Effects of precursor particle size on the performance of LiNi
Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemic...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Nie, Min [verfasserIn] Xia, Yun-Fei [verfasserIn] Wang, Zhen-Bo [verfasserIn] Yu, Fu-Da [verfasserIn] Zhang, Yin [verfasserIn] Wu, Jin [verfasserIn] Wu, Bing [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Ceramics international - Amsterdam [u.a.] : Elsevier Science, 1995, 41, Seite 15185-15192 |
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| Übergeordnetes Werk: |
volume:41 ; pages:15185-15192 |
| DOI / URN: |
10.1016/j.ceramint.2015.08.093 |
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| Katalog-ID: |
ELV005022347 |
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| 520 | |a Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. Although the CV and EIS tests show that NCM523-D3 has the maximal impedance among all samples, but the bigger crystallite dimension and larger SSA of NCM523-D3 are the key factors affecting the outstanding capacity and rate performance of the material. | ||
| 650 | 4 | |a LiNi | |
| 650 | 4 | |a Precursor particle size | |
| 650 | 4 | |a XRD Rietveld refinement | |
| 650 | 4 | |a BET specific surface area | |
| 650 | 4 | |a Crystallite dimension | |
| 700 | 1 | |a Xia, Yun-Fei |e verfasserin |4 aut | |
| 700 | 1 | |a Wang, Zhen-Bo |e verfasserin |4 aut | |
| 700 | 1 | |a Yu, Fu-Da |e verfasserin |4 aut | |
| 700 | 1 | |a Zhang, Yin |e verfasserin |4 aut | |
| 700 | 1 | |a Wu, Jin |e verfasserin |4 aut | |
| 700 | 1 | |a Wu, Bing |e verfasserin |4 aut | |
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10.1016/j.ceramint.2015.08.093 doi (DE-627)ELV005022347 (ELSEVIER)S0272-8842(15)01618-1 DE-627 ger DE-627 rda eng 670 DE-600 51.60 bkl 58.45 bkl Nie, Min verfasserin aut Effects of precursor particle size on the performance of LiNi 2015 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. Although the CV and EIS tests show that NCM523-D3 has the maximal impedance among all samples, but the bigger crystallite dimension and larger SSA of NCM523-D3 are the key factors affecting the outstanding capacity and rate performance of the material. LiNi Precursor particle size XRD Rietveld refinement BET specific surface area Crystallite dimension Xia, Yun-Fei verfasserin aut Wang, Zhen-Bo verfasserin aut Yu, Fu-Da verfasserin aut Zhang, Yin verfasserin aut Wu, Jin verfasserin aut Wu, Bing verfasserin aut Enthalten in Ceramics international Amsterdam [u.a.] : Elsevier Science, 1995 41, Seite 15185-15192 Online-Ressource (DE-627)320584305 (DE-600)2018052-4 (DE-576)25523063X 0272-8842 nnns volume:41 pages:15185-15192 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_34 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde 58.45 Gesteinshüttenkunde AR 41 15185-15192 |
| spelling |
10.1016/j.ceramint.2015.08.093 doi (DE-627)ELV005022347 (ELSEVIER)S0272-8842(15)01618-1 DE-627 ger DE-627 rda eng 670 DE-600 51.60 bkl 58.45 bkl Nie, Min verfasserin aut Effects of precursor particle size on the performance of LiNi 2015 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. Although the CV and EIS tests show that NCM523-D3 has the maximal impedance among all samples, but the bigger crystallite dimension and larger SSA of NCM523-D3 are the key factors affecting the outstanding capacity and rate performance of the material. LiNi Precursor particle size XRD Rietveld refinement BET specific surface area Crystallite dimension Xia, Yun-Fei verfasserin aut Wang, Zhen-Bo verfasserin aut Yu, Fu-Da verfasserin aut Zhang, Yin verfasserin aut Wu, Jin verfasserin aut Wu, Bing verfasserin aut Enthalten in Ceramics international Amsterdam [u.a.] : Elsevier Science, 1995 41, Seite 15185-15192 Online-Ressource (DE-627)320584305 (DE-600)2018052-4 (DE-576)25523063X 0272-8842 nnns volume:41 pages:15185-15192 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_34 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde 58.45 Gesteinshüttenkunde AR 41 15185-15192 |
| allfields_unstemmed |
