Ag/Co

Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic perform...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Ashok, Anchu [verfasserIn] Kumar, Anand [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2020

Schlagwörter:	Glycerol electro-oxidation Solution combustion synthesis Second wave combustion synthesis

Übergeordnetes Werk:	Enthalten in: International journal of hydrogen energy - New York, NY [u.a.] : Elsevier, 1976, 46
Übergeordnetes Werk:	volume:46

DOI / URN:	10.1016/j.ijhydene.2020.04.118

Katalog-ID:	ELV005341663

Internformat


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520			\|a Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic performance. The bimetallic AgCo catalyst was synthesized via conventional solution combustion (AgCo-SCS); in addition, a novel second wave solution combustion synthesis (AgCo-SWC) was also used to synthesize a sample with a higher degree of surface alloying between the elements. XRD results of AgCo-SWC show peak shifts in 2θ to indicate the formation of a solid solution alloy that could improve the structural and electronic characteristic of the material. In AgCo-SCS, smaller Ag particles are found to be more on the surface, while in AgCo-SWC, Ag particles were largely covered with cobalt particles. The electro-oxidation results indicate that AgCo-SWC has improved electrochemical properties in terms of higher oxidation current and lower onset potential, which makes it an ideal candidate for glycerol oxidation reaction.
650		4	\|a Glycerol electro-oxidation
650		4	\|a Solution combustion synthesis
650		4	\|a Second wave combustion synthesis
700	1		\|a Kumar, Anand \|e verfasserin \|0 (orcid)0000-0003-1378-4986 \|4 aut
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912			\|a GBV_ILN_2005
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publishDate	2020
allfields	10.1016/j.ijhydene.2020.04.118 doi (DE-627)ELV005341663 (ELSEVIER)S0360-3199(20)31474-9 DE-627 ger DE-627 rda eng 660 620 DE-600 52.56 bkl Ashok, Anchu verfasserin aut Ag/Co 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic performance. The bimetallic AgCo catalyst was synthesized via conventional solution combustion (AgCo-SCS); in addition, a novel second wave solution combustion synthesis (AgCo-SWC) was also used to synthesize a sample with a higher degree of surface alloying between the elements. XRD results of AgCo-SWC show peak shifts in 2θ to indicate the formation of a solid solution alloy that could improve the structural and electronic characteristic of the material. In AgCo-SCS, smaller Ag particles are found to be more on the surface, while in AgCo-SWC, Ag particles were largely covered with cobalt particles. The electro-oxidation results indicate that AgCo-SWC has improved electrochemical properties in terms of higher oxidation current and lower onset potential, which makes it an ideal candidate for glycerol oxidation reaction. Glycerol electro-oxidation Solution combustion synthesis Second wave combustion synthesis Kumar, Anand verfasserin (orcid)0000-0003-1378-4986 aut Enthalten in International journal of hydrogen energy New York, NY [u.a.] : Elsevier, 1976 46 Online-Ressource (DE-627)301511357 (DE-600)1484487-4 (DE-576)096806397 1879-3487 nnns volume:46 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 52.56 Regenerative Energieformen alternative Energieformen AR 46
spelling	10.1016/j.ijhydene.2020.04.118 doi (DE-627)ELV005341663 (ELSEVIER)S0360-3199(20)31474-9 DE-627 ger DE-627 rda eng 660 620 DE-600 52.56 bkl Ashok, Anchu verfasserin aut Ag/Co 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic performance. The bimetallic AgCo catalyst was synthesized via conventional solution combustion (AgCo-SCS); in addition, a novel second wave solution combustion synthesis (AgCo-SWC) was also used to synthesize a sample with a higher degree of surface alloying between the elements. XRD results of AgCo-SWC show peak shifts in 2θ to indicate the formation of a solid solution alloy that could improve the structural and electronic characteristic of the material. In AgCo-SCS, smaller Ag particles are found to be more on the surface, while in AgCo-SWC, Ag particles were largely covered with cobalt particles. The electro-oxidation results indicate that AgCo-SWC has improved electrochemical properties in terms of higher oxidation current and lower onset potential, which makes it an ideal candidate for glycerol oxidation reaction. Glycerol electro-oxidation Solution combustion synthesis Second wave combustion synthesis Kumar, Anand verfasserin (orcid)0000-0003-1378-4986 aut Enthalten in International journal of hydrogen energy New York, NY [u.a.] : Elsevier, 1976 46 Online-Ressource (DE-627)301511357 (DE-600)1484487-4 (DE-576)096806397 1879-3487 nnns volume:46 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 52.56 Regenerative Energieformen alternative Energieformen AR 46
