZrC grains exhibited a gradient distribution with a range of 180 nm to 5.9 μm. The thickness of the coating was proportional to the square root of the carburizing time, following the classical parabolic law, reaching a coating thickness of 7.2 μm after carburizing for 10 h. The microhardness tested on the coating surface reached 1500 HV and nanohardness measured on the cross-section of the ZrC coating reached 27 GPa, displaying a remarkable improvement compared to the zirconium substrate (192 HV and 3.6 GPa). The average fracture toughness of ZrC coating measured via Vickers indentation was 1.9 MPa·m1⁄2. In response to a scratch where the scratch load increased linearly from 0 to 100 N, the coating demonstrated excellent adhesion with the substrate. As per the obtained results, we expect that the interstitial carburization method can also be applied to various Zr-based alloys. Hard coating Ceramic coating Diffusion Hot pressing Refractory material Carburizing Liu, Fuyuan verfasserin aut Wang, Qin verfasserin aut Li, Junming verfasserin aut Zhong, Lisheng verfasserin aut Xu, Yunhua verfasserin aut Hui, Pengfei verfasserin aut Zhu, Jianlei verfasserin aut Yan, Fuxue verfasserin aut Zhao, Mingxuan verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 834 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:834 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 834 |
| allfields_unstemmed |
10.1016/j.jallcom.2020.155110 doi (DE-627)ELV004092627 (ELSEVIER)S0925-8388(20)31473-0 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Zhao, Ziyuan verfasserin aut Microstructure and mechanical properties of ZrC coating on zirconium fabricated by interstitial carburization 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon atoms diffused into the surface of Zr forming a ZrC coating. The microstructure of the coating was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron backscattered diffraction (EBSD). The obtained coating was completely dense and pure ceramic, consisting of a single ZrC phase with a volume fraction of 100%. The diameter of ZrC grains exhibited a gradient distribution with a range of 180 nm to 5.9 μm. The thickness of the coating was proportional to the square root of the carburizing time, following the classical parabolic law, reaching a coating thickness of 7.2 μm after carburizing for 10 h. The microhardness tested on the coating surface reached 1500 HV and nanohardness measured on the cross-section of the ZrC coating reached 27 GPa, displaying a remarkable improvement compared to the zirconium substrate (192 HV and 3.6 GPa). The average fracture toughness of ZrC coating measured via Vickers indentation was 1.9 MPa·m1⁄2. In response to a scratch where the scratch load increased linearly from 0 to 100 N, the coating demonstrated excellent adhesion with the substrate. As per the obtained results, we expect that the interstitial carburization method can also be applied to various Zr-based alloys. Hard coating Ceramic coating Diffusion Hot pressing Refractory material Carburizing Liu, Fuyuan verfasserin aut Wang, Qin verfasserin aut Li, Junming verfasserin aut Zhong, Lisheng verfasserin aut Xu, Yunhua verfasserin aut Hui, Pengfei verfasserin aut Zhu, Jianlei verfasserin aut Yan, Fuxue verfasserin aut Zhao, Mingxuan verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 834 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:834 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 834 |
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10.1016/j.jallcom.2020.155110 doi (DE-627)ELV004092627 (ELSEVIER)S0925-8388(20)31473-0 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Zhao, Ziyuan verfasserin aut Microstructure and mechanical properties of ZrC coating on zirconium fabricated by interstitial carburization 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon atoms diffused into the surface of Zr forming a ZrC coating. The microstructure of the coating was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron backscattered diffraction (EBSD). The obtained coating was completely dense and pure ceramic, consisting of a single ZrC phase with a volume fraction of 100%. The diameter of ZrC grains exhibited a gradient distribution with a range of 180 nm to 5.9 μm. The thickness of the coating was proportional to the square root of the carburizing time, following the classical parabolic law, reaching a coating thickness of 7.2 μm after carburizing for 10 h. The microhardness tested on the coating surface reached 1500 HV and nanohardness measured on the cross-section of the ZrC coating reached 27 GPa, displaying a remarkable improvement compared to the zirconium substrate (192 HV and 3.6 GPa). The average fracture toughness of ZrC coating measured via Vickers indentation was 1.9 MPa·m1⁄2. In response to a scratch where the scratch load increased linearly from 0 to 100 N, the coating demonstrated excellent adhesion with the substrate. As per the obtained results, we expect that the interstitial carburization method can also be applied to various Zr-based alloys. Hard coating Ceramic coating Diffusion Hot pressing Refractory material Carburizing Liu, Fuyuan verfasserin aut Wang, Qin verfasserin aut Li, Junming verfasserin aut Zhong, Lisheng verfasserin aut Xu, Yunhua verfasserin aut Hui, Pengfei verfasserin aut Zhu, Jianlei verfasserin aut Yan, Fuxue verfasserin aut Zhao, Mingxuan verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 834 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:834 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 834 |
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10.1016/j.jallcom.2020.155110 doi (DE-627)ELV004092627 (ELSEVIER)S0925-8388(20)31473-0 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Zhao, Ziyuan verfasserin aut Microstructure and mechanical properties of ZrC coating on zirconium fabricated by interstitial carburization 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon atoms diffused into the surface of Zr forming a ZrC coating. The microstructure of the coating was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron backscattered diffraction (EBSD). The obtained coating was completely dense and pure ceramic, consisting of a single ZrC phase with a volume fraction of 100%. The diameter of ZrC grains exhibited a gradient distribution with a range of 180 nm to 5.9 μm. The thickness of the coating was proportional to the square root of the carburizing time, following the classical parabolic law, reaching a coating thickness of 7.2 μm after carburizing for 10 h. The microhardness tested on the coating surface reached 1500 HV and