10.1016/j.ceramint.2015.08.093 doi (DE-627)ELV005022347 (ELSEVIER)S0272-8842(15)01618-1 DE-627 ger DE-627 rda eng 670 DE-600 51.60 bkl 58.45 bkl Nie, Min verfasserin aut Effects of precursor particle size on the performance of LiNi 2015 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. Although the CV and EIS tests show that NCM523-D3 has the maximal impedance among all samples, but the bigger crystallite dimension and larger SSA of NCM523-D3 are the key factors affecting the outstanding capacity and rate performance of the material. LiNi Precursor particle size XRD Rietveld refinement BET specific surface area Crystallite dimension Xia, Yun-Fei verfasserin aut Wang, Zhen-Bo verfasserin aut Yu, Fu-Da verfasserin aut Zhang, Yin verfasserin aut Wu, Jin verfasserin aut Wu, Bing verfasserin aut Enthalten in Ceramics international Amsterdam [u.a.] : Elsevier Science, 1995 41, Seite 15185-15192 Online-Ressource (DE-627)320584305 (DE-600)2018052-4 (DE-576)25523063X 0272-8842 nnns volume:41 pages:15185-15192 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_34 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde 58.45 Gesteinshüttenkunde AR 41 15185-15192 |
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10.1016/j.ceramint.2015.08.093 doi (DE-627)ELV005022347 (ELSEVIER)S0272-8842(15)01618-1 DE-627 ger DE-627 rda eng 670 DE-600 51.60 bkl 58.45 bkl Nie, Min verfasserin aut Effects of precursor particle size on the performance of LiNi 2015 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. Although the CV and EIS tests show that NCM523-D3 has the maximal impedance among all samples, but the bigger crystallite dimension and larger SSA of NCM523-D3 are the key factors affecting the outstanding capacity and rate performance of the material. LiNi Precursor particle size XRD Rietveld refinement BET specific surface area Crystallite dimension Xia, Yun-Fei verfasserin aut Wang, Zhen-Bo verfasserin aut Yu, Fu-Da verfasserin aut Zhang, Yin verfasserin aut Wu, Jin verfasserin aut Wu, Bing verfasserin aut Enthalten in Ceramics international Amsterdam [u.a.] : Elsevier Science, 1995 41, Seite 15185-15192 Online-Ressource (DE-627)320584305 (DE-600)2018052-4 (DE-576)25523063X 0272-8842 nnns volume:41 pages:15185-15192 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_34 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde 58.45 Gesteinshüttenkunde AR 41 15185-15192 |
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10.1016/j.ceramint.2015.08.093 doi (DE-627)ELV005022347 (ELSEVIER)S0272-8842(15)01618-1 DE-627 ger DE-627 rda eng 670 DE-600 51.60 bkl 58.45 bkl Nie, Min verfasserin aut Effects of precursor particle size on the performance of LiNi 2015 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. Although the CV and EIS tests show that NCM523-D3 has the maximal impedance among all samples, but the bigger crystallite dimension and larger SSA of NCM523-D3 are the key factors affecting the outstanding capacity and rate performance of the material. LiNi Precursor particle size XRD Rietveld refinement BET specific surface area Crystallite dimension Xia, Yun-Fei verfasserin aut Wang, Zhen-Bo verfasserin aut Yu, Fu-Da verfasserin aut Zhang, Yin verfasserin aut Wu, Jin verfasserin aut Wu, Bing verfasserin aut Enthalten in Ceramics international Amsterdam [u.a.] : Elsevier Science, 1995 41, Seite 15185-15192 Online-Ressource (DE-627)320584305 (DE-600)2018052-4 (DE-576)25523063X 0272-8842 nnns volume:41 pages:15185-15192 GBV_USEFLAG_U SYSFLAG_U GBV_ELV GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_34 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_647 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2098 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde 58.45 Gesteinshüttenkunde AR 41 15185-15192 |
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Nie, Min |
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Nie, Min ddc 670 bkl 51.60 bkl 58.45 misc LiNi misc Precursor particle size misc XRD Rietveld refinement misc BET specific surface area misc Crystallite dimension Effects of precursor particle size on the performance of LiNi |