allfields_unstemmed	10.1016/j.ijhydene.2020.04.118 doi (DE-627)ELV005341663 (ELSEVIER)S0360-3199(20)31474-9 DE-627 ger DE-627 rda eng 660 620 DE-600 52.56 bkl Ashok, Anchu verfasserin aut Ag/Co 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic performance. The bimetallic AgCo catalyst was synthesized via conventional solution combustion (AgCo-SCS); in addition, a novel second wave solution combustion synthesis (AgCo-SWC) was also used to synthesize a sample with a higher degree of surface alloying between the elements. XRD results of AgCo-SWC show peak shifts in 2θ to indicate the formation of a solid solution alloy that could improve the structural and electronic characteristic of the material. In AgCo-SCS, smaller Ag particles are found to be more on the surface, while in AgCo-SWC, Ag particles were largely covered with cobalt particles. The electro-oxidation results indicate that AgCo-SWC has improved electrochemical properties in terms of higher oxidation current and lower onset potential, which makes it an ideal candidate for glycerol oxidation reaction. Glycerol electro-oxidation Solution combustion synthesis Second wave combustion synthesis Kumar, Anand verfasserin (orcid)0000-0003-1378-4986 aut Enthalten in International journal of hydrogen energy New York, NY [u.a.] : Elsevier, 1976 46 Online-Ressource (DE-627)301511357 (DE-600)1484487-4 (DE-576)096806397 1879-3487 nnns volume:46 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 52.56 Regenerative Energieformen alternative Energieformen AR 46
allfieldsGer	10.1016/j.ijhydene.2020.04.118 doi (DE-627)ELV005341663 (ELSEVIER)S0360-3199(20)31474-9 DE-627 ger DE-627 rda eng 660 620 DE-600 52.56 bkl Ashok, Anchu verfasserin aut Ag/Co 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic performance. The bimetallic AgCo catalyst was synthesized via conventional solution combustion (AgCo-SCS); in addition, a novel second wave solution combustion synthesis (AgCo-SWC) was also used to synthesize a sample with a higher degree of surface alloying between the elements. XRD results of AgCo-SWC show peak shifts in 2θ to indicate the formation of a solid solution alloy that could improve the structural and electronic characteristic of the material. In AgCo-SCS, smaller Ag particles are found to be more on the surface, while in AgCo-SWC, Ag particles were largely covered with cobalt particles. The electro-oxidation results indicate that AgCo-SWC has improved electrochemical properties in terms of higher oxidation current and lower onset potential, which makes it an ideal candidate for glycerol oxidation reaction. Glycerol electro-oxidation Solution combustion synthesis Second wave combustion synthesis Kumar, Anand verfasserin (orcid)0000-0003-1378-4986 aut Enthalten in International journal of hydrogen energy New York, NY [u.a.] : Elsevier, 1976 46 Online-Ressource (DE-627)301511357 (DE-600)1484487-4 (DE-576)096806397 1879-3487 nnns volume:46 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 52.56 Regenerative Energieformen alternative Energieformen AR 46
allfieldsSound	10.1016/j.ijhydene.2020.04.118 doi (DE-627)ELV005341663 (ELSEVIER)S0360-3199(20)31474-9 DE-627 ger DE-627 rda eng 660 620 DE-600 52.56 bkl Ashok, Anchu verfasserin aut Ag/Co 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic performance. The bimetallic AgCo catalyst was synthesized via conventional solution combustion (AgCo-SCS); in addition, a novel second wave solution combustion synthesis (AgCo-SWC) was also used to synthesize a sample with a higher degree of surface alloying between the elements. XRD results of AgCo-SWC show peak shifts in 2θ to indicate the formation of a solid solution alloy that could improve the structural and electronic characteristic of the material. In AgCo-SCS, smaller Ag particles are found to be more on the surface, while in AgCo-SWC, Ag particles were largely covered with cobalt particles. The electro-oxidation results indicate that AgCo-SWC has improved electrochemical properties in terms of higher oxidation current and lower onset potential, which makes it an ideal candidate for glycerol oxidation reaction. Glycerol electro-oxidation Solution combustion synthesis Second wave combustion synthesis Kumar, Anand verfasserin (orcid)0000-0003-1378-4986 aut Enthalten in International journal of hydrogen energy New York, NY [u.a.] : Elsevier, 1976 46 Online-Ressource (DE-627)301511357 (DE-600)1484487-4 (DE-576)096806397 1879-3487 nnns volume:46 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 52.56 Regenerative Energieformen alternative Energieformen AR 46