nanohardness measured on the cross-section of the ZrC coating reached 27 GPa, displaying a remarkable improvement compared to the zirconium substrate (192 HV and 3.6 GPa). The average fracture toughness of ZrC coating measured via Vickers indentation was 1.9 MPa·m1⁄2. In response to a scratch where the scratch load increased linearly from 0 to 100 N, the coating demonstrated excellent adhesion with the substrate. As per the obtained results, we expect that the interstitial carburization method can also be applied to various Zr-based alloys. Hard coating Ceramic coating Diffusion Hot pressing Refractory material Carburizing Liu, Fuyuan verfasserin aut Wang, Qin verfasserin aut Li, Junming verfasserin aut Zhong, Lisheng verfasserin aut Xu, Yunhua verfasserin aut Hui, Pengfei verfasserin aut Zhu, Jianlei verfasserin aut Yan, Fuxue verfasserin aut Zhao, Mingxuan verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 834 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:834 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 834 |
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Hard coating Ceramic coating Diffusion Hot pressing Refractory material Carburizing |
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Zhao, Ziyuan @@aut@@ Liu, Fuyuan @@aut@@ Wang, Qin @@aut@@ Li, Junming @@aut@@ Zhong, Lisheng @@aut@@ Xu, Yunhua @@aut@@ Hui, Pengfei @@aut@@ Zhu, Jianlei @@aut@@ Yan, Fuxue @@aut@@ Zhao, Mingxuan @@aut@@ |
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2020-01-01T00:00:00Z |
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Zhao, Ziyuan |
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670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Microstructure and mechanical properties of ZrC coating on zirconium fabricated by interstitial carburization Hard coating Ceramic coating Diffusion Hot pressing Refractory material Carburizing |
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Zhao, Ziyuan Liu, Fuyuan Wang, Qin Li, Junming Zhong, Lisheng Xu, Yunhua Hui, Pengfei Zhu, Jianlei Yan, Fuxue Zhao, Mingxuan |
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microstructure and mechanical properties of zrc coating on zirconium fabricated by interstitial carburization |
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Microstructure and mechanical properties of ZrC coating on zirconium fabricated by interstitial carburization |
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Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon atoms diffused into the surface of Zr forming a ZrC coating. The microstructure of the coating was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron backscattered diffraction (EBSD). The obtained coating was completely dense and pure ceramic, consisting of a single ZrC phase with a volume fraction of 100%. The diameter of ZrC grains exhibited a gradient distribution with a range of 180 nm to 5.9 μm. The thickness of the coating was proportional to the square root of the carburizing time, following the classical parabolic law, reaching a coating thickness of 7.2 μm after carburizing for 10 h. The microhardness tested on the coating surface reached 1500 HV and nanohardness measured on the cross-section of the ZrC coating reached 27 GPa, displaying a remarkable improvement compared to the zirconium substrate (192 HV and 3.6 GPa). The average fracture toughness of ZrC coating measured via Vickers indentation was 1.9 MPa·m1⁄2. In response to a scratch where the scratch load increased linearly from 0 to 100 N, the coating demonstrated excellent adhesion with the substrate. As per the obtained results, we expect that the interstitial carburization method can also be applied to various Zr-based alloys. |
| abstractGer |
Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon atoms diffused into the surface of Zr forming a ZrC coating. The microstructure of the coating was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron backscattered diffraction (EBSD). The obtained coating was completely dense and pure ceramic, consisting of a single ZrC phase with a volume fraction of 100%. The diameter of ZrC grains exhibited a gradient distribution with a range of 180 nm to 5.9 μm. The thickness of the coating was proportional to the square root of the carburizing time, following the classical parabolic law, reaching a coating thickness of 7.2 μm after carburizing for 10 h. The microhardness tested on the coating surface reached 1500 HV and nanohardness measured on the cross-section of the ZrC coating reached 27 GPa, displaying a remarkable improvement compared to the zirconium substrate (192 HV and 3.6 GPa). The average fracture toughness of ZrC coating measured via Vickers indentation was 1.9 MPa·m1⁄2. In response to a scratch where the scratch load increased linearly from 0 to 100 N, the coating demonstrated excellent adhesion with the substrate. As per the obtained results, we expect that the interstitial carburization method can also be applied to various Zr-based alloys. |
| abstract_unstemmed |
Herein, ZrC coating was fabricated on the surface of zirconium via interstitial carburization. High-carbon steel was selected as the carbon source to supply the interstitial carbon atoms and was hot-pressed with zirconium substrate at 1150 °C and uniaxial pressure of 2 MPa. The interstitial carbon atoms diffused into the surface of Zr forming a ZrC coating. The microstructure of the coating was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron backscattered diffraction (EBSD). The obtained coating was completely dense and pure ceramic, consisting of a single ZrC phase with a volume fraction of 100%. The diameter of ZrC grains exhibited a gradient distribution with a range of 180 nm to 5.9 μm. The thickness of the coating was proportional to the square root of the carburizing time, following the classical parabolic law, reaching a coating thickness of 7.2 μm after carburizing for 10 h. The microhardness tested on the coating surface reached 1500 HV and nanohardness measured on the cross-section of the ZrC coating reached 27 GPa, displaying a remarkable improvement compared to the zirconium substrate (192 HV and 3.6 GPa). The average fracture toughness of ZrC coating measured via Vickers indentation was 1.9 MPa·m1⁄2. In response to a scratch where the scratch load increased linearly from 0 to 100 N, the coating demonstrated excellent adhesion with the substrate. As per the obtained results, we expect that the interstitial carburization method can also be applied to various Zr-based alloys. |
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| score |
7.4013615 |