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670 DE-600 51.60 bkl 58.45 bkl Effects of precursor particle size on the performance of LiNi LiNi Precursor particle size XRD Rietveld refinement BET specific surface area Crystallite dimension |
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ddc 670 bkl 51.60 bkl 58.45 misc LiNi misc Precursor particle size misc XRD Rietveld refinement misc BET specific surface area misc Crystallite dimension |
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ddc 670 bkl 51.60 bkl 58.45 misc LiNi misc Precursor particle size misc XRD Rietveld refinement misc BET specific surface area misc Crystallite dimension |
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ddc 670 bkl 51.60 bkl 58.45 misc LiNi misc Precursor particle size misc XRD Rietveld refinement misc BET specific surface area misc Crystallite dimension |
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Effects of precursor particle size on the performance of LiNi |
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Effects of precursor particle size on the performance of LiNi |
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Nie, Min Xia, Yun-Fei Wang, Zhen-Bo Yu, Fu-Da Zhang, Yin Wu, Jin Wu, Bing |
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10.1016/j.ceramint.2015.08.093 |
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effects of precursor particle size on the performance of lini |
| title_auth |
Effects of precursor particle size on the performance of LiNi |
| abstract |
Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. Although the CV and EIS tests show that NCM523-D3 has the maximal impedance among all samples, but the bigger crystallite dimension and larger SSA of NCM523-D3 are the key factors affecting the outstanding capacity and rate performance of the material. |
| abstractGer |
Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. Although the CV and EIS tests show that NCM523-D3 has the maximal impedance among all samples, but the bigger crystallite dimension and larger SSA of NCM523-D3 are the key factors affecting the outstanding capacity and rate performance of the material. |
| abstract_unstemmed |
Ni0.5Co0.2Mn0.3(OH)2 precursors with different particle sizes and Li2CO3 were used as the raw materials to synthesis layered structure LiNi0.5Co0.2Mn0.3O2 material in this paper. XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. Although the CV and EIS tests show that NCM523-D3 has the maximal impedance among all samples, but the bigger crystallite dimension and larger SSA of NCM523-D3 are the key factors affecting the outstanding capacity and rate performance of the material. |
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XRD Rietveld refinement, BET specific surface area (SSA) analysis, particle distribution analysis and other electrochemical tests were performed to determine the effects of particle size on the performance of LiNi0.5Co0.2Mn0.3O2 material. Physical and electrochemical characterizations demonstrate that sample NCM523-D3 (3μm) has the best layered structure, and with the decrease in precursor particle size, the cation mixing degree shows up a decrease trend while the specific surface area increases from 0.236m2 g−1 to 0.937m2 g−1. Sample NCM523-D3 presents a better rate capability than NCM523-D6 and -D9, whose average capacity for 1C, 2C, 5C and 10C reaches 155.7, 145.1, 128.2 and 97.5mAhg−1, respectively. 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code="a">Wang, Zhen-Bo</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Yu, Fu-Da</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Zhang, Yin</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Wu, Jin</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Wu, Bing</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Ceramics international</subfield><subfield code="d">Amsterdam [u.a.] : Elsevier Science, 1995</subfield><subfield code="g">41, 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