language	English
source	Enthalten in International journal of hydrogen energy 46 volume:46
sourceStr	Enthalten in International journal of hydrogen energy 46 volume:46
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institution	findex.gbv.de
topic_facet	Glycerol electro-oxidation Solution combustion synthesis Second wave combustion synthesis
dewey-raw	660
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container_title	International journal of hydrogen energy
authorswithroles_txt_mv	Ashok, Anchu @@aut@@ Kumar, Anand @@aut@@
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abstract	Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic performance. The bimetallic AgCo catalyst was synthesized via conventional solution combustion (AgCo-SCS); in addition, a novel second wave solution combustion synthesis (AgCo-SWC) was also used to synthesize a sample with a higher degree of surface alloying between the elements. XRD results of AgCo-SWC show peak shifts in 2θ to indicate the formation of a solid solution alloy that could improve the structural and electronic characteristic of the material. In AgCo-SCS, smaller Ag particles are found to be more on the surface, while in AgCo-SWC, Ag particles were largely covered with cobalt particles. The electro-oxidation results indicate that AgCo-SWC has improved electrochemical properties in terms of higher oxidation current and lower onset potential, which makes it an ideal candidate for glycerol oxidation reaction.
abstractGer	Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic performance. The bimetallic AgCo catalyst was synthesized via conventional solution combustion (AgCo-SCS); in addition, a novel second wave solution combustion synthesis (AgCo-SWC) was also used to synthesize a sample with a higher degree of surface alloying between the elements. XRD results of AgCo-SWC show peak shifts in 2θ to indicate the formation of a solid solution alloy that could improve the structural and electronic characteristic of the material. In AgCo-SCS, smaller Ag particles are found to be more on the surface, while in AgCo-SWC, Ag particles were largely covered with cobalt particles. The electro-oxidation results indicate that AgCo-SWC has improved electrochemical properties in terms of higher oxidation current and lower onset potential, which makes it an ideal candidate for glycerol oxidation reaction.
abstract_unstemmed	Herein, we report two different modes of combustion synthesis to prepare Ag/Co3O4 for glycerol electro-oxidation reaction. The synthesis technique allows us to deposit and disperse cobalt on the surface of silver and understand the effect of silver-cobalt interactions on the electrocatalytic performance. The bimetallic AgCo catalyst was synthesized via conventional solution combustion (AgCo-SCS); in addition, a novel second wave solution combustion synthesis (AgCo-SWC) was also used to synthesize a sample with a higher degree of surface alloying between the elements. XRD results of AgCo-SWC show peak shifts in 2θ to indicate the formation of a solid solution alloy that could improve the structural and electronic characteristic of the material. In AgCo-SCS, smaller Ag particles are found to be more on the surface, while in AgCo-SWC, Ag particles were largely covered with cobalt particles. The electro-oxidation results indicate that AgCo-SWC has improved electrochemical properties in terms of higher oxidation current and lower onset potential, which makes it an ideal candidate for glycerol oxidation reaction.
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title_short	Ag/Co
remote_bool	true
author2	Kumar, Anand
author2Str	Kumar, Anand
ppnlink	301511357
mediatype_str_mv	c
isOA_txt	false
hochschulschrift_bool	false
doi_str	10.1016/j.ijhydene.2020.04.118
up_date	2024-07-06T17:38:28.634Z
_version_	1803852194656550